[Code of Federal Regulations] [Title 49, Volume 2] [Revised as of October 1, 2003] From the U.S. Government Printing Office via GPO Access [CITE: 49CFR180.209] [Page 1060-1064] TITLE 49--TRANSPORTATION CHAPTER I--RESEARCH AND SPECIAL PROGRAMS ADMINISTRATION, DEPARTMENT OF TRANSPORTATION PART 180_CONTINUING QUALIFICATION AND MAINTENANCE OF PACKAGINGS--Table of Contents Subpart C_Qualification, Maintenance and Use of Cylinders Sec. 180.209 Requirements for requalification of specification cylinders. (a) Periodic qualification of cylinders. (1) Each specification cylinder that becomes due for periodic requalification, as specified in the following table, must be requalified and marked in conformance with the requirements of this subpart. Requalification records must be maintained in accordance with Sec. 180.215. Table 1 follows: Table 1--Requalification of Cylinders \1\ ------------------------------------------------------------------------ Specification under which Minimum test Requalification cylinder was made pressure (psig) \2\ period (years) ------------------------------------------------------------------------ DOT 3....................... 3000 psig........... 5 DOT 3A, 3AA................. 5/3 times service 5, 10, or 12 (see pressure, except Sec. 180.209(b), noncorrosive (f), (h), and (j) service (see Sec. 180.209(g)). DOT 3AL..................... 5/3 times service 5 or 12 (see Sec. pressure. 180.209(j)) DOT 3AX, 3AAX............... 5/3 times service 5 pressure. 3B, 3BN..................... 2 times service 5 or 10 (see Sec. pressure (see Sec. 180.209(f)) 180.209(g)). 3E.......................... Test not required... 3HT......................... 5/3 times service 3 (see Sec. Sec. pressure. 180.209(k) and 180.213(c)) 3T.......................... 5/3 times service 5 pressure. 4AA480...................... 2 times service 5 or 10 (see Sec. pressure (see Sec. 180.209(h)) 180.209(g)). 4B, 4BA, 4BW, 4B-240ET...... 2 times service 5, 10, or 12 (see pressure, except Sec. 180.209(e), non-corrosive (f), and (j)) service (see Sec. 180.209(g)). 4D, 4DA, 4DS................ 2 times service..... 5 DOT 4E...................... 2 times service 5 pressure, except non-corrosive (see Sec. 180.209(g)). 4L.......................... Test not required... 8, 8AL...................... .................... 10 or 20 (see Sec. 180.209(i)) Exemption cylinder.......... See current See current exemption. exemption Foreign cylinder (see Sec. As marked on 5 (see Sec. Sec. 173.301(j) of this cylinder, but not 180.209(l) and subchapter for restrictions less than 5/3 of 180.213(d)(2)) on use). any service or working pressure marking. ------------------------------------------------------------------------ \1\ Any cylinder not exceeding 2 inches outside diameter and less than 2 feet in length is excepted from volumetric expansion test. \2\ For cylinders not marked with a service pressure, see Sec. 173.301a(b) of this subchapter. (b) DOT 3A or 3AA cylinders. (1) A cylinder conforming to specification DOT 3A or 3AA with a water capacity of 56.7 kg (125 lb) or less that is removed from any cluster, bank, group, rack, or vehicle each time it is filled, may be requalified every ten years instead of every five years, provided the cylinder conforms to all of the following conditions: (i) The cylinder was manufactured after December 31, 1945. (ii) The cylinder is used exclusively for air; argon; cyclopropane; ethylene; helium; hydrogen; krypton; neon; nitrogen; nitrous oxide; oxygen; sulfur [[Page 1061]] hexafluoride; xenon; chlorinated hydrocarbons, fluorinated hydrocarbons, liquefied hydrocarbons, and mixtures thereof that are commercially free from corroding components; permitted mixtures of these gases (see Sec. 173.301(d) of this subchapter); and permitted mixtures of these gases with up to 30 percent by volume of carbon dioxide, provided the gas has a dew point at or below minus (52 [deg]F) at 1 atmosphere. (iii) Before each refill, the cylinder is removed from any cluster, bank, group, rack or vehicle and passes the hammer test specified in CGA Pamphlet C-6 (incorporated by reference; see Sec. 171.7 of this subchapter). (iv) The cylinder is dried immediately after hydrostatic testing to remove all traces of water. (v) The cylinder is not used for underwater breathing. (vi) Each cylinder is stamped with a five-pointed star at least one- fourth of an inch high immediately following the test date. (2) If, since the last required requalification, a cylinder has not been used exclusively for the gases specifically identified in paragraph (b)(1)(ii) of this section, but currently conforms with all other provisions of paragraph (b)(1) of this section, it may be requalified every 10 years instead of every five years, provided it is first requalified and examined as prescribed by Sec. 173.302a(b) (2), (3) and (4) of this subchapter. (3) Except as specified in paragraph (b)(2) of this section, if a cylinder, marked with a star, is filled with a compressed gas other than as specified in paragraph (b)(1)(ii) of this section, the star following the most recent test date must be obliterated. The cylinder must be requalified five years from the marked test date, or prior to the first filling with a compressed gas, if the required five-year requalification period has passed. (c) DOT 4-series cylinders. A DOT 4-series cylinder, except a 4L cylinder, that at any time shows evidence of a leak or of internal or external corrosion, denting, bulging or rough usage to the extent that it is likely to be weakened appreciably, or that has lost five percent or more of its official tare weight must be requalified before being refilled and offered for transportation. (Refer to CGA Pamphlet C-6 or C-6.3, as applicable, regarding cylinder weakening.) After testing, the actual tare weight must be recorded as the new tare weight. (d) Cylinders 5.44 kg (12 lb) or less with service pressures of 300 psig or less. A cylinder of 5.44 (12 lb) or less water capacity authorized for service pressure of 300 psig or less must be given a complete external visual inspection at the time periodic requalification becomes due. External visual inspection must be in accordance with CGA Pamphlet C-6 or C-6.1 (incorporated by reference; see Sec. 171.7 of this subchapter). The cylinder may be proof pressure tested. The test is successful if the cylinder, when examined under test pressure, does not display a defect described in Sec. 180.205(i)(1) (ii) or (iii). Upon successful completion of the test and inspection, the cylinder must be marked in accordance with Sec. 180.213. (e) Proof pressure test A cylinder made in conformance with specifications DOT 4B, 4BA, 4BW, or 4E used exclusively for: liquefied petroleum gas that meets the detail requirement limits in Table I of ASTM D 1835, ``Standard Specification for Liquefied Petroleum (LP) Gases'' (incorporated by reference; see Sec. 171.7 of this subchapter) or an equivalent standard containing the same limits; anhydrous dimethylamine; anhydrous methylamine; anhydrous trimethylamine; methyl chloride; methylacetylene-propadiene stabilized; or dichlorodifluoromethane, difluoroethane, difluorochloroethane, chlorodifluoromethane, chlorotetrafluoroethane, trifluorochloroethylene, or mixture thereof, or mixtures of one or more with trichlorofluoromethane; and commercially free from corroding components and protected externally by a suitable corrosion-resistant coating (such as galvanizing or painting) may be requalified by volumetric expansion testing every 12 years instead of every five years. As an alternative, the cylinder may be subjected to a proof pressure test at least two times the marked service pressure, but this latter type of test must be repeated every seven years after expiration of the first 12-year period. When subjected to a proof [[Page 1062]] pressure test, the cylinder must be carefully examined under test pressure and removed from service if a leak or defect is found. (f) Poisonous materials. A cylinder conforming to specification DOT 3A, 3AA, 3B, 4BA, or 4BW having a service pressure of 300 psig or less and used exclusively for methyl bromide, liquid; mixtures of methyl bromide and ethylene dibromide, liquid; mixtures of methyl bromide and chlorpicrin, liquid; mixtures of methyl bromide and petroleum solvents, liquid; or methyl bromide and nonflammable, nonliquefied compressed gas mixtures, liquid; commercially free of corroding components, and protected externally by a suitable corrosion resistant coating (such as galvanizing or painting) and internally by a suitable corrosion resistant lining (such as galvanizing) may be tested every 10 years instead of every five years, provided a visual internal and external examination of the cylinder is conducted every five years in accordance with CGA Pamphlet C-6 (incorporated by reference; see Sec. 171.7 of this subchapter). The cylinder must be examined at each filling, and rejected if a dent, corroded area, leak or other condition indicates possible weakness. (g) Visual inspections. A cylinder conforming to a specification listed in the table in this paragraph and used exclusively in the service indicated may, instead of a periodic hydrostatic test, be given a complete external visual inspection at the time periodic requalification becomes due. External visual inspection must be in accordance with CGA Pamphlet C-6 or C-6.3, as applicable (incorporated by reference; see Sec. 171.7 of this subchapter). When this inspection is used instead of hydrostatic pressure testing, subsequent inspections are required at five-year intervals after the first inspection. After May 31, 2004, inspections must be made only by persons holding a current RIN and the results recorded and maintained in accordance with Sec. 180.215. Records must include: date of inspection (month and year); DOT specification number; cylinder identification (registered symbol and serial number, date of manufacture, and owner); type of cylinder protective coating (including statement as to need of refinishing or recoating); conditions checked (e.g., leakage, corrosion, gouges, dents or digs in shell or heads, broken or damaged footring or protective ring or fire damage); disposition of cylinder (returned to service, returned to cylinder manufacturer for repairs or condemned). A cylinder passing requalification by the external visual inspection must be marked in accordance with Sec. 180.213. Specification cylinders must be in exclusive service as shown in the following table: ------------------------------------------------------------------------ Cylinders conforming to-- Used exclusively for-- ------------------------------------------------------------------------ DOT 3A, DOT 3AA, DOT 3A480X, DOT 4AA480 Anhydrous ammonia of at least 99.95% purity. DOT 3A, DOT 3AA, DOT 3A480X, DOT 3B, Butadiene, inhibited, that is DOT 4B, DOT 4BA, DOT 4BW. commercially free from corroding components. DOT 3A, DOT 3A480X, DOT 3AA, DOT 3B, Cyclopropane that is DOT 4AA480, DOT 4B, DOT 4BA, DOT 4BW. commercially free from corroding components. DOT 3A, DOT 3AA, DOT 3A480X, DOT 4B, Chlorinated hydrocarbons and DOT 4BA, DOT 4BW, DOT 4E. mixtures thereof that are commercially free from corroding components. DOT 3A, DOT 3AA, DOT 3A480X, DOT 4B, Fluorinated hydrocarbons and DOT 4BA, DOT 4BW, DOT 4E. mixtures thereof that are commercially free from corroding components. DOT 3A, DOT 3AA, DOT 3A480X, DOT 3B, Liquefied hydrocarbon gas that DOT 4B, DOT 4BA, DOT 4BW, DOT 4E. is commercially free from corroding components. DOT 3A, DOT 3AA, DOT 3A480X, DOT 3B, Liquefied petroleum gas that DOT 4B, DOT 4BA, DOT 4BW, DOT 4E. meets the detail requirements limits in Table 1 of ASTM 1835, Standard Specification for Liquefied Petroleum (LP) Gases (incorporated by reference; see Sec. 171.7 of this subchapter) or an equivalent standard containing the same limits. DOT 3A, DOT 3AA, DOT 3B, DOT 4B, DOT Methylacetylene-propadiene, 4BA, DOT 4BW, DOT 4E. stabilized, that is commercially free from corroding components. DOT 3A, DOT 3AA, DOT 3B, DOT 4B, DOT Anhydrous mono, 4BA, DOT 4BW. di,trimethylamines that are commercially free from corroding components. DOT 4B240, DOT 4BW240.................. Ethyleneimine, stabilized. ------------------------------------------------------------------------ (h) Cylinders containing anhydrous ammonia. A cylinder conforming to specification DOT 3A, 3A480X, or 4AA480 [[Page 1063]] used exclusively for anhydrous ammonia, commercially free from corroding components, and protected externally by a suitable corrosion-resistant coating (such as paint) may be requalified every 10 years instead of every five years. (i) Requalification of DOT-8 series cylinders. (1) Each owner of a DOT-8 series cylinder used to transport acetylene must have the cylinder shell and the porous filler requalified in accordance with CGA Pamphlet C-13 (incorporated by reference; see Sec. 171.7 of this subchapter). Requalification must be performed in accordance with the following schedule: ---------------------------------------------------------------------------------------------------------------- Shell (visual inspection) Porous filler requalification requalification --------------------------------------- Date of cylinder manufacture ---------------------------------------- Initial Subsequent Initial Subsequent ---------------------------------------------------------------------------------------------------------------- Before January 1, 1991.......... Before January 1, 10 years.......... Before January 1, Not required. 2001. 2011. On or after January 1, 1991..... 10 years \1\...... 10 years.......... 3 to 20 years \2\. Not required. ---------------------------------------------------------------------------------------------------------------- \1\ Years from date of cylinder manufacture. \2\ For a cylinder manufactured on or after January 1, 1991, requalification of the porous filler must be performed no sooner than 5 years, and no later than 20 years, from the date of manufacture. (2) Unless requalified and marked in accordance with CGA Pamphlet C- 13 (incorporated by reference; see Sec. 171.7 of this subchapter) before October 1, 1994, an acetylene cylinder must be requalified by a person who holds a current RIN. (3) If a cylinder valve is replaced, a cylinder valve of the same weight must be used or the tare weight of the cylinder must be adjusted to compensate for valve weight differential. (4) The person performing a visual inspection or requalification must record the results as specified in Sec. 180.215. (5) The person performing a visual inspection or requalification must mark the cylinder as specified in Sec. 180.213. (j) Cylinder used as a fire extinguisher. Only a DOT specification cylinder used as a fire extinguisher and meeting Special Provision 18 in Sec. 172.102(c)(1) of this subchapter may be requalified in accordance with this paragraph (j). (1) A DOT 4B, 4BA, 4B240ET or 4BW cylinder may be tested as follows: (i) For a cylinder with a water capacity of 5.44 kg (12 lb) or less, by volumetric expansion test using the water jacket method or by proof pressure test. A requalification must be performed by the end of 12 years after the original test date and at 12-year intervals thereafter. (ii) For a cylinder having a water capacity over 5.44 kg (12 lb)-- (A) By proof pressure test. A requalification must be performed by the end of 12 years after the original test date and at 7-year intervals; or (B) By volumetric expansion test using the water jacket method. A requalification must be performed 12 years after the original test date and at 12-year intervals thereafter. (2) A DOT 3A, 3AA, or 3AL cylinder must be requalified by volumetric expansion test using the water jacket method. A requalification must be performed 12 years after the original test date and at 12-year intervals thereafter. (k) 3HT cylinders. In addition to the other requirements of this section, a cylinder marked DOT-3HT must be requalified in accordance with CGA Pamphlet C-8. (l) Requalification of foreign cylinders filled for export. A cylinder manufactured outside the United States, other than as provided in Sec. 171.12a of this subchapter, that has not been manufactured, inspected, tested and marked in accordance with part 178 of this subchapter may be filled with compressed gas in the United States, and shipped solely for export if it meets the following requirements, in addition to other requirements of this subchapter: (1) It has been inspected, tested and marked (with only the month and year of test) in conformance with the procedures and requirements of this subpart or the Associate Administrator has authorized the filling company to fill foreign cylinders under an alternative method of qualification; and [[Page 1064]] (2) It is offered for transportation in conformance with the requirements of Sec. 173.301(l) of this subchapter. [67 FR 51660, Aug. 8, 2002, as amended at 68 FR 24662, May 8, 2003; 68 FR 55544, Sept. 26, 2003; 68 FR 48572, Aug. 14, 2003]