[Code of Federal Regulations]
[Title 40, Volume 9]
[Revised as of July 1, 2006]
From the U.S. Government Printing Office via GPO Access
[CITE: 40CFR63.14]
[Page 63-68]
TITLE 40--PROTECTION OF ENVIRONMENT
CHAPTER I--ENVIRONMENTAL PROTECTION AGENCY (CONTINUED)
PART 63_NATIONAL EMISSION STANDARDS FOR HAZARDOUS AIR POLLUTANTS FOR
SOURCE CATEGORIES--Table of Contents
Subpart A_General Provisions
Sec. 63.14 Incorporations by reference.
(a) The materials listed in this section are incorporated by
reference in the corresponding sections noted. These incorporations by
reference were approved by the Director of the Federal Register in
accordance with 5 U.S.C. 552(a) and 1 CFR part 51. These materials are
incorporated as they exist on the date of the approval, and notice of
any change in these materials will be published in the Federal Register.
The materials are available for purchase at the corresponding addresses
noted below, and all are available for inspection at the National
Archives and Records Administration (NARA), at the Air and Radiation
Docket and Information Center, U.S. EPA, 401 M St., SW., Washington, DC,
and at the EPA Library (MD-35), U.S. EPA, Research Triangle Park, North
Carolina. For information on the availability of this material at NARA,
call 202-741-6030, or go to: http://www.archives.gov/federal--register/
code--of--federal--regulations/ibr--locations.html.
(b) The following materials are available for purchase from at least
one of the following addresses: American Society for Testing and
Materials (ASTM), 100 Barr Harbor Drive, Post Office Box C700, West
Conshohocken, PA 19428-2959; or ProQuest, 300 North Zeeb Road, Ann
Arbor, MI 48106.
(1) ASTM D523-89, Standard Test Method for Specular Gloss, IBR
approved for Sec. 63.782.
(2) ASTM D1193-77, 91, Standard Specification for Reagent Water, IBR
approved for Appendix A: Method 306, Sections 7.1.1 and 7.4.2.
(3) ASTM D1331-89, Standard Test Methods for Surface and Interfacial
Tension of Solutions of Surface Active Agents, IBR approved for Appendix
A: Method 306B, Sections 6.2, 11.1, and 12.2.2.
(4) ASTM D1475-90, Standard Test Method for Density of Paint,
Varnish Lacquer, and Related Products, IBR approved for Sec. 63.788,
Appendix A.
(5) ASTM D1946-77, 90, 94, Standard Method for Analysis of Reformed
Gas by Gas Chromatography, IBR approved for Sec. 63.11(b)(6).
(6) ASTM D2369-93, 95, Standard Test Method for Volatile Content of
Coatings, IBR approved for Sec. 63.788, Appendix A.
(7) ASTM D2382-76, 88, Heat of Combustion of Hydrocarbon Fuels by
Bomb Calorimeter (High-Precision Method), IBR approved for Sec.
63.11(b)(6).
(8) ASTM D2879-83, 96, Test Method for Vapor Pressure-Temperature
Relationship and Initial Decomposition Temperature of Liquids by
[[Page 64]]
Isoteniscope, IBR approved for Sec. 63.111 and Sec. 63.2406.
(9) ASTM D3257-93, Standard Test Methods for Aromatics in Mineral
Spirits by Gas Chromatography, IBR approved for Sec. 63.786(b).
(10) ASTM 3695-88, Standard Test Method for Volatile Alcohols in
Water by Direct Aqueous-Injection Gas Chromatography, IBR approved for
Sec. 63.365(e)(1) of Subpart O.
(11) ASTM D3792-91, Standard Method for Water Content of Water-
Reducible Paints by Direct Injection into a Gas Chromatograph, IBR
approved for Sec. 63.788, Appendix A.
(12) ASTM D3912-80, Standard Test Method for Chemical Resistance of
Coatings Used in Light-Water Nuclear Power Plants, IBR approved for
Sec. 63.782.
(13) ASTM D4017-90, 96a, Standard Test Method for Water in Paints
and Paint Materials by the Karl Fischer Titration Method, IBR approved
for Sec. 63.788, Appendix A.
(14) ASTM D4082-89, Standard Test Method for Effects of Gamma
Radiation on Coatings for Use in Light-Water Nuclear Power Plants, IBR
approved for Sec. 63.782.
(15) ASTM D4256-89, 94, Standard Test Method for Determination of
the Decontaminability of Coatings Used in Light-Water Nuclear Power
Plants, IBR approved for Sec. 63.782.
(16) ASTM D4809-95, Standard Test Method for Heat of Combustion of
Liquid Hydrocarbon Fuels by Bomb Calorimeter (Precision Method), IBR
approved for Sec. 63.11(b)(6).
(17) ASTM E180-93, Standard Practice for Determining the Precision
of ASTM Methods for Analysis and Testing of Industrial Chemicals, IBR
approved for Sec. 63.786(b).
(18) ASTM E260-91, 96, General Practice for Packed Column Gas
Chromatography, IBR approved for Sec. Sec. 63.750(b)(2) and
63.786(b)(5).
(19)-(20) [Reserved]
(21) ASTM D2099-00, Standard Test Method for Dynamic Water
Resistance of Shoe Upper Leather by the Maeser Water Penetration Tester,
IBR approved for Sec. 63.5350.
(22)-(23) [Reserved]
(24) ASTM D2697-86 (Reapproved 1998), ``Standard Test Method for
Volume Nonvolatile Matter in Clear or Pigmented Coatings,'' IBR approved
for Sec. Sec. 63.3161(f)(1), 63.3521(b)(1), 63.3941(b)(1),
63.4141(b)(1), 63.4741(b)(1), 63.4941(b)(1), and 63.5160(c).
(25) ASTM D6093-97 (Reapproved 2003), ``Standard Test Method for
Percent Volume Nonvolatile Matter in Clear or Pigmented Coatings Using a
Helium Gas Pycnometer,'' IBR approved for Sec. Sec. 63.3161(f)(1),
63.3521(b)(1), 63.3941(b)(1), 63.4141(b)(1), 63.4741(b)(1),
63.4941(b)(1), and 63.5160(c).
(26) ASTM D1475-98 (Reapproved 2003), ``Standard Test Method for
Density of Liquid Coatings, Inks, and Related Products,'' IBR approved
for Sec. Sec. 63.3151(b), 63.3941(b)(4), 63.3941(c), 63.3951(c),
63.4141(b)(3), 63.4141(c), and 63.4551(c).
(27) ASTM D6522-00, Standard Test Method for Determination of
Nitrogen Oxides, Carbon Monoxide, and Oxygen Concentrations in Emissions
from Natural Gas Fired Reciprocating Engines, Combustion Turbines,
Boilers, and Process Heaters Using Portable Analyzers,\1\ IBR approved
for Sec. 63.9307(c)(2), Table 4 of Subpart ZZZZ, and Table 5 to Subpart
DDDDD of this part.
(28) [Reserved]
(29) ASTM D6420-99, Standard Test Method for Determination of
Gaseous Organic Compounds by Direct Interface Gas Chromatography-Mass
Spectrometry, IBR approved for Sec. Sec. 63.5799 and 63.5850.
(30) ASTM E 515-95 (Reapproved 2000), Standard Test Method for Leaks
Using Bubble Emission Techniques, IBR approved for Sec. 63.425(i)(2).
(31) ASTM D5291-02, Standard Test Methods for Instrumental
Determination of Carbon, Hydrogen, and Nitrogen in Petroleum Products
and Lubricants, IBR approved for Sec. 63.3981, appendix A.
(32) ASTM D5965-02, ``Standard Test Methods for Specific Gravity of
Coating Powders,'' IBR approved for Sec. Sec. 63.3151(b) and
63.3951(c).
(33) ASTM D6053-00, Standard Test Method for Determination of
Volatile Organic Compound (VOC) Content of Electrical Insulating
Varnishes, IBR approved for Sec. 63.3981, appendix A.
(34) E145-94 (Reapproved 2001), Standard Specification for Gravity-
Convection and Forced-Ventilation Ovens, IBR approved for Sec. 63.4581,
Appendix A.
[[Page 65]]
(35) ASTM D6784-02, Standard Test Method for Elemental, Oxidized,
Particle-Bound and Total Mercury in Flue Gas Generated from Coal-Fired
Stationary Sources (Ontario Hydro Method),\1\ IBR approved for Table 5
to Subpart DDDDD of this part.
(36) ASTM D5066-91 (Reapproved 2001), ``Standard Test Method for
Determination of the Transfer Efficiency Under Production Conditions for
Spray Application of Automotive Paints-Weight Basis,'' IBR approved for
Sec. 63.3161(g).
(37) ASTM D5087-02, ``Standard Test Method for Determining Amount of
Volatile Organic Compound (VOC) Released from Solventborne Automotive
Coatings and Available for Removal in a VOC Control Device
(Abatement),'' IBR approved for Sec. Sec. 63.3165(e) and 63.3176,
appendix A.
(38) ASTM D6266-00a, ``Test Method for Determining the Amount of
Volatile Organic Compound (VOC) Released from Waterborne Automotive
Coatings and Available for Removal in a VOC Control Device
(Abatement),'' IBR approved for Sec. 63.3165(e).
(39) ASTM Method D388-99,.\1\ Standard Classification of Coals by
Rank,\1\ IBR approved for Sec. 63.7575.
(40) ASTM D396-02a, Standard Specification for Fuel Oils,\1\ IBR
approved for Sec. 63.7575.
(41) ASTM D1835-03a, Standard Specification for Liquified Petroleum
(LP) Gases,\1\ IBR approved for Sec. 63.7575.
(42) ASTM D2013-01, Standard Practice for Preparing Coal Samples for
Analysis,\1\ IBR approved for Table 6 to Subpart DDDDD of this part.
(43) ASTM D2234-00, .\1\ Standard Practice for Collection of a Gross
Sample of Coal,\1\ IBR approved for Table 6 to Subpart DDDDD of this
part.
(44) ASTM D3173-02, Standard Test Method for Moisture in the
Analysis Sample of Coal and Coke,\1\ IBR approved for Table 6 to Subpart
DDDDD of this part.
(45) ASTM D3683-94 (Reapproved 2000), Standard Test Method for Trace
Elements in Coal and Coke Ash Absorption,\1\ IBR approved for Table 6 to
Subpart DDDDD of this part.
(46) ASTM D3684-01, Standard Test Method for Total Mercury in Coal
by the Oxygen Bomb Combustion/Atomic Absorption Method,\1\ IBR approved
for Table 6 to Subpart DDDDD of this part.
(47) ASTM D5198-92 (Reapproved 2003), Standard Practice for Nitric
Acid Digestion of Solid Waste,\1\ IBR approved for Table 6 to Subpart
DDDDD of this part.
(48) ASTM D5865-03a, Standard Test Method for Gross Calorific Value
of Coal and Coke,\1\ IBR approved for Table 6 to Subpart DDDDD of this
part.
(49) ASTM D6323-98 (Reapproved 2003), Standard Guide for Laboratory
Subsampling of Media Related to Waste Management Activities,\1\ IBR
approved for Table 6 to Subpart DDDDD of this part.
(50) ASTM E711-87 (Reapproved 1996), Standard Test Method for Gross
Calorific Value of Refuse-Derived Fuel by the Bomb Calorimeter,\1\ IBR
approved for Table 6 to Subpart DDDDD of this part.
(51) ASTM E776-87 (Reapproved 1996), Standard Test Method for Forms
of Chlorine in Refuse-Derived Fuel,\1\ IBR approved for Table 6 to
Subpart DDDDD of this part.
(52) ASTM E871-82 (Reapproved 1998), Standard Method of Moisture
Analysis of Particulate Wood Fuels,\1\ IBR approved for Table 6 to
Subpart DDDDD of this part.
(53) ASTM E885-88 (Reapproved 1996), Standard Test Methods for
Analyses of Metals in Refuse-Derived Fuel by Atomic Absorption
Spectroscopy,\1\ IBR approved for Table 6 to Subpart DDDDD of this part
63.
(54) ASTM D6348-03, Standard Test Method for Determination of
Gaseous Compounds by Extractive Direct Interface Fourier Transform
Infrared (FTIR) Spectroscopy, incorporation by reference (IBR) approved
for Table 4 to Subpart DDDD of this part and Appendix B to subpart DDDD
of this part as specified in the subpart.
(c) The materials listed below are available for purchase from the
American Petroleum Institute (API), 1220 L Street, NW., Washington, DC
20005.
(1) API Publication 2517, Evaporative Loss from External Floating-
Roof Tanks, Third Edition, February 1989, IBR approved for Sec. 63.111
and Sec. 63.2406.
(2) API Publication 2518, Evaporative Loss from Fixed-roof Tanks,
Second Edition, October 1991, IBR approved for
[[Page 66]]
Sec. 63.150(g)(3)(i)(C) of subpart G of this part.
(3) API Manual of Petroleum Measurement Specifications (MPMS)
Chapter 19.2, Evaporative Loss From Floating-Roof Tanks (formerly API
Publications 2517 and 2519), First Edition, April 1997, IBR approved for
Sec. 63.1251 of subpart GGG of this part.
(d) State and Local Requirements. The materials listed below are
available at the Air and Radiation Docket and Information Center, U.S.
EPA, 401 M St., SW., Washington, DC.
(1) California Regulatory Requirements Applicable to the Air Toxics
Program, January 5, 1999, IBR approved for Sec. 63.99(a)(5)(ii) of
subpart E of this part.
(2) New Jersey's Toxic Catastrophe Prevention Act Program, (July 20,
1998), Incorporation By Reference approved for Sec. 63.99 (a)(30)(i) of
subpart E of this part.
(3)(i) Letter of June 7, 1999 to the U.S. Environmental Protection
Agency Region 3 from the Delaware Department of Natural Resources and
Environmental Control requesting formal full delegation to take over
primary responsibility for implementation and enforcement of the
Chemical Accident Prevention Program under Section 112(r) of the Clean
Air Act Amendments of 1990.
(ii) Delaware Department of Natural Resources and Environmental
Control, Division of Air and Waste Management, Accidental Release
Prevention Regulation, sections 1 through 5 and sections 7 through 14,
effective January 11, 1999, IBR approved for Sec. 63.99(a)(8)(i) of
subpart E of this part.
(iii) State of Delaware Regulations Governing the Control of Air
Pollution (October 2000), IBR approved for Sec. 63.99(a)(8)(ii)-(v) of
subpart E of this part.
(4) Massachusetts Regulations Applicable to Hazardous Air Pollutants
(July 2002). Incorporation By Reference approved for Sec.
63.99(a)(21)(ii) of subpart E of this part.
(5) New Hampshire Regulations Applicable to Hazardous Air
Pollutants, March, 2003. Incorporation by Reference approved for Sec.
63.99(a)(29)(iii) of subpart E of this part.
(6) Maine Regulations Applicable to Hazardous Air Pollutants (March
2006). Incorporation By Reference approved for Sec. 63.99(a)(19)(iii)
of subpart E of this part.
(e) The materials listed below are available for purchase from the
National Institute of Standards and Technology, Springfield, VA 22161,
(800) 553-6847.
(1) Handbook 44, Specificiations, Tolerances, and Other Technical
Requirements for Weighing and Measuring Devices 1998, IBR approved for
Sec. 63.1303(e)(3).
(2) [Reserved]
(f) The following material is available from the National Council of
the Paper Industry for Air and Stream Improvement, Inc. (NCASI), P.O.
Box 133318, Research Triangle Park, NC 27709-3318 or at http://
www.ncasi.org.
(1) NCASI Method DI/MEOH-94.02, Methanol in Process Liquids GC/FID
(Gas Chromatography/Flame Ionization Detection), August 1998, Methods
Manual, NCASI, Research Triangle Park, NC, IBR approved for Sec.
63.457(c)(3)(ii) of subpart S of this part.
(2) NCASI Method CI/WP-98.01, Chilled Impinger Method For Use At
Wood Products Mills to Measure Formaldehyde, Methanol, and Phenol, 1998,
Methods Manual, NCASI, Research Triangle Park, NC, IBR approved for
Table 4 to Subpart DDDD of this part.
(3) NCASI Method IM/CAN/WP-99.02, Impinger/Canister Source Sampling
Method For Selected HAPs and Other Compounds at Wood Products
Facilities, January 2004, Methods Manual, NCASI, Research Triangle Park,
NC, IBR approved for Table 4 to Subpart DDDD of this part and Appendix B
to subpart DDDD of this part.
(4) NCASI Method ISS/FP-A105.01, Impinger Source Sampling Method for
Selected Aldehydes, Ketones, and Polar Compounds, December 2005, Methods
Manual, NCASI, Research Triangle Park, NC, IBR approved for table 4 to
subpart DDDD of this part and appendix B to subpart DDDD of this part.
(g) The materials listed below are available for purchase from AOAC
International, Customer Services, Suite 400, 2200 Wilson Boulevard,
Arlington, Virginia, 22201-3301, Telephone (703) 522-3032, Fax (703)
522-5468.
[[Page 67]]
(1) AOAC Official Method 978.01 Phosphorus (Total) in Fertilizers,
Automated Method, Sixteenth edition, 1995, IBR approved for Sec.
63.626(d)(3)(vi).
(2) AOAC Official Method 969.02 Phosphorus (Total) in Fertilizers,
Alkalimetric Quinolinium Molybdophosphate Method, Sixteenth edition,
1995, IBR approved for Sec. 63.626(d)(3)(vi).
(3) AOAC Official Method 962.02 Phosphorus (Total) in Fertilizers,
Gravimetric Quinolinium Molybdophosphate Method, Sixteenth edition,
1995, IBR approved for Sec. 63.626(d)(3)(vi).
(4) AOAC Official Method 957.02 Phosphorus (Total) in Fertilizers,
Preparation of Sample Solution, Sixteenth edition, 1995, IBR approved
for Sec. 63.626(d)(3)(vi).
(5) AOAC Official Method 929.01 Sampling of Solid Fertilizers,
Sixteenth edition, 1995, IBR approved for Sec. 63.626(d)(3)(vi).
(6) AOAC Official Method 929.02 Preparation of Fertilizer Sample,
Sixteenth edition, 1995, IBR approved for Sec. 63.626(d)(3)(vi).
(7) AOAC Official Method 958.01 Phosphorus (Total) in Fertilizers,
Spectrophotometric Molybdovanadophosphate Method, Sixteenth edition,
1995, IBR approved for Sec. 63.626(d)(3)(vi).
(h) The materials listed below are available for purchase from The
Association of Florida Phosphate Chemists, P.O. Box 1645, Bartow,
Florida, 33830, Book of Methods Used and Adopted By The Association of
Florida Phosphate Chemists, Seventh Edition 1991, IBR.
(1) Section IX, Methods of Analysis for Phosphate Rock, No. 1
Preparation of Sample, IBR approved for Sec. 63.606(c)(3)(ii) and Sec.
63.626(c)(3)(ii).
(2) Section IX, Methods of Analysis for Phosphate Rock, No. 3
Phosphorus--P2O5 or
Ca3(PO4)2, Method A-Volumetric Method,
IBR approved for Sec. 63.606(c)(3)(ii) and Sec. 63.626(c)(3)(ii).
(3) Section IX, Methods of Analysis for Phosphate Rock, No. 3
Phosphorus-P2O5 or
Ca3(PO4)2, Method B--Gravimetric
Quimociac Method, IBR approved for Sec. 63.606(c)(3)(ii) and Sec.
63.626(c)(3)(ii).
(4) Section IX, Methods of Analysis For Phosphate Rock, No. 3
Phosphorus-P2O5 or
Ca3(PO4)2, Method C--Spectrophotometric
Method, IBR approved for Sec. 63.606(c)(3)(ii) and Sec.
63.626(c)(3)(ii).
(5) Section XI, Methods of Analysis for Phosphoric Acid,
Superphosphate, Triple Superphosphate, and Ammonium Phosphates, No. 3
Total Phosphorus-P2O5, Method A--Volumetric
Method, IBR approved for Sec. 63.606(c)(3)(ii), Sec. 63.626(c)(3)(ii),
and Sec. 63.626(d)(3)(v).
(6) Section XI, Methods of Analysis for Phosphoric Acid,
Superphosphate, Triple Superphosphate, and Ammonium Phosphates, No. 3
Total Phosphorus-P2O5, Method B--Gravimetric
Quimociac Method, IBR approved for Sec. 63.606(c)(3)(ii), Sec.
63.626(c)(3)(ii), and Sec. 63.626(d)(3)(v).
(7) Section XI, Methods of Analysis for Phosphoric Acid,
Superphosphate, Triple Superphosphate, and Ammonium Phosphates, No. 3
Total Phosphorus-P2O5, Method C--
Spectrophotometric Method, IBR approved for Sec. 63.606(c)(3)(ii),
Sec. 63.626(c)(3)(ii), and Sec. 63.626(d)(3)(v).
(i) The following materials are available for purchase from at least
one of the following addresses: ASME International, Orders/Inquiries,
P.O. Box 2900, Fairfield, NJ 07007-2900; or Global Engineering
Documents, Sales Department, 15 Inverness Way East, Englewood, CO 80112.
(1) ANSI/ASME PTC 19.10-1981, ``Flue and Exhaust Gas Analyses [Part
10, Instruments and Apparatus],'' IBR approved for Sec. Sec.
63.309(k)(1)(iii), 63.865(b), 63.3166(a)(3), 63.3360(e)(1)(iii),
63.3545(a)(3), 63.3555(a)(3), 63.4166(a)(3), 63.4362(a)(3),
63.4766(a)(3), 63.4965(a)(3), 63.5160(d)(1)(iii), 63.9307(c)(2), and
63.9323(a)(3) and Table 5 to Subpart DDDDD of this part.
(2) [Reserved]
(j) The following material is available for purchase from: British
Standards Institute, 389 Chiswick High Road, London W4 4AL, United
Kingdom.
(1) BS EN 1593:1999, Non-destructive Testing: Leak Testing--Bubble
Emission Techniques, IBR approved for Sec. 63.425(i)(2).
(2) [Reserved]
(k) The following materials are available for purchase from the
National Technical Information Service (NTIS),
[[Page 68]]
5285 Port Royal Road, Springfield, VA 22161, (703) 605-6000 or (800)
553-6847; or for purchase from the Superintendent of Documents, U.S.
Government Printing Office, Washington, DC 20402, (202) 512-1800:
(1) The following methods as published in the test methods
compendium known as ``Test Methods for Evaluating Solid Waste, Physical/
Chemical Methods,'' EPA Publication SW-846, Third Edition. A suffix of
``A'' in the method number indicates revision one (the method has been
revised once). A suffix of ``B'' in the method number indicates revision
two (the method has been revised twice).
(i) Method 0023A, ``Sampling Method for Polychlorinated Dibenzo-p-
Dioxins and Polychlorinated Dibenzofuran Emissions from Stationary
Sources,'' dated December 1996 and in Update III, IBR approved for Sec.
63.1208(b)(1) of Subpart EEE of this part.
(ii) Method 9071B, ``n-Hexane Extractable Material (HEM) for Sludge,
Sediment, and Solid Samples,'' dated April 1998 and in Update IIIA, IBR
approved for Sec. 63.7824(e) of Subpart FFFFF of this part.
(iii) Method 9095A, ``Paint Filter Liquids Test,'' dated December
1996 and in Update III, IBR approved for Sec. Sec. 63.7700(b) and
63.7765 of Subpart EEEEE of this part.
(2) [Reserved]
[59 FR 12430, Mar. 16, 1994]
Editorial Note: For Federal Register citations affecting Sec.
63.14, see the List of CFR Sections Affected, which appears in the
Finding Aids section of the printed volume and on GPO Access.