[Code of Federal Regulations] [Title 40, Volume 27] [Revised as of July 1, 2002] From the U.S. Government Printing Office via GPO Access [CITE: 40CFR761.253] [Page 652] TITLE 40--PROTECTION OF ENVIRONMENT CHAPTER I--ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) PART 761--POLYCHLORINATED BIPHENYLS (PCBs) MANUFACTURING, PROCESSING, DISTRIBUTION IN COMMERCE, AND USE PROHIBITIONS--Table of Contents Subpart M--Determining a PCB Concentration for Purposes of Abandonment or Disposal of Natural Gas Pipeline: Selecting Sample Sites, Collecting Surface Samples, and Analyzing Standard PCB Wipe Samples Sec. 761.253 Chemical analysis. (a) Extract PCBs from the standard wipe sample collection medium and clean-up the extracted PCBs in accordance with either Method 3500B/3540C or Method 3500B/3550B from EPA's SW-846, Test Methods for Evaluating Solid Waste, or a method validated under subpart Q of this part. Use Method 8082 from SW-846, or a method validated under subpart Q of this part, to analyze these extracts for PCBs. (b) Report all PCB sample concentrations in [mu]g/100 cm2 (16 square inches) of surface sampled. If sampling an area smaller than 100 cm2, report converted sample concentrations in accordance with Sec. 761.243(b).