[Code of Federal Regulations] [Title 40, Volume 25] [Revised as of July 1, 2007] From the U.S. Government Printing Office via GPO Access [CITE: 40CFR261.41] [Page 107-204] TITLE 40--PROTECTION OF ENVIRONMENT CHAPTER I--ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) PART 261_IDENTIFICATION AND LISTING OF HAZARDOUS WASTE--Table of Contents Subpart E_Exclusions/Exemptions Sec. 261.41 Notification and Recordkeeping for Used, Intact Cathode Ray Tubes (CRTs) Exported for Reuse. (a) Persons who export used, intact CRTs for reuse must send a one- time notification to the Regional Administrator. The notification must include a statement that the notifier plans to export used, intact CRTs for reuse, the notifier's name, address, and EPA ID number (if applicable) and the name and phone number of a contact person. (b) Persons who export used, intact CRTs for reuse must keep copies of normal business records, such as contracts, demonstrating that each shipment of exported CRTs will be reused. This documentation must be retained for a period of at least three years from the date the CRTs were exported. [[Page 108]] Appendix I to Part 261--Representative Sampling Methods The methods and equipment used for sampling waste materials will vary with the form and consistency of the waste materials to be sampled. Samples collected using the sampling protocols listed below, for sampling waste with properties similar to the indicated materials, will be considered by the Agency to be representative of the waste. Extremely viscous liquid--ASTM Standard D140-70 Crushed or powdered material--ASTM Standard D346-75 Soil or rock-like material--ASTM Standard D420-69 Soil-like material--ASTM Standard D1452-65 Fly Ash-like material--ASTM Standard D2234-76 [ASTM Standards are available from ASTM, 1916 Race St., Philadelphia, PA 19103] Containerized liquid waste--``COLIWASA.'' Liquid waste in pits, ponds, lagoons, and similar reservoirs--``Pond Sampler.'' This manual also contains additional information on application of these protocols. [45 FR 33119, May 19, 1980, as amended at 70 FR 34562, June 14, 2005] Appendix II to Part 261 [Reserved] Appendix III to Part 261 [Reserved] Appendix IV to Part 261 [Reserved for Radioactive Waste Test Methods] Appendix V to Part 261 [Reserved for Infectious Waste Treatment Specifications] Appendix VI to Part 261 [Reserved for Etiologic Agents] Appendix VII to Part 261--Basis for Listing Hazardous Waste ------------------------------------------------------------------------ Hazardous constituents for which EPA hazardous waste No. listed ------------------------------------------------------------------------ F001............................ Tetrachloroethylene, methylene chloride trichloroethylene, 1,1,1- trichloroethane, carbon tetrachloride, chlorinated fluorocarbons. F002............................ Tetrachloroethylene, methylene chloride, trichloroethylene, 1,1,1- trichloroethane, 1,1,2- trichloroethane, chlorobenzene, 1,1,2- trichloro-1,2,2-trifluoroethane, ortho-dichlorobenzene, trichlorofluoromethane. F003............................ N.A. F004............................ Cresols and cresylic acid, nitrobenzene. F005............................ Toluene, methyl ethyl ketone, carbon disulfide, isobutanol, pyridine, 2- ethoxyethanol, benzene, 2- nitropropane. F006............................ Cadmium, hexavalent chromium, nickel, cyanide (complexed). F007............................ Cyanide (salts). F008............................ Cyanide (salts). F009............................ Cyanide (salts). F010............................ Cyanide (salts). F011............................ Cyanide (salts). F012............................ Cyanide (complexed). F019............................ Hexavalent chromium, cyanide (complexed). F020............................ Tetra- and pentachlorodibenzo-p- dioxins; tetra and pentachlorodi- benzofurans; tri- and tetrachlorophenols and their chlorophenoxy derivative acids, esters, ethers, amine and other salts. F021............................ Penta- and hexachlorodibenzo-p- dioxins; penta- and hexachlorodibenzofurans; pentachlorophenol and its derivatives. F022............................ Tetra-, penta-, and hexachlorodibenzo- p-dioxins; tetra-, penta-, and hexachlorodibenzofurans. F023............................ Tetra-, and pentachlorodibenzo-p- dioxins; tetra- and pentachlorodibenzofurans; tri- and tetra chlorophenols and their chlorophenoxy derivative acids, esters, ethers, amine and other salts. F024............................ Chloromethane, dichloromethane, trichloromethane, carbon tetrachloride, chloroethylene, 1,1- dichloroethane, 1,2-dichloroethane, trans-1-2-dichloroethylene, 1,1- dichloroethylene, 1,1,1- trichloroethane, 1,1,2- trichloroethane, trichloroethylene, 1,1,1,2-tetra-chloroethane, 1,1,2,2- tetrachloroethane, tetrachloroethylene, pentachloroethane, hexachloroethane, allyl chloride (3-chloropropene), dichloropropane, dichloropropene, 2- chloro-1,3-butadiene, hexachloro-1,3- butadiene, hexachlorocyclopentadiene, hexachlorocyclohexane, benzene, chlorbenzene, dichlorobenzenes, 1,2,4- trichlorobenzene, tetrachlorobenzene, pentachlorobenzene, hexachlorobenzene, toluene, naphthalene. F025............................ Chloromethane; Dichloromethane; Trichloromethane; Carbon tetrachloride; Chloroethylene; 1,1- Dichloroethane; 1,2-Dichloroethane; trans-1,2-Dichloroethylene; 1,1- Dichloroethylene; 1,1,1- Trichloroethane; 1,1,2- Trichloroethane; Trichloroethylene; 1,1,1,2-Tetrachloroethane; 1,1,2,2- Tetrachloroethane; Tetrachloroethylene; Pentachloroethane; Hexachloroethane; Allyl chloride (3-Chloropropene); Dichloropropane; Dichloropropene; 2- Chloro-1,3-butadiene; Hexachloro-1,3- butadiene; Hexachlorocyclopentadiene; Benzene; Chlorobenzene; Dichlorobenzene; 1,2,4-Tri chlorobenzene; Tetrachlorobenzene; Pentachlorobenzene; Hexachlorobenzene; Toluene; Naphthalene. F026............................ Tetra-, penta-, and hexachlorodibenzo- p-dioxins; tetra-, penta-, and hexachlorodibenzofurans. F027............................ Tetra-, penta-, and hexachlorodibenzo- p- dioxins; tetra-, penta-, and hexachlorodibenzofurans; tri-, tetra- , and pentachlorophenols and their chlorophenoxy derivative acids, esters, ethers, amine and other salts. F028............................ Tetra-, penta-, and hexachlorodibenzo- p- dioxins; tetra-, penta-, and hexachlorodibenzofurans; tri-, tetra- , and pentachlorophenols and their chlorophenoxy derivative acids, esters, ethers, amine and other salts. F032............................ Benz(a)anthracene, benzo(a)pyrene, dibenz(a,h)-anthracene, indeno(1,2,3- cd)pyrene, pentachlorophenol, arsenic, chromium, tetra-, penta-, hexa-, heptachlorodibenzo-p-dioxins, tetra-, penta-, hexa-, heptachlorodibenzofurans. [[Page 109]] F034............................ Benz(a)anthracene, benzo(k)fluoranthene, benzo(a)pyrene, dibenz(a,h)anthracene, indeno(1,2,3- cd)pyrene, naphthalene, arsenic, chromium. F035............................ Arsenic, chromium, lead. F037............................ Benzene, benzo(a)pyrene, chrysene, lead, chromium. F038............................ Benzene, benzo(a)pyrene, chrysene, lead, chromium. F039............................ All constituents for which treatment standards are specified for multi- source leachate (wastewaters and nonwastewaters) under 40 CFR 268.43, Table CCW. K001............................ Pentachlorophenol, phenol, 2- chlorophenol, p-chloro-m-cresol, 2,4- dimethylphenyl, 2,4-dinitrophenol, trichlorophenols, tetrachlorophenols, 2,4-dinitrophenol, creosote, chrysene, naphthalene, fluoranthene, benzo(b)fluoranthene, benzo(a)pyrene, indeno(1,2,3-cd)pyrene, benz(a)anthracene, dibenz(a)anthracene, acenaphthalene. K002............................ Hexavalent chromium, lead K003............................ Hexavalent chromium, lead. K004............................ Hexavalent chromium. K005............................ Hexavalent chromium, lead. K006............................ Hexavalent chromium. K007............................ Cyanide (complexed), hexavalent chromium. K008............................ Hexavalent chromium. K009............................ Chloroform, formaldehyde, methylene chloride, methyl chloride, paraldehyde, formic acid. K010............................ Chloroform, formaldehyde, methylene chloride, methyl chloride, paraldehyde, formic acid, chloroacetaldehyde. K011............................ Acrylonitrile, acetonitrile, hydrocyanic acid. K013............................ Hydrocyanic acid, acrylonitrile, acetonitrile. K014............................ Acetonitrile, acrylamide. K015............................ Benzyl chloride, chlorobenzene, toluene, benzotrichloride. K016............................ Hexachlorobenzene, hexachlorobutadiene, carbon tetrachloride, hexachloroethane, perchloroethylene. K017............................ Epichlorohydrin, chloroethers [bis(chloromethyl) ether and bis (2- chloroethyl) ethers], trichloropropane, dichloropropanols. K018............................ 1,2-dichloroethane, trichloroethylene, hexachlorobutadiene, hexachlorobenzene. K019............................ Ethylene dichloride, 1,1,1- trichloroethane, 1,1,2- trichloroethane, tetrachloroethanes (1,1,2,2-tetrachloroethane and 1,1,1,2-tetrachloroethane), trichloroethylene, tetrachloroethylene, carbon tetrachloride, chloroform, vinyl chloride, vinylidene chloride. K020............................ Ethylene dichloride, 1,1,1- trichloroethane, 1,1,2- trichloroethane, tetrachloroethanes (1,1,2,2-tetrachloroethane and 1,1,1,2-tetrachloroethane), trichloroethylene, tetrachloroethylene, carbon tetrachloride, chloroform, vinyl chloride, vinylidene chloride. K021............................ Antimony, carbon tetrachloride, chloroform. K022............................ Phenol, tars (polycyclic aromatic hydrocarbons). K023............................ Phthalic anhydride, maleic anhydride. K024............................ Phthalic anhydride, 1,4- naphthoquinone. K025............................ Meta-dinitrobenzene, 2,4- dinitrotoluene. K026............................ Paraldehyde, pyridines, 2-picoline. K027............................ Toluene diisocyanate, toluene-2, 4- diamine. K028............................ 1,1,1-trichloroethane, vinyl chloride. K029............................ 1,2-dichloroethane, 1,1,1- trichloroethane, vinyl chloride, vinylidene chloride, chloroform. K030............................ Hexachlorobenzene, hexachlorobutadiene, hexachloroethane, 1,1,1,2- tetrachloroethane, 1,1,2,2- tetrachloroethane, ethylene dichloride. K031............................ Arsenic. K032............................ Hexachlorocyclopentadiene. K033............................ Hexachlorocyclopentadiene. K034............................ Hexachlorocyclopentadiene. K035............................ Creosote, chrysene, naphthalene, fluoranthene benzo(b) fluoranthene, benzo(a)pyrene, indeno(1,2,3-cd) pyrene, benzo(a)anthracene, dibenzo(a)anthracene, acenaphthalene. K036............................ Toluene, phosphorodithioic and phosphorothioic acid esters. K037............................ Toluene, phosphorodithioic and phosphorothioic acid esters. K038............................ Phorate, formaldehyde, phosphorodithioic and phosphorothioic acid esters. K039............................ Phosphorodithioic and phosphorothioic acid esters. K040............................ Phorate, formaldehyde, phosphorodithioic and phosphorothioic acid esters. K041............................ Toxaphene. K042............................ Hexachlorobenzene, ortho- dichlorobenzene. K043............................ 2,4-dichlorophenol, 2,6- dichlorophenol, 2,4,6- trichlorophenol. K044............................ N.A. K045............................ N.A. K046............................ Lead. K047............................ N.A. K048............................ Hexavalent chromium, lead. K049............................ Hexavalent chromium, lead. K050............................ Hexavalent chromium. K051............................ Hexavalent chromium, lead. K052............................ Lead. K060............................ Cyanide, napthalene, phenolic compounds, arsenic. K061............................ Hexavalent chromium, lead, cadmium. K062............................ Hexavalent chromium, lead. K064............................ Lead, cadmium. K065............................ Do. K066............................ Do. K069............................ Hexavalent chromium, lead, cadmium. K071............................ Mercury. K073............................ Chloroform, carbon tetrachloride, hexachloroethane, trichloroethane, tetrachloroethylene, dichloroethylene, 1,1,2,2- tetrachloroethane. K083............................ Aniline, diphenylamine, nitrobenzene, phenylenediamine. K084............................ Arsenic. K085............................ Benzene, dichlorobenzenes, trichlorobenzenes, tetrachlorobenzenes, pentachlorobenzene, hexachlorobenzene, benzyl chloride. K086............................ Lead, hexavalent chromium. K087............................ Phenol, naphthalene. K088............................ Cyanide (complexes). K090............................ Chromium. K091............................ Do. K093............................ Phthalic anhydride, maleic anhydride. K094............................ Phthalic anhydride. K095............................ 1,1,2-trichloroethane, 1,1,1,2- tetrachloroethane, 1,1,2,2- tetrachloroethane. K096............................ 1,2-dichloroethane, 1,1,1- trichloroethane, 1,1,2- trichloroethane. K097............................ Chlordane, heptachlor. K098............................ Toxaphene. K099............................ 2,4-dichlorophenol, 2,4,6- trichlorophenol. K100............................ Hexavalent chromium, lead, cadmium. K101............................ Arsenic. K102............................ Arsenic. K103............................ Aniline, nitrobenzene, phenylenediamine. K104............................ Aniline, benzene, diphenylamine, nitrobenzene, phenylenediamine. K105............................ Benzene, monochlorobenzene, dichlorobenzenes, 2,4,6- trichlorophenol. [[Page 110]] K106............................ Mercury. K107............................ 1,1-Dimethylhydrazine (UDMH). K108............................ 1,1-Dimethylhydrazine (UDMH). K109............................ 1,1-Dimethylhydrazine (UDMH). K110............................ 1,1-Dimethylhydrazine (UDMH). K111............................ 2,4-Dinitrotoluene. K112............................ 2,4-Toluenediamine, o-toluidine, p- toluidine, aniline. K113............................ 2,4-Toluenediamine, o-toluidine, p- toluidine, aniline. K114............................ 2,4-Toluenediamine, o-toluidine, p- toluidine. K115............................ 2,4-Toluenediamine. K116............................ Carbon tetrachloride, tetrachloroethylene, chloroform, phosgene. K117............................ Ethylene dibromide. K118............................ Ethylene dibromide. K123............................ Ethylene thiourea. K124............................ Ethylene thiourea. K125............................ Ethylene thiourea. K126............................ Ethylene thiourea. K131............................ Dimethyl sulfate, methyl bromide. K132............................ Methyl bromide. K136............................ Ethylene dibromide. K141............................ Benzene, benz(a)anthracene, benzo(a)pyrene, benzo(b)fluoranthene, benzo(k)fluoranthene, dibenz(a,h)anthracene, indeno(1,2,3- cd)pyrene. K142............................ Benzene, benz(a)anthracene, benzo(a)pyrene, benzo(b)fluoranthene, benzo(k)fluoranthene, dibenz(a,h)anthracene, indeno(1,2,3- cd)pyrene. K143............................ Benzene, benz(a)anthracene, benzo(b)fluoranthene, benzo(k)fluoranthene. K144............................ Benzene, benz(a)anthracene, benzo(a)pyrene, benzo(b)fluoranthene, benzo(k)fluoranthene, dibenz(a,h)anthracene. K145............................ Benzene, benz(a)anthracene, benzo(a)pyrene, dibenz(a,h)anthracene, naphthalene. K147............................ Benzene, benz(a)anthracene, benzo(a)pyrene, benzo(b)fluoranthene, benzo(k)fluoranthene, dibenz(a,h)anthracene, indeno(1,2,3- cd)pyrene. K148............................ Benz(a)anthracene, benzo(a)pyrene, benzo(b)fluoranthene, benzo(k)fluoranthene, dibenz(a,h)anthracene, indeno(1,2,3- cd)pyrene. K149............................ Benzotrichloride, benzyl chloride, chloroform, chloromethane, chlorobenzene, 1,4-dichlorobenzene, hexachlorobenzene, pentachlorobenzene, 1,2,4,5- tetrachlorobenzene, toluene. K150............................ Carbon tetrachloride, chloroform, chloromethane, 1,4-dichlorobenzene, hexachlorobenzene, pentachlorobenzene, 1,2,4,5- tetrachlorobenzene, 1,1,2,2- tetrachloroethane, tetrachloroethylene, 1,2,4- trichlorobenzene. K151............................ Benzene, carbon tetrachloride, chloroform, hexachlorobenzene, pentachlorobenzene, toluene, 1,2,4,5- tetrachlorobenzene, tetrachloroethylene. K156............................ Benomyl, carbaryl, carbendazim, carbofuran, carbosulfan, formaldehyde, methylene chloride, triethylamine. K157............................ Carbon tetrachloride, formaldehyde, methyl chloride, methylene chloride, pyridine, triethylamine. K158............................ Benomyl, carbendazim, carbofuran, carbosulfan, chloroform, methylene chloride. K159............................ Benzene, butylate, eptc, molinate, pebulate, vernolate. K161............................ Antimony, arsenic, metam-sodium, ziram. K169............................ Benzene. K170............................ Benzo(a)pyrene, dibenz(a,h)anthracene, benzo (a) anthracene, benzo (b)fluoranthene, benzo(k)fluoranthene, 3- methylcholanthrene, 7, 12- dimethylbenz(a)anthracene. K171............................ Benzene, arsenic. K172............................ Benzene, arsenic. K174............................ 1,2,3,4,6,7,8-Heptachlorodibenzo-p- dioxin (1,2,3,4,6,7,8-HpCDD), 1,2,3,4,6,7,8-Heptachlorodibenzofuran (1,2,3,4,6,7,8-HpCDF), 1,2,3,4,7,8,9- Heptachlorodibenzofuran (1,2,3,6,7,8,9-HpCDF), HxCDDs (All Hexachlorodibenzo-p-dioxins), HxCDFs (All Hexachlorodibenzofurans), PeCDDs (All Pentachlorodibenzo-p-dioxins), OCDD (1,2,3,4,6,7,8,9- Octachlorodibenzo-p-dioxin, OCDF (1,2,3,4,6,7,8,9- Octachlorodibenzofuran), PeCDFs (All Pentachlorodibenzofurans), TCDDs (All tetrachlorodi-benzo-p-dioxins), TCDFs (All tetrachlorodibenzofurans). K175............................ Mercury K176............................ Arsenic, Lead. K177............................ Antimony. K178............................ Thallium. K181............................ Aniline, o-anisidine, 4-chloroaniline, p-cresidine, 2,4-dimethylaniline, 1,2- phenylenediamine, 1,3- phenylenediamine. ------------------------------------------------------------------------ N.A.--Waste is hazardous because it fails the test for the characteristic of ignitability, corrosivity, or reactivity. [46 FR 4619, Jan. 16, 1981] Editorial Note: For Federal Register citations affecting Appendix VII, part 261, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume and on GPO Access. Appendix VIII to Part 261--Hazardous Constituents ---------------------------------------------------------------------------------------------------------------- Chemical Hazardous Common name Chemical abstracts name abstracts No. waste No. ---------------------------------------------------------------------------------------------------------------- A2213...................................... Ethanimidothioic acid, 2- 30558-43-1 U394 (dimethylamino) -N-hydroxy-2-oxo-, methyl ester. Acetonitrile............................... Same............................... 75-05-8 U003 Acetophenone............................... Ethanone, 1-phenyl-................ 98-86-2 U004 2-Acetylaminefluarone...................... Acetamide, N-9H-fluoren-2-yl-...... 53-96-3 U005 Acetyl chloride............................ Same............................... 75-36-5 U006 1-Acetyl-2-thiourea........................ Acetamide, N-(aminothioxomethyl)-.. 591-08-2 P002 Acrolein................................... 2-Propenal......................... 107-02-8 P003 Acrylamide................................. 2-Propenamide...................... 79-06-1 U007 Acrylonitrile.............................. 2-Propenenitrile................... 107-13-1 U009 [[Page 111]] Aflatoxins................................. Same............................... 1402-68-2 ........... Aldicarb................................... Propanal, 2-methyl-2-(methylthio)-, 116-06-3 P070 O-[(methylamino)carbonyl]oxime. Aldicarb sulfone........................... Propanal, 2-methyl-2- 1646-88-4 P203 (methylsulfonyl) -, O- [(methylamino) carbonyl] oxime. Aldrin..................................... 1,4,5,8-Dimethanonaphthalene, 309-00-2 P004 1,2,3,4,10,10-10-hexachloro- 1,4,4a,5,8,8a-hexahydro-, (1alpha,4alpha,4abeta,5alpha,8alph a, 8abeta)-. Allyl alcohol.............................. 2-Propen-1-ol...................... 107-18-6 P005 Allyl chloride............................. 1-Propane, 3-chloro................ 107-05-1 ........... Aluminum phosphide......................... Same............................... 20859-73-8 P006 4-Aminobiphenyl............................ [1,1'-Biphenyl]-4-amine............ 92-67-1 ........... 5-(Aminomethyl)-3-isoxazolol............... 3(2H)-Isoxazolone, 5-(aminomethyl)- 2763-96-4 P007 4-Aminopyridine............................ 4-Pyridinamine..................... 504-24-5 P008 Amitrole................................... 1H-1,2,4-Triazol-3-amine........... 61-82-5 U011 Ammonium vanadate.......................... Vanadic acid, ammonium salt........ 7803-55-6 P119 Aniline.................................... Benzenamine........................ 62-53-3 U012 o-Anisidine (2-methoxyaniline)............. Benzenamine, 2-Methoxy-............ 90-04-0 ........... Antimony................................... Same............................... 7440-36-0 ........... Antimony compounds, N.O.S. \1\............. ................................... ................. ........... Aramite.................................... Sulfurous acid, 2-chloroethyl 2-[4- 140-57-8 ........... (1,1-dimethylethyl)phenoxy]-1- methylethyl ester. Arsenic.................................... Same............................... 7440-38-2 ........... Arsenic compounds, N.O.S. \1\.............. ................................... ................. ........... Arsenic acid............................... Arsenic acid H3 AsO4............... 7778-39-4 P010 Arsenic pentoxide.......................... Arsenic oxide As2 O5............... 1303-28-2 P011 Arsenic trioxide........................... Arsenic oxide As2 O3............... 1327-53-3 P012 Auramine................................... Benzenamine, 4,4'- 492-80-8 U014 carbonimidoylbis[N,N-dimethyl. Azaserine.................................. L-Serine, diazoacetate (ester)..... 115-02-6 U015 Barban..................................... Carbamic acid, (3-chlorophenyl) -, 101-27-9 U280 4-chloro-2-butynyl ester. Barium..................................... Same............................... 7440-39-3 ........... Barium compounds, N.O.S. \1\............... ................................... ................. ........... Barium cyanide............................. Same............................... 542-62-1 P013 Bendiocarb................................. 1,3-Benzodioxol-4-ol, 2,2-dimethyl- 22781-23-3 U278 , methyl carbamate. Bendiocarb phenol.......................... 1,3-Benzodioxol-4-ol, 2,2-dimethyl- 22961-82-6 U364 ,. Benomyl.................................... Carbamic acid, [1- [(butylamino) 17804-35-2 U271 carbonyl]- 1H-benzimidazol-2-yl] - , methyl ester. Benz[c]acridine............................ Same............................... 225-51-4 U016 Benz[a]anthracene.......................... Same............................... 56-55-3 U018 Benzal chloride............................ Benzene, (dichloromethyl)-......... 98-87-3 U017 Benzene.................................... Same............................... 71-43-2 U019 Benzenearsonic acid........................ Arsonic acid, phenyl-.............. 98-05-5 ........... Benzidine.................................. [1,1'-Biphenyl]-4,4 '-diamine...... 92-87-5 U021 Benzo[b]fluoranthene....................... Benz[e]acephenanthrylene........... 205-99-2 ........... Benzo[j]fluoranthene....................... Same............................... 205-82-3 ........... Benzo(k)fluoranthene....................... Same............................... 207-08-9 ........... Benzo[a]pyrene............................. Same............................... 50-32-8 U022 p-Benzoquinone............................. 2,5-Cyclohexadiene-1,4-dione....... 106-51-4 U197 Benzotrichloride........................... Benzene, (trichloromethyl)-........ 98-07-7 U023 Benzyl chloride............................ Benzene, (chloromethyl)-........... 100-44-7 P028 Beryllium powder........................... Same............................... 7440-41-7 P015 Beryllium compounds, N.O.S. \1\............ ................................... ................. ........... Bis(pentamethylene)-thiuram tetrasulfide... Piperidine, 1,1'- 120-54-7 ........... (tetrathiodicarbonothioyl)-bis-. Bromoacetone............................... 2-Propanone, 1-bromo-.............. 598-31-2 P017 Bromoform.................................. Methane, tribromo-................. 75-25-2 U225 4-Bromophenyl phenyl ether................. Benzene, 1-bromo-4-phenoxy-........ 101-55-3 U030 Brucine.................................... Strychnidin-10-one, 2,3-dimethoxy-. 357-57-3 P018 Butyl benzyl phthalate..................... 1,2-Benzenedicarboxylic acid, butyl 85-68-7 ........... phenylmethyl ester. Butylate................................... Carbamothioic acid, bis(2- 2008-41-5 ........... methylpropyl)-, S-ethyl ester. Cacodylic acid............................. Arsinic acid, dimethyl-............ 75-60-5 U136 Cadmium.................................... Same............................... 7440-43-9 ........... Cadmium compounds, N.O.S. \1\.............. ................................... ................. ........... Calcium chromate........................... Chromic acid H2 CrO4, calcium salt. 13765-19-0 U032 Calcium cyanide............................ Calcium cyanide Ca(CN)2............ 592-01-8 P021 Carbaryl................................... 1-Naphthalenol, methylcarbamate.... 63-25-2 U279 Carbendazim................................ Carbamic acid, 1H-benzimidazol-2- 10605-21-7 U372 yl, methyl ester. [[Page 112]] Carbofuran................................. 7-Benzofuranol, 2,3-dihydro-2,2- 1563-66-2 P127 dimethyl-, methylcarbamate. Carbofuran phenol.......................... 7-Benzofuranol, 2,3-dihydro-2,2- 1563-38-8 U367 dimethyl-. Carbon disulfide........................... Same............................... 75-15-0 P022 Carbon oxyfluoride......................... Carbonic difluoride................ 353-50-4 U033 Carbon tetrachloride....................... Methane, tetrachloro-.............. 56-23-5 U211 Carbosulfan................................ Carbamic acid, [(dibutylamino) 55285-14-8 P189 thio] methyl-, 2,3-dihydro-2,2- dimethyl-7-benzofuranyl ester. Chloral.................................... Acetaldehyde, trichloro-........... 75-87-6 U034 Chlorambucil............................... Benzenebutanoic acid, 4-[bis(2- 305-03-3 U035 chloroethyl)amino]-. Chlordane.................................. 4,7-Methano-1H-indene, 57-74-9 U036 1,2,4,5,6,7,8,8-octachloro- 2,3,3a,4,7,7a-hexahydro-. Chlordane (alpha and gamma isomers)........ ................................... ................. U036 Chlorinated benzenes, N.O.S. \1\........... ................................... ................. ........... Chlorinated ethane, N.O.S. \1\............. ................................... ................. ........... Chlorinated fluorocarbons, N.O.S. \1\...... ................................... ................. ........... Chlorinated naphthalene, N.O.S. \1\........ ................................... ................. ........... Chlorinated phenol, N.O.S. \1\............. ................................... ................. ........... Chlornaphazin.............................. Naphthalenamine, N,N'-bis(2- 494-03-1 U026 chloroethyl)-. Chloroacetaldehyde......................... Acetaldehyde, chloro-.............. 107-20-0 P023 Chloroalkyl ethers, N.O.S. \1\............. ................................... ................. ........... p-Chloroaniline............................ Benzenamine, 4-chloro-............. 106-47-8 P024 Chlorobenzene.............................. Benzene, chloro-................... 108-90-7 U037 Chlorobenzilate............................ Benzeneacetic acid, 4-chloro-alpha- 510-15-6 U038 (4-chlorophenyl)-alpha-hydroxy-, ethyl ester. p-Chloro-m-cresol.......................... Phenol, 4-chloro-3-methyl-......... 59-50-7 U039 2-Chloroethyl vinyl ether.................. Ethene, (2-chloroethoxy)-.......... 110-75-8 U042 Chloroform................................. Methane, trichloro-................ 67-66-3 U044 Chloromethyl methyl ether.................. Methane, chloromethoxy-............ 107-30-2 U046 beta-Chloronaphthalene..................... Naphthalene, 2-chloro-............. 91-58-7 U047 o-Chlorophenol............................. Phenol, 2-chloro-.................. 95-57-8 U048 1-(o-Chlorophenyl)thiourea................. Thiourea, (2-chlorophenyl)-........ 5344-82-1 P026 Chloroprene................................ 1,3-Butadiene, 2-chloro-........... 126-99-8 ........... 3-Chloropropionitrile...................... Propanenitrile, 3-chloro-.......... 542-76-7 P027 Chromium................................... Same............................... 7440-47-3 ........... Chromium compounds, N.O.S. \1\............. ................................... ................. ........... Chrysene................................... Same............................... 218-01-9 U050 Citrus red No. 2........................... 2-Naphthalenol, 1-[(2,5- 6358-53-8 ........... dimethoxyphenyl)azo]-. Coal tar creosote.......................... Same............................... 8007-45-2 ........... Copper cyanide............................. Copper cyanide CuCN................ 544-92-3 P029 Copper dimethyldithiocarbamate............. Copper, 137-29-1 ........... bis(dimethylcarbamodithioato-S,S')- ,. Creosote................................... Same............................... ................. U051 p-Cresidine................................ 2-Methoxy-5-methylbenzenamine...... 120-71-8 ........... Cresol (Cresylic acid)..................... Phenol, methyl-.................... 1319-77-3 U052 Crotonaldehyde............................. 2-Butenal.......................... 4170-30-3 U053 m-Cumenyl methylcarbamate.................. Phenol, 3-(methylethyl)-, methyl 64-00-6 P202 carbamate. Cyanides (soluble salts and complexes) ................................... ................. P030 N.O.S. \1\. Cyanogen................................... Ethanedinitrile.................... 460-19-5 P031 Cyanogen bromide........................... Cyanogen bromide (CN)Br............ 506-68-3 U246 Cyanogen chloride.......................... Cyanogen chloride (CN)Cl........... 506-77-4 P033 Cycasin.................................... beta-D-Glucopyranoside, (methyl-ONN- 14901-08-7 ........... azoxy)methyl. Cycloate................................... Carbamothioic acid, cyclohexylethyl- 1134-23-2 ........... , S-ethyl ester. 2-Cyclohexyl-4,6-dinitrophenol............. Phenol, 2-cyclohexyl-4,6-dinitro-.. 131-89-5 P034 Cyclophosphamide........................... 2H-1,3,2-Oxazaphosphorin-2-amine, 50-18-0 U058 N,N-bis(2-chloroethyl)tetrahydro-, 2-oxide. 2,4-D...................................... Acetic acid, (2,4-dichlorophenoxy)- 94-75-7 U240 2,4-D, salts, esters....................... ................................... ................. U240 Daunomycin................................. 5,12-Naphthacenedione, 8-acetyl-10- 20830-81-3 U059 [(3-amino-2,3,6-trideoxy-alpha-L- lyxo- hexopyranosyl)oxy]-7,8,9,10- tetrahydro-6,8,11-trihydroxy-1- methoxy-, (8S-cis)-. Dazomet.................................... 2H-1,3,5-thiadiazine-2-thione, 533-74-4 ........... tetrahydro-3,5-dimethyl. DDD........................................ Benzene, 1,1'-(2,2- 72-54-8 U060 dichloroethylidene)bis[4-chloro-. DDE........................................ Benzene, 1,1'- 72-55-9 ........... (dichloroethenylidene)bis[4-chloro- . [[Page 113]] DDT........................................ Benzene, 1,1'-(2,2,2- 50-29-3 U061 trichloroethylidene)bis[4-chloro-. Diallate................................... Carbamothioic acid, bis(1- 2303-16-4 U062 methylethyl)-, S-(2,3-dichloro-2- propenyl) ester. Dibenz[a,h]acridine........................ Same............................... 226-36-8 ........... Dibenz[a,j]acridine........................ Same............................... 224-42-0 ........... Dibenz[a,h]anthracene...................... Same............................... 53-70-3 U063 7H-Dibenzo[c,g]carbazole................... Same............................... 194-59-2 ........... Dibenzo[a,e]pyrene......................... Naphtho[1,2,3,4-def]chrysene....... 192-65-4 ........... Dibenzo[a,h]pyrene......................... Dibenzo[b,def]chrysene............. 189-64-0 ........... Dibenzo[a,i]pyrene......................... Benzo[rst]pentaphene............... 189-55-9 U064 1,2-Dibromo-3-chloropropane................ Propane, 1,2-dibromo-3-chloro-..... 96-12-8 U066 Dibutyl phthalate.......................... 1,2-Benzenedicarboxylic acid, 84-74-2 U069 dibutyl ester. o-Dichlorobenzene.......................... Benzene, 1,2-dichloro-............. 95-50-1 U070 m-Dichlorobenzene.......................... Benzene, 1,3-dichloro-............. 541-73-1 U071 p-Dichlorobenzene.......................... Benzene, 1,4-dichloro-............. 106-46-7 U072 Dichlorobenzene, N.O.S. \1\................ Benzene, dichloro-................. 25321-22-6 ........... 3,3'-Dichlorobenzidine..................... [1,1'-Biphenyl]-4,4'-diamine, 3,3'- 91-94-1 U073 dichloro-. 1,4-Dichloro-2-butene...................... 2-Butene, 1,4-dichloro-............ 764-41-0 U074 Dichlorodifluoromethane.................... Methane, dichlorodifluoro-......... 75-71-8 U075 Dichloroethylene, N.O.S. \1\............... Dichloroethylene................... 25323-30-2 ........... 1,1-Dichloroethylene....................... Ethene, 1,1-dichloro-.............. 75-35-4 U078 1,2-Dichloroethylene....................... Ethene, 1,2-dichloro-, (E)-........ 156-60-5 U079 Dichloroethyl ether........................ Ethane, 1,1'oxybis[2-chloro-....... 111-44-4 U025 Dichloroisopropyl ether.................... Propane, 2,2'-oxybis[2-chloro-..... 108-60-1 U027 Dichloromethoxy ethane..................... Ethane, 1,1'- 111-91-1 U024 [methylenebis(oxy)]bis[2-chloro-. Dichloromethyl ether....................... Methane, oxybis[chloro-............ 542-88-1 P016 2,4-Dichlorophenol......................... Phenol, 2,4-dichloro-.............. 120-83-2 U081 2,6-Dichlorophenol......................... Phenol, 2,6-dichloro-.............. 87-65-0 U082 Dichlorophenylarsine....................... Arsonous dichloride, phenyl-....... 696-28-6 P036 Dichloropropane, N.O.S. \1\................ Propane, dichloro-................. 26638-19-7 ........... Dichloropropanol, N.O.S. \1\............... Propanol, dichloro-................ 26545-73-3 ........... Dichloropropene, N.O.S. \1\................ 1-Propene, dichloro-............... 26952-23-8 ........... 1,3-Dichloropropene........................ 1-Propene, 1,3-dichloro-........... 542-75-6 U084 Dieldrin................................... 2,7:3,6-Dimethanonaphth[2,3- 60-57-1 P037 b]oxirene, 3,4,5,6,9,9-hexachloro- 1a,2,2a,3,6,6a,7,7a-octahydro-, (1aalpha,2beta,2aalpha,3beta,6beta , 6aalpha,7beta,7aalpha)-. 1,2:3,4-Diepoxybutane...................... 2,2'-Bioxirane..................... 1464-53-5 U085 Diethylarsine.............................. Arsine, diethyl-................... 692-42-2 P038 Diethylene glycol, dicarbamate............. Ethanol, 2,2'-oxybis-, dicarbamate. 5952-26-1 U395 1,4-Diethyleneoxide........................ 1,4-Dioxane........................ 123-91-1 U108 Diethylhexyl phthalate..................... 1,2-Benzenedicarboxylic acid, bis(2- 117-81-7 U028 ethylhexyl) ester. N,N'-Diethylhydrazine...................... Hydrazine, 1,2-diethyl-............ 1615-80-1 U086 O,O-Diethyl S-methyl dithiophosphate....... Phosphorodithioic acid, O,O-diethyl 3288-58-2 U087 S-methyl ester. Diethyl-p-nitrophenyl phosphate............ Phosphoric acid, diethyl 4- 311-45-5 P041 nitrophenyl ester. Diethyl phthalate.......................... 1,2-Benzenedicarboxylic acid, 84-66-2 U088 diethyl ester. O,O-Diethyl O-pyrazinyl phosphoro- thioate. Phosphorothioic acid, O,O-diethyl O- 297-97-2 P040 pyrazinyl ester. Diethylstilbesterol........................ Phenol, 4,4'-(1,2-diethyl-1,2- 56-53-1 U089 ethenediyl)bis-, (E)-. Dihydrosafrole............................. 1,3-Benzodioxole, 5-propyl-........ 94-58-6 U090 Diisopropylfluorophosphate (DFP)........... Phosphorofluoridic acid, bis(1- 55-91-4 P043 methylethyl) ester. Dimethoate................................. Phosphorodithioic acid, O,O- 60-51-5 P044 dimethyl S-[2-(methylamino)-2- oxoethyl] ester. 3,3'-Dimethoxybenzidine.................... [1,1'-Biphenyl]-4,4'-diamine, 3,3'- 119-90-4 U091 dimethoxy-. p-Dimethylaminoazobenzene.................. Benzenamine, N,N-dimethyl-4- 60-11-7 U093 (phenylazo)-. 2,4-Dimethylaniline (2,4-xylidine)......... Benzenamine, 2,4-dimethyl-......... 95-68-1 ........... 7,12-Dimethylbenz[a]anthracene............. Benz[a]anthracene, 7,12-dimethyl-.. 57-97-6 U094 3,3'-Dimethylbenzidine..................... [1,1'-Biphenyl]-4,4'-diamine, 3,3'- 119-93-7 U095 dimethyl-. Dimethylcarbamoyl chloride................. Carbamic chloride, dimethyl-....... 79-44-7 U097 1,1-Dimethylhydrazine...................... Hydrazine, 1,1-dimethyl-........... 57-14-7 U098 1,2-Dimethylhydrazine...................... Hydrazine, 1,2-dimethyl-........... 540-73-8 U099 alpha,alpha-Dimethylphenethylamine......... Benzeneethanamine, alpha,alpha- 122-09-8 P046 dimethyl-. 2,4-Dimethylphenol......................... Phenol, 2,4-dimethyl-.............. 105-67-9 U101 Dimethyl phthalate......................... 1,2-Benzenedicarboxylic acid, 131-11-3 U102 dimethyl ester. Dimethyl sulfate........................... Sulfuric acid, dimethyl ester...... 77-78-1 U103 Dimetilan.................................. Carbamic acid, dimethyl-, 1- 644-64-4 P191 [(dimethylamino) carbonyl]-5- methyl-1H-pyrazol-3-yl ester. [[Page 114]] Dinitrobenzene, N.O.S. \1\................. Benzene, dinitro-.................. 25154-54-5 ........... 4,6-Dinitro-o-cresol....................... Phenol, 2-methyl-4,6-dinitro-...... 534-52-1 P047 4,6-Dinitro-o-cresol salts................. ................................... ................. P047 2,4-Dinitrophenol.......................... Phenol, 2,4-dinitro-............... 51-28-5 P048 2,4-Dinitrotoluene......................... Benzene, 1-methyl-2,4-dinitro-..... 121-14-2 U105 2,6-Dinitrotoluene......................... Benzene, 2-methyl-1,3-dinitro-..... 606-20-2 U106 Dinoseb.................................... Phenol, 2-(1-methylpropyl)-4,6- 88-85-7 P020 dinitro-. Di-n-octyl phthalate....................... 1,2-Benzenedicarboxylic acid, 117-84-0 U017 dioctyl ester. Diphenylamine.............................. Benzenamine, N-phenyl-............. 122-39-4 ........... 1,2-Diphenylhydrazine...................... Hydrazine, 1,2-diphenyl-........... 122-66-7 U109 Di-n-propylnitrosamine..................... 1-Propanamine, N-nitroso-N-propyl-. 621-64-7 U111 Disulfiram................................. Thioperoxydicarbonic diamide, 97-77-8 ........... tetraethyl. Disulfoton................................. Phosphorodithioic acid, O,O-diethyl 298-04-4 P039 S-[2-(ethylthio)ethyl] ester. Dithiobiuret............................... Thioimidodicarbonic diamide [(H2 541-53-7 P049 N)C(S)]2 NH. Endosulfan................................. 6,9-Methano-2,4,3- 115-29-7 P050 benzodioxathiepin, 6,7,8,9,10,10- hexachloro-1,5,5a,6,9,9a- hexahydro-, 3-oxide. Endothall.................................. 7-Oxabicyclo[2.2.1]heptane-2,3- 145-73-3 P088 dicarboxylic acid. Endrin..................................... 2,7:3,6-Dimethanonaphth[2,3- 72-20-8 P051 b]oxirene, 3,4,5,6,9,9-hexachloro- 1a,2,2a,3,6,6a,7,7a-octa-hydro-, (1aalpha,2beta,2abeta,3alpha,6alph a, 6abeta,7beta,7aalpha)-. Endrin metabolites......................... ................................... ................. P051 Epichlorohydrin............................ Oxirane, (chloromethyl)-........... 106-89-8 U041 Epinephrine................................ 1,2-Benzenediol, 4-[1-hydroxy-2- 51-43-4 P042 (methylamino)ethyl]-, (R)-. EPTC....................................... Carbamothioic acid, dipropyl-, S- 759-94-4 ........... ethyl ester. Ethyl carbamate (urethane)................. Carbamic acid, ethyl ester......... 51-79-6 U238 Ethyl cyanide.............................. Propanenitrile..................... 107-12-0 P101 Ethyl Ziram................................ Zinc, bis(diethylcarbamodithioato- 14324-55-1 ........... S,S')-. Ethylenebisdithiocarbamic acid............. Carbamodithioic acid, 1,2- 111-54-6 U114 ethanediylbis-. Ethylenebisdithiocarbamic acid, salts and ................................... ................. U114 esters. Ethylene dibromide......................... Ethane, 1,2-dibromo-............... 106-93-4 U067 Ethylene dichloride........................ Ethane, 1,2-dichloro-.............. 107-06-2 U077 Ethylene glycol monoethyl ether............ Ethanol, 2-ethoxy-................. 110-80-5 U359 Ethyleneimine.............................. Aziridine.......................... 151-56-4 P054 Ethylene oxide............................. Oxirane............................ 75-21-8 U115 Ethylenethiourea........................... 2-Imidazolidinethione.............. 96-45-7 U116 Ethylidene dichloride...................... Ethane, 1,1-dichloro-.............. 75-34-3 U076 Ethyl methacrylate......................... 2-Propenoic acid, 2-methyl-, ethyl 97-63-2 U118 ester. Ethyl methanesulfonate..................... Methanesulfonic acid, ethyl ester.. 62-50-0 U119 Famphur.................................... Phosphorothioic acid, O-[4- 52-85-7 P097 [(dimethylamino)sulfonyl]phenyl] O,O-dimethyl ester. Ferbam..................................... Iron, tris(dimethylcarbamodithioato- 14484-64-1 ........... S,S')-,. Fluoranthene............................... Same............................... 206-44-0 U120 Fluorine................................... Same............................... 7782-41-4 P056 Fluoroacetamide............................ Acetamide, 2-fluoro-............... 640-19-7 P057 Fluoroacetic acid, sodium salt............. Acetic acid, fluoro-, sodium salt.. 62-74-8 P058 Formaldehyde............................... Same............................... 50-00-0 U122 Formetanate hydrochloride.................. Methanimidamide, N,N-dimethyl-N'-[3- 23422-53-9 P198 [[(methylamino) carbonyl]oxy]phenyl]-, monohydrochloride. Formic acid................................ Same............................... 64-18-6 U123 Formparanate............................... Methanimidamide, N,N-dimethyl-N'-[2- 17702-57-7 P197 methyl-4-[[(methylamino) carbonyl]oxy]phenyl]-. Glycidylaldehyde........................... Oxiranecarboxyaldehyde............. 765-34-4 U126 Halomethanes, N.O.S. \1\................... ................................... ................. ........... Heptachlor................................. 4,7-Methano-1H-indene, 76-44-8 P059 1,4,5,6,7,8,8-heptachloro- 3a,4,7,7a-tetrahydro-. Heptachlor epoxide......................... 2,5-Methano-2H-indeno[1,2- 1024-57-3 ........... b]oxirene, 2,3,4,5,6,7,7- heptachloro-1a,1b,5,5a,6,6a-hexa- hydro-, (1aalpha,1bbeta,2alpha,5alpha, 5abeta,6beta,6aalpha)-. Heptachlor epoxide (alpha, beta, and gamma ................................... ................. ........... isomers). Heptachlorodibenzofurans................... ................................... ................. ........... [[Page 115]] Heptachlorodibenzo-p-dioxins............... ................................... ................. ........... Hexachlorobenzene.......................... Benzene, hexachloro-............... 118-74-1 U127 Hexachlorobutadiene........................ 1,3-Butadiene, 1,1,2,3,4,4- 87-68-3 U128 hexachloro-. Hexachlorocyclopentadiene.................. 1,3-Cyclopentadiene, 1,2,3,4,5,5- 77-47-4 U130 hexachloro-. Hexachlorodibenzo-p-dioxins................ ................................... ................. ........... Hexachlorodibenzofurans.................... ................................... ................. ........... Hexachloroethane........................... Ethane, hexachloro-................ 67-72-1 U131 Hexachlorophene............................ Phenol, 2,2'-methylenebis[3,4,6- 70-30-4 U132 trichloro-. Hexachloropropene.......................... 1-Propene, 1,1,2,3,3,3-hexachloro-. 1888-71-7 U243 Hexaethyl tetraphosphate................... Tetraphosphoric acid, hexaethyl 757-58-4 P062 ester. Hydrazine.................................. Same............................... 302-01-2 U133 Hydrogen cyanide........................... Hydrocyanic acid................... 74-90-8 P063 Hydrogen fluoride.......................... Hydrofluoric acid.................. 7664-39-3 U134 Hydrogen sulfide........................... Hydrogen sulfide H2 S.............. 7783-06-4 U135 Indeno[1,2,3-cd]pyrene..................... Same............................... 193-39-5 U137 3-Iodo-2-propynyl n-butylcarbamate......... Carbamic acid, butyl-, 3-iodo-2- 55406-53-6 ........... propynyl ester. Isobutyl alcohol........................... 1-Propanol, 2-methyl-.............. 78-83-1 U140 Isodrin.................................... 1,4,5,8-Dimethanonaphthalene, 465-73-6 P060 1,2,3,4,10,10-hexachloro- 1,4,4a,5,8,8a-hexa hydro-, (1alpha, 4alpha, 4abeta, 5beta, 8beta, 8abeta)-. Isolan..................................... Carbamic acid, dimethyl-, 3-methyl- 119-38-0 P192 1-(1-methylethyl)-1H-pyrazol-5-yl ester. Isosafrole................................. 1,3-Benzodioxole, 5-(1-propenyl)-.. 120-58-1 U141 Kepone..................................... 1,3,4-Metheno-2H- 143-50-0 U142 cyclobuta[cd]pentalen-2-one, 1,1a,3,3a,4,5,5,5a,5b,6- decachlorooctahydro-. Lasiocarpine............................... 2-Butenoic acid, 2-methyl-,7-[[2,3- 303-34-4 U143 dihydroxy-2-(1-methoxyethyl)-3- methyl-1- oxobutoxy]methyl]-2,3,5,7a- tetrahydro-1H-pyrrolizin-1-yl ester,. [1S- [1alpha(Z),7(2S*,3R*),7aalpha]]-. Lead....................................... Same............................... 7439-92-1 ........... Lead compounds, N.O.S. \1\................. ................................... ................. ........... Lead acetate............................... Acetic acid, lead(2+) salt......... 301-04-2 U144 Lead phosphate............................. Phosphoric acid, lead(2+) salt 7446-27-7 U145 (2:3). Lead subacetate............................ Lead, bis(acetato-O)tetrahydroxytri- 1335-32-6 U146 . Lindane.................................... Cyclohexane, 1,2,3,4,5,6-hexachloro- 58-89-9 U129 , (1alpha,2alpha,3beta,4alpha, 5alpha,6beta)-. Maleic anhydride........................... 2,5-Furandione..................... 108-31-6 U147 Maleic hydrazide........................... 3,6-Pyridazinedione, 1,2-dihydro-.. 123-33-1 U148 Malononitrile.............................. Propanedinitrile................... 109-77-3 U149 Manganese dimethyldithiocarbamate.......... Manganese, 15339-36-3 P196 bis(dimethylcarbamodithioato-S,S')- ,. Melphalan.................................. L-Phenylalanine, 4-[bis(2- 148-82-3 U150 chloroethyl)aminol]-. Mercury.................................... Same............................... 7439-97-6 U151 Mercury compounds, N.O.S. \1\.............. ................................... ................. ........... Mercury fulminate.......................... Fulminic acid, mercury(2+) salt.... 628-86-4 P065 Metam Sodium............................... Carbamodithioic acid, methyl-, 137-42-8 monosodium salt. Methacrylonitrile.......................... 2-Propenenitrile, 2-methyl-........ 126-98-7 U152 Methapyrilene.............................. 1,2-Ethanediamine, N,N-dimethyl-N'- 91-80-5 U155 2-pyridinyl-N'-(2-thienylmethyl)-. Methiocarb................................. Phenol, (3,5-dimethyl-4- 2032-65-7 P199 (methylthio)-, methylcarbamate. Methomyl................................... Ethanimidothioic acid, N- 16752-77-5 P066 [[(methylamino)carbonyl]oxy]-, methyl ester. Methoxychlor............................... Benzene, 1,1'-(2,2,2- 72-43-5 U247 trichloroethylidene)bis[4-methoxy-. Methyl bromide............................. Methane, bromo-.................... 74-83-9 U029 Methyl chloride............................ Methane, chloro-................... 74-87-3 U045 Methyl chlorocarbonate..................... Carbonochloridic acid, methyl ester 79-22-1 U156 Methyl chloroform.......................... Ethane, 1,1,1-trichloro-........... 71-55-6 U226 3-Methylcholanthrene....................... Benz[j]aceanthrylene, 1,2-dihydro-3- 56-49-5 U157 methyl-. 4,4'-Methylenebis(2-chloroaniline)......... Benzenamine, 4,4'-methylenebis[2- 101-14-4 U158 chloro-. Methylene bromide.......................... Methane, dibromo-.................. 74-95-3 U068 Methylene chloride......................... Methane, dichloro-................. 75-09-2 U080 Methyl ethyl ketone (MEK).................. 2-Butanone......................... 78-93-3 U159 [[Page 116]] Methyl ethyl ketone peroxide............... 2-Butanone, peroxide............... 1338-23-4 U160 Methyl hydrazine........................... Hydrazine, methyl-................. 60-34-4 P068 Methyl iodide.............................. Methane, iodo-..................... 74-88-4 U138 Methyl isocyanate.......................... Methane, isocyanato-............... 624-83-9 P064 2-Methyllactonitrile....................... Propanenitrile, 2-hydroxy-2-methyl- 75-86-5 P069 Methyl methacrylate........................ 2-Propenoic acid, 2-methyl-, methyl 80-62-6 U162 ester. Methyl methanesulfonate.................... Methanesulfonic acid, methyl ester. 66-27-3 ........... Methyl parathion........................... Phosphorothioic acid, O,O-dimethyl 298-00-0 P071 O-(4-nitrophenyl) ester. Methylthiouracil........................... 4(1H)-Pyrimidinone, 2,3-dihydro-6- 56-04-2 U164 methyl-2-thioxo-. Metolcarb.................................. Carbamic acid, methyl-, 3- 1129-41-5 P190 methylphenyl ester. Mexacarbate................................ Phenol, 4-(dimethylamino)-3,5- 315-18-4 P128 dimethyl-, methylcarbamate (ester). Mitomycin C................................ Azirino[2',3':3,4]pyrrolo[1,2- 50-07-7 U010 a]indole-4,7-dione, 6-amino-8- [[(aminocarbonyl)oxy]methyl]- 1,1a,2,8,8a,8b-hexahydro-8a- methoxy-5- methyl-, [1aS- (1aalpha,8beta,8aalpha,8balpha)]-.. MNNG....................................... Guanidine, N-methyl-N'-nitro-N- 70-25-7 U163 nitroso-. Molinate................................... 1H-Azepine-1-carbothioic acid, 2212-67-1 ........... hexahydro-, S-ethyl ester. Mustard gas................................ Ethane, 1,1'-thiobis[2-chloro-..... 505-60-2 ........... Naphthalene................................ Same............................... 91-20-3 U165 1,4-Naphthoquinone......................... 1,4-Naphthalenedione............... 130-15-4 U166 alpha-Naphthylamine........................ 1-Naphthalenamine.................. 134-32-7 U167 beta-Naphthylamine......................... 2-Naphthalenamine.................. 91-59-8 U168 alpha-Naphthylthiourea..................... Thiourea, 1-naphthalenyl-.......... 86-88-4 P072 Nickel..................................... Same............................... 7440-02-0 ........... Nickel compounds, N.O.S. \1\............... ................................... ................. ........... Nickel carbonyl............................ Nickel carbonyl Ni(CO)4, (T-4)-.... 13463-39-3 P073 Nickel cyanide............................. Nickel cyanide Ni(CN)2............. 557-19-7 P074 Nicotine................................... Pyridine, 3-(1-methyl-2- 54-11-5 P075 pyrrolidinyl)-, (S)-. Nicotine salts............................. ................................... ................. P075 Nitric oxide............................... Nitrogen oxide NO.................. 10102-43-9 P076 p-Nitroaniline............................. Benzenamine, 4-nitro-.............. 100-01-6 P077 Nitrobenzene............................... Benzene, nitro-.................... 98-95-3 U169 Nitrogen dioxide........................... Nitrogen oxide NO2................. 10102-44-0 P078 Nitrogen mustard........................... Ethanamine, 2-chloro-N-(2- 51-75-2 ........... chloroethyl)-N-methyl-. Nitrogen mustard, hydrochloride salt....... ................................... ................. ........... Nitrogen mustard N-oxide................... Ethanamine, 2-chloro-N-(2- 126-85-2 ........... chloroethyl)-N-methyl-, N-oxide. Nitrogen mustard, N-oxide, hydro- chloride ................................... ................. ........... salt. Nitroglycerin.............................. 1,2,3-Propanetriol, trinitrate..... 55-63-0 P081 p-Nitrophenol.............................. Phenol, 4-nitro-................... 100-02-7 U170 2-Nitropropane............................. Propane, 2-nitro-.................. 79-46-9 U171 Nitrosamines, N.O.S. \1\................... ................................... 35576-91-1 ........... N-Nitrosodi-n-butylamine................... 1-Butanamine, N-butyl-N-nitroso-... 924-16-3 U172 N-Nitrosodiethanolamine.................... Ethanol, 2,2'-(nitrosoimino)bis-... 1116-54-7 U173 N-Nitrosodiethylamine...................... Ethanamine, N-ethyl-N-nitroso-..... 55-18-5 U174 N-Nitrosodimethylamine..................... Methanamine, N-methyl-N-nitroso-... 62-75-9 P082 N-Nitroso-N-ethylurea...................... Urea, N-ethyl-N-nitroso-........... 759-73-9 U176 N-Nitrosomethylethylamine.................. Ethanamine, N-methyl-N-nitroso-.... 10595-95-6 ........... N-Nitroso-N-methylurea..................... Urea, N-methyl-N-nitroso-.......... 684-93-5 U177 N-Nitroso-N-methylurethane................. Carbamic acid, methylnitroso-, 615-53-2 U178 ethyl ester. N-Nitrosomethylvinylamine.................. Vinylamine, N-methyl-N-nitroso-.... 4549-40-0 P084 N-Nitrosomorpholine........................ Morpholine, 4-nitroso-............. 59-89-2 ........... N-Nitrosonornicotine....................... Pyridine, 3-(1-nitroso-2- 16543-55-8 ........... pyrrolidinyl)-, (S)-. N-Nitrosopiperidine........................ Piperidine, 1-nitroso-............. 100-75-4 U179 N-Nitrosopyrrolidine....................... Pyrrolidine, 1-nitroso-............ 930-55-2 U180 N-Nitrososarcosine......................... Glycine, N-methyl-N-nitroso-....... 13256-22-9 ........... 5-Nitro-o-toluidine........................ Benzenamine, 2-methyl-5-nitro-..... 99-55-8 U181 Octachlorodibenzo-p-dioxin (OCDD).......... 1,2,3,4,6,7,8,9-Octachlorodibenzo-p- 3268-87-9 ........... dioxin. Octachlorodibenzofuran (OCDF).............. 1,2,3,4,6,7,8,9- 39001-02-0 ........... Octachlorodibenofuran. Octamethylpyrophosphoramide................ Diphosphoramide, octamethyl-....... 152-16-9 P085 Osmium tetroxide........................... Osmium oxide OsO4, (T-4)-.......... 20816-12-0 P087 Oxamyl..................................... Ethanimidothioc acid, 2- 23135-22-0 P194 (dimethylamino)-N- [[(methylamino)carbonyl]oxy]-2-oxo- , methyl ester. [[Page 117]] Paraldehyde................................ 1,3,5-Trioxane, 2,4,6-trimethyl-... 123-63-7 U182 Parathion.................................. Phosphorothioic acid, O,O-diethyl O- 56-38-2 P089 (4-nitrophenyl) ester. Pebulate................................... Carbamothioic acid, butylethyl-, S- 1114-71-2 ........... propyl ester. Pentachlorobenzene......................... Benzene, pentachloro-.............. 608-93-5 U183 Pentachlorodibenzo-p-dioxins............... ................................... ................. ........... Pentachlorodibenzofurans................... ................................... ................. ........... Pentachloroethane.......................... Ethane, pentachloro-............... 76-01-7 U184 Pentachloronitrobenzene (PCNB)............. Benzene, pentachloronitro-......... 82-68-8 U185 Pentachlorophenol.......................... Phenol, pentachloro-............... 87-86-5 See F027 Phenacetin................................. Acetamide, N-(4-ethoxyphenyl)-..... 62-44-2 U187 Phenol..................................... Same............................... 108-95-2 U188 1,2-Phenylenediamine....................... 1,2-Benzenediamine................. 95-54-5 ........... 1,3-Phenylenediamine....................... 1,3-Benzenediamine................. 108-45-2 ........... Phenylenediamine........................... Benzenediamine..................... 25265-76-3 ........... Phenylmercury acetate...................... Mercury, (acetato-O)phenyl-........ 62-38-4 P092 Phenylthiourea............................. Thiourea, phenyl-.................. 103-85-5 P093 Phosgene................................... Carbonic dichloride................ 75-44-5 P095 Phosphine.................................. Same............................... 7803-51-2 P096 Phorate.................................... Phosphorodithioic acid, O,O-diethyl 298-02-2 P094 S-[(ethylthio)methyl] ester. Phthalic acid esters, N.O.S. \1\........... ................................... ................. ........... Phthalic anhydride......................... 1,3-Isobenzofurandione............. 85-44-9 U190 Physostigmine.............................. Pyrrolo[2,3-b]indol-5-01, 57-47-6 P204 1,2,3,3a,8,8a-hexahydro-1,3a,8- trimethyl-, methylcarbamate (ester), (3aS-cis)-. Physostigmine salicylate................... Benzoic acid, 2-hydroxy-, compd. 57-64-7 P188 with (3aS-cis) -1,2,3,3a,8,8a- hexahydro-1,3a,8-trimethylpyrrolo [2,3-b]indol-5-yl methylcarbamate ester (1:1). 2-Picoline................................. Pyridine, 2-methyl-................ 109-06-8 U191 Polychlorinated biphenyls, N.O.S. \1\...... ................................... ................. ........... Potassium cyanide.......................... Potassium cyanide K(CN)............ 151-50-8 P098 Potassium dimethyldithiocarbamate.......... Carbamodithioic acid, dimethyl, 128-03-0 ........... potassium salt. Potassium n-hydroxymethyl-n-methyl- Carbamodithioic acid, 51026-28-9 ........... dithiocarbamate. (hydroxymethyl)methyl-, monopotassium salt. Potassium n-methyldithiocarbamate.......... Carbamodithioic acid, methyl- 137-41-7 ........... monopotassium salt. Potassium pentachlorophenate............... Pentachlorophenol, potassium salt.. 7778736 None Potassium silver cyanide................... Argentate(1-), bis(cyano-C)-, 506-61-6 P099 potassium. Promecarb.................................. Phenol, 3-methyl-5-(1-methylethyl)- 2631-37-0 P201 , methyl carbamate. Pronamide.................................. Benzamide, 3,5-dichloro-N-(1,1- 23950-58-5 U192 dimethyl-2-propynyl)-. 1,3-Propane sultone........................ 1,2-Oxathiolane, 2,2-dioxide....... 1120-71-4 U193 n-Propylamine.............................. 1-Propanamine...................... 107-10-8 U194 Propargyl alcohol.......................... 2-Propyn-1-ol...................... 107-19-7 P102 Propham.................................... Carbamic acid, phenyl-, 1- 122-42-9 U373 methylethyl ester. Propoxur................................... Phenol, 2-(1-methylethoxy)-, 114-26-1 U411 methylcarbamate. Propylene dichloride....................... Propane, 1,2-dichloro-............. 78-87-5 U083 1,2-Propylenimine.......................... Aziridine, 2-methyl-............... 75-55-8 P067 Propylthiouracil........................... 4(1H)-Pyrimidinone, 2,3-dihydro-6- 51-52-5 ........... propyl-2-thioxo-. Prosulfocarb............................... Carbamothioic acid, dipropyl-, S- 52888-80-9 U387 (phenylmethyl) ester. Pyridine................................... Same............................... 110-86-1 U196 Reserpine.................................. Yohimban-16-carboxylic acid, 11,17- 50-55-5 U200 dimethoxy-18-[(3,4,5- trimethoxybenzoyl)oxy]-smethyl ester, (3beta,16beta,17alpha,18beta,20alp ha)-. Resorcinol................................. 1,3-Benzenediol.................... 108-46-3 U201 Saccharin.................................. 1,2-Benzisothiazol-3(2H)-one, 1,1- 81-07-2 U202 dioxide. Saccharin salts............................ ................................... ................. U202 Safrole.................................... 1,3-Benzodioxole, 5-(2-propenyl)-.. 94-59-7 U203 Selenium................................... Same............................... 7782-49-2 ........... Selenium compounds, N.O.S. \1\............. ................................... ................. ........... Selenium dioxide........................... Selenious acid..................... 7783-00-8 U204 Selenium sulfide........................... Selenium sulfide SeS2.............. 7488-56-4 U205 [[Page 118]] Selenium, tetrakis(dimethyl- Carbamodithioic acid, dimethyl-, 144-34-3 ........... dithiocarbamate). tetraanhydrosulfide with orthothioselenious acid. Selenourea................................. Same............................... 630-10-4 P103 Silver..................................... Same............................... 7440-22-4 ........... Silver compounds, N.O.S. \1\............... ................................... ................. ........... Silver cyanide............................. Silver cyanide Ag(CN).............. 506-64-9 P104 Silvex (2,4,5-TP).......................... Propanoic acid, 2-(2,4,5- 93-72-1 See F027 trichlorophenoxy)-. Sodium cyanide............................. Sodium cyanide Na(CN).............. 143-33-9 P106 Sodium dibutyldithiocarbamate.............. Carbamodithioic acid, dibutyl, 136-30-1 ........... sodium salt. Sodium diethyldithiocarbamate.............. Carbamodithioic acid, diethyl-, 148-18-5 sodium salt. Sodium dimethyldithiocarbamate............. Carbamodithioic acid, dimethyl-, 128-04-1 ........... sodium salt. Sodium pentachlorophenate.................. Pentachlorophenol, sodium salt..... 131522 None Streptozotocin............................. D-Glucose, 2-deoxy-2- 18883-66-4 U206 [[(methylnitrosoamino)carbonyl]ami no]-. Strychnine................................. Strychnidin-10-one................. 57-24-9 P108 Strychnine salts........................... ................................... ................. P108 Sulfallate................................. Carbamodithioic acid, diethyl-, 2- 95-06-7 ........... chloro-2-propenyl ester. TCDD....................................... Dibenzo[b,e][1,4]dioxin, 2,3,7,8- 1746-01-6 ........... tetrachloro-. Tetrabutylthiuram disulfide................ Thioperoxydicarbonic diamide, 1634-02-2 ........... tetrabutyl. 1,2,4,5-Tetrachlorobenzene................. Benzene, 1,2,4,5-tetrachloro-...... 95-94-3 U207 Tetrachlorodibenzo-p-dioxins............... ................................... ................. ........... Tetrachlorodibenzofurans................... ................................... ................. ........... Tetrachloroethane, N.O.S. \1\.............. Ethane, tetrachloro-, N.O.S........ 25322-20-7 ........... 1,1,1,2-Tetrachloroethane.................. Ethane, 1,1,1,2-tetrachloro-....... 630-20-6 U208 1,1,2,2-Tetrachloroethane.................. Ethane, 1,1,2,2-tetrachloro-....... 79-34-5 U209 Tetrachloroethylene........................ Ethene, tetrachloro-............... 127-18-4 U210 2,3,4,6-Tetrachlorophenol.................. Phenol, 2,3,4,6-tetrachloro-....... 58-90-2 See F027 2,3,4,6-tetrachlorophenol, potassium salt.. same............................... 53535276 None 2,3,4,6-tetrachlorophenol, sodium salt..... same............................... 25567559 None Tetraethyldithiopyrophosphate.............. Thiodiphosphoric acid, tetraethyl 3689-24-5 P109 ester. Tetraethyl lead............................ Plumbane, tetraethyl-.............. 78-00-2 P110 Tetraethyl pyrophosphate................... Diphosphoric acid, tetraethyl ester 107-49-3 P111 Tetramethylthiuram monosulfide............. Bis(dimethylthiocarbamoyl) sulfide. 97-74-5 ........... Tetranitromethane.......................... Methane, tetranitro-............... 509-14-8 P112 Thallium................................... Same............................... 7440-28-0 ........... Thallium compounds, N.O.S. \1\............. ................................... ................. ........... Thallic oxide.............................. Thallium oxide Tl2 O3.............. 1314-32-5 P113 Thallium(I) acetate........................ Acetic acid, thallium(1+) salt..... 563-68-8 U214 Thallium(I) carbonate...................... Carbonic acid, dithallium(1+) salt. 6533-73-9 U215 Thallium(I) chloride....................... Thallium chloride TlCl............. 7791-12-0 U216 Thallium(I) nitrate........................ Nitric acid, thallium(1+) salt..... 10102-45-1 U217 Thallium selenite.......................... Selenious acid, dithallium(1+) salt 12039-52-0 P114 Thallium(I) sulfate........................ Sulfuric acid, dithallium(1+) salt. 7446-18-6 P115 Thioacetamide.............................. Ethanethioamide.................... 62-55-5 U218 Thiodicarb................................. Ethanimidothioic acid, N,N'- 59669-26-0 U410 [thiobis [(methylimino) carbonyloxy]] bis-, dimethyl ester. Thiofanox.................................. 2-Butanone, 3,3-dimethyl-1- 39196-18-4 P045 (methylthio)-, 0- [(methylamino)carbonyl] oxime. Thiomethanol............................... Methanethiol....................... 74-93-1 U153 Thiophanate-methyl......................... Carbamic acid, [1,2-phyenylenebis 23564-05-8 U409 (iminocarbonothioyl)] bis-, dimethyl ester. Thiophenol................................. Benzenethiol....................... 108-98-5 P014 Thiosemicarbazide.......................... Hydrazinecarbothioamide............ 79-19-6 P116 Thiourea................................... Same............................... 62-56-6 U219 Thiram..................................... Thioperoxydicarbonic diamide [(H2 137-26-8 U244 N)C(S)]2 S2, tetramethyl-. Tirpate.................................... 1,3-Dithiolane-2-carboxaldehyde, 26419-73-8 P185 2,4-dimethyl-, O-[(methylamino) carbonyl] oxime. Toluene.................................... Benzene, methyl-................... 108-88-3 U220 Toluenediamine............................. Benzenediamine, ar-methyl-......... 25376-45-8 U221 Toluene-2,4-diamine........................ 1,3-Benzenediamine, 4-methyl-...... 95-80-7 ........... Toluene-2,6-diamine........................ 1,3-Benzenediamine, 2-methyl-...... 823-40-5 ........... Toluene-3,4-diamine........................ 1,2-Benzenediamine, 4-methyl-...... 496-72-0 ........... Toluene diisocyanate....................... Benzene, 1,3-diisocyanatomethyl-... 26471-62-5 U223 o-Toluidine................................ Benzenamine, 2-methyl-............. 95-53-4 U328 o-Toluidine hydrochloride.................. Benzenamine, 2-methyl-, 636-21-5 U222 hydrochloride. p-Toluidine................................ Benzenamine, 4-methyl-............. 106-49-0 U353 Toxaphene.................................. Same............................... 8001-35-2 P123 Triallate.................................. Carbamothioic acid, bis(1- 2303-17-5 U389 methylethyl)-, S-(2,3,3-trichloro- 2-propenyl) ester. [[Page 119]] 1,2,4-Trichlorobenzene..................... Benzene, 1,2,4-trichloro-.......... 120-82-1 ........... 1,1,2-Trichloroethane...................... Ethane, 1,1,2-trichloro-........... 79-00-5 U227 Trichloroethylene.......................... Ethene, trichloro-................. 79-01-6 U228 Trichloromethanethiol...................... Methanethiol, trichloro-........... 75-70-7 P118 Trichloromonofluoromethane................. Methane, trichlorofluoro-.......... 75-69-4 U121 2,4,5-Trichlorophenol...................... Phenol, 2,4,5-trichloro-........... 95-95-4 See F027 2,4,6-Trichlorophenol...................... Phenol, 2,4,6-trichloro-........... 88-06-2 See F027 2,4,5-T.................................... Acetic acid, (2,4,5- 93-76-5 See F027 trichlorophenoxy)-. Trichloropropane, N.O.S. \1\............... ................................... 25735-29-9 ........... 1,2,3-Trichloropropane..................... Propane, 1,2,3-trichloro-.......... 96-18-4 ........... Triethylamine.............................. Ethanamine, N,N-diethyl-........... 121-44-8 U404 O,O,O-Triethyl phosphorothioate............ Phosphorothioic acid, O,O,O- 126-68-1 ........... triethyl ester. 1,3,5-Trinitrobenzene...................... Benzene, 1,3,5-trinitro-........... 99-35-4 U234 Tris(1-aziridinyl)phosphine sulfide........ Aziridine, 1,1',1''- 52-24-4 ........... phosphinothioylidynetris-. Tris(2,3-dibromopropyl) phosphate.......... 1-Propanol, 2,3-dibromo-, phosphate 126-72-7 U235 (3:1). Trypan blue................................ 2,7-Naphthalenedisulfonic acid, 72-57-1 U236 3,3'-[(3,3'-dimethyl[1,1'- biphenyl]-4,4'-diyl)bis(azo)]- bis[5-amino-4-hydroxy-, tetrasodium salt.. Uracil mustard............................. 2,4-(1H,3H)-Pyrimidinedione, 5- 66-75-1 U237 [bis(2-chloroethyl)amino]-. Vanadium pentoxide......................... Vanadium oxide V2 O5............... 1314-62-1 P120 Vernolate.................................. Carbamothioic acid, dipropyl-,S- 1929-77-7 ........... propyl ester. Vinyl chloride............................. Ethene, chloro-.................... 75-01-4 U043 Warfarin................................... 2H-1-Benzopyran-2-one, 4-hydroxy-3- 81-81-2 U248 (3-oxo-1-phenylbutyl)-, when present at concentrations less than 0.3%. Warfarin................................... 2H-1-Benzopyran-2-one, 4-hydroxy-3- 81-81-2 P001 (3-oxo-1-phenylbutyl)-, when present at concentrations greater than 0.3%. Warfarin salts, when present at ................................... ................. U248 concentrations less than 0.3%. Warfarin salts, when present at ................................... ................. P001 concentrations greater than 0.3%. Zinc cyanide............................... Zinc cyanide Zn(CN)2............... 557-21-1 P121 Zinc phosphide............................. Zinc phosphide Zn3 P2, when present 1314-84-7 P122 at concentrations greater than 10%. Zinc phosphide............................. Zinc phosphide Zn3 P2, when present 1314-84-7 U249 at concentrations of 10% or less. Ziram...................................... ZInc, bis(dimethylcarbamodithioato- 137-30-4 P205 S,S')-, (T-4)-. ---------------------------------------------------------------------------------------------------------------- \1\ The abbreviation N.O.S. (not otherwise specified) signifies those members of the general class not specifically listed by name in this appendix. [53 FR 13388, Apr. 22, 1988, as amended at 53 FR 43881, Oct. 31, 1988; 54 FR 50978, Dec. 11, 1989; 55 FR 50483, Dec. 6, 1990; 56 FR 7568, Feb. 25, 1991; 59 FR 468, Jan. 4, 1994; 59 FR 31551, June 20, 1994; 60 FR 7853, Feb. 9, 1995; 60 FR 19165, Apr. 17, 1995; 62 FR 32977, June 17, 1997; 63 FR 24625, May 4, 1998; 65 FR 14475, Mar. 17, 2000; 65 FR 67127, Nov. 8, 2000; 70 FR 9177, Feb. 24, 2005; 71 FR 40271, July 14, 2006] [[Page 120]] Appendix IX to Part 261--Wastes Excluded Under Sec. Sec. 260.20 and 260.22 Table 1--Wastes Excluded From Non-Specific Sources ------------------------------------------------------------------------ Facility Address Waste description ------------------------------------------------------------------------ Aluminum Company 750 Norcold Ave., Wastewater treatment plant (WWTP) of America. Sidney, Ohio sludges generated from the 45365. chemical conversion coating of aluminum (EPA Hazardous Waste No. F019) and WWTP sludges generated from electroplating operations (EPA Hazardous Waste No. F006) and stored in an on-site landfill. This is an exclusion for approximately 16,772 cubic yards of landfilled WWTP filter cake. This exclusion applies only if the waste filter cake remains in place or, if excavated, is disposed of in a Subtitle D landfill which is permitted, licensed, or registered by a state to manage industrial solid waste. This exclusion was published on April 6, 1999. 1. The constituent concentrations measured in the TCLP extract may not exceed the following levels (mg/L): Arsenic--5; Barium--100; Chromium--5; Cobalt--210; Copper-- 130; Nickel--70; Vanadium--30; Zinc--1000; Fluoride--400; Acetone--400; Methylene Chloride-- 0.5; Bis(2-ethylhexyl)phthalate-- 0.6. 2. (a) If, anytime after disposal of the delisted waste, Alcoa possesses or is otherwise made aware of any environmental data (including but not limited to leachate data or groundwater monitoring data) or any other data relevant to the delisted waste indicating that any constituent identified in Condition (1) is at a level in the leachate higher than the delisting level established in Condition (1), or is at a level in the ground water or soil higher than the health based level, then Alcoa must report such data, in writing, to the Regional Administrator within 10 days of first possessing or being made aware of that data. (b) Based on the information described in paragraph (a) and any other information received from any source, the Regional Administrator will make a preliminary determination as to whether the reported information requires Agency action to protect human health or the environment. Further action may include suspending or revoking this exclusion, or other appropriate response necessary to protect human health and the environment. (c) If the Regional Administrator determines that the reported information does require Agency action, the Regional Administrator will notify the facility in writing of the actions the Regional Administrator believes are necessary to protect human health and the environment. The notice shall include a statement of the proposed action and a statement providing the facility with an opportunity to present information as to why the proposed Agency action is not necessary or to suggest an alternative action. The facility shall have 10 days from the date of the Regional Administrator's notice to present such information. (d) Following the receipt of information from the facility described in paragraph (c) or (if no information is presented under paragraph (c) the initial receipt of information described in paragraph (a), the Regional Administrator will issue a final written determination describing the Agency actions that are necessary to protect human health or the environment. Any required action described in the Regional Administrator's determination shall become effective immediately, unless the Regional Administrator provides otherwise. Alumnitec, Inc. Jeffersonville, Dewatered wastewater treatment (formerly IN. sludge (EPA Hazardous Waste No. Profile F019) generated from the chemical Extrusion Co., conversion of aluminum after formerly United April 29, 1986. Technologies Automotive, Inc.). American Metals Westlake, Ohio... Wastewater treatment plant (WWTP) Corporation. sludges from the chemical conversion coating (phosphating) of aluminum (EPA Hazardous Waste No. F019) and other solid wastes previously disposed in an on-site landfill. This is a one-time exclusion for 12,400 cubic yards of landfilled WWTP sludge. This exclusion is effective on January 15, 2002. 1. Delisting Levels: (A) The constituent concentrations measured in the TCLP extract may not exceed the following levels (mg/L): antimony--1.52; arsenic-- 0.691; barium--100; beryllium-- 3.07; cadmium--1; chromium--5; cobalt--166; copper--67,300; lead--5; mercury--0.2; nickel-- 209; selenium--1; silver--5; thallium--0.65; tin--1,660; vanadium--156; and zinc--2,070. (B) The total constituent concentrations in any sample may not exceed the following levels (mg/kg): arsenic--9,280; mercury-- 94; and polychlorinated biphenyls--0.265. (C) Concentrations of dioxin and furan congeners cannot exceed values which would result in a cancer risk greater than or equal to 10-6 as predicted by the model. 2. Verification Sampling--USG shall collect six additional vertically composited samples of sludge from locations that compliment historical data and shall analyze the samples by TCLP for metals including antimony, arsenic, barium, beryllium, cadmium, chromium, lead, mercury, nickel, selenium, silver, thallium, tin, vanadium, and zinc. If the samples exceed the levels in Condition (1)(a), USG must notify EPA. The corresponding sludge and all sludge yet to be disposed remains hazardous until USG has demonstrated by additional sampling that all constituents of concern are below the levels set forth in condition 1. [[Page 121]] 3. Reopener Language--(a) If, anytime after disposal of the delisted waste, USG possesses or is otherwise made aware of any data (including but not limited to leachate data or groundwater monitoring data) or any other data relevant to the delisted waste indicating that any constituent identified in Condition (1) is at a level higher than the delisting level established in Condition (1), or is at a level in the groundwater exceeding maximum allowable point of exposure concentration referenced by the model, then USG must report such data, in writing, to the Regional Administrator within 10 days of first possessing or being made aware of that data. (b) Based on the information described in paragraph (a) and any other information received from any source, the Regional Administrator will make a preliminary determination as to whether the reported information requires Agency action to protect human health or the environment. Further action may include suspending, or revoking the exclusion, or other appropriate response necessary to protect human health and the environment. (c) If the Regional Administrator determines that the reported information does require Agency action, the Regional Administrator will notify USG in writing of the actions the Regional Administrator believes are necessary to protect human health and the environment. The notice shall include a statement of the proposed action and a statement providing USG with an opportunity to present information as to why the proposed Agency action is not necessary or to suggest an alternative action. USG shall have 10 days from the date of the Regional Administrator's notice to present the information. (d) If after 10 days USG presents no further information, the Regional Administrator will issue a final written determination describing the Agency actions that are necessary to protect human health or the environment. Any required action described in the Regional Administrator's determination shall become effective immediately, unless the Regional Administrator provides otherwise. 4. Notifications--USG must provide a one-time written notification to any State Regulatory Agency to which or through which the waste described above will be transported for disposal at least 60 days prior to the commencement of such activities. Failure to provide such a notification will result in a violation of the delisting petition and a possible revocation of the decision. American Steel Scottsburg, IN... Wastewater treatment plant (WWTP) Cord. sludge from electroplating operations (EPA Hazardous Waste No. F006) generated at a maximum annual rate of 3,000 cubic yards per year, after January 26, 1999, and disposed of in a Subtitle D landfill. 1. Verification Testing: American Steel Cord must implement an annual testing program to demonstrate, based on the analysis of a minimum of four representative samples, that the constituent concentrations measured in the TCLP extract of the waste are within specific levels. The constituent concentrations must not exceed the following levels (mg/l) which are back-calculated from the delisting health-based levels and a DAF of 68. Arsenic--3.4; Barium--100; Cadmium--.34; Chromium--5; Copper--88.4.; Lead-- 1.02; Mercury--.136; Nickel-- 6.8.; Selenium--1; Silver--5; Zinc--680; Cyanide--13.6; Acetone--272; Benzo butyl phthlate--476; Chloroform--.68; 1,4-Dichlorobenzene--.272; cis- 1,2-Dichloroethene--27.2; Methylene chloride--.34; Naphthalene--68; Styrene--6.8; Tetrachloroethene--.34; Toluene-- 68; and Xylene--680. American Steel Cord must measure and record the pH of the waste using SW 846 method 9045 and must record all pH measurements performed in accordance with the TCLP. 2. Changes in Operating Conditions: If American Steel Cord significantly changes the manufacturing or treatment process or the chemicals used in the manufacturing or treatment process, American Steel Cord may handle the WWTP filter press sludge generated from the new process under this exclusion only after the facility has demonstrated that the waste meets the levels set forth in paragraph 1 and that no new hazardous constituents listed in Appendix VIII of Part 261 have been introduced. 3. Data Submittals: The data obtained through annual verification testing or compliance with paragraph 2 must be submitted to U.S. EPA Region 5, 77 W. Jackson Blvd., Chicago, IL 60604-3590, within 60 days of sampling. Records of operating conditions and analytical data must be compiled, summarized, and maintained on site for a minimum of five years and must be made available for inspection. All data must be accompanied by a signed copy of the certification statement in 260.22(I)(12). 4. (a) If, anytime after disposal of the delisted waste, American Steel Cord possesses or is otherwise made aware of any environmental data (including but not limited to leachate data or groundwater monitoring data) or any other data relevant to the delisted waste indicating that any constituent identified in Condition (1) is at a level in the leachate higher than the delisting level established in Condition (1), or is at a level in the ground water or soil higher than the health based level, then American Steel Cord must report such data, in writing, to the Regional Administrator within 10 days of first possessing or being made aware of that data. (b) Based on the information described in paragraph (a) and any other information received from any source, the Regional Administrator will make a preliminary determination as to whether the reported information requires Agency action to protect human health or the environment. Further action may include suspending, or revoking the exclusion, or other appropriate response necessary to protect human health and the environment. [[Page 122]] (c) If the Regional Administrator determines that the reported information does require Agency action, the Regional Administrator will notify the facility in writing of the actions the Regional Administrator believes are necessary to protect human health and the environment. The notice shall include a statement of the proposed action and a statement providing the facility with an opportunity to present information as to why the proposed Agency action is not necessary or to suggest an alternative action. The facility shall have 10 days from the date of the Regional Administrator's notice to present such information. (d) Following the receipt of information from the facility described in paragraph (c) or (if no information is presented under paragraph (c) the initial receipt of information described in paragraph (a), the Regional Administrator will issue a final written determination describing the Agency actions that are necessary to protect human health or the environment. Any required action described in the Regional Administrator's determination shall become effective immediately, unless the Regional Administrator provides otherwise. Ampex Recording Opelika, Alabama. Solvent recovery residues in the Media powder or pellet form (EPA Corporation. Hazardous Waste Nos. F003 and F005) generated from the recovery of spent solvents from the manufacture of tape recording media (generated at a maximum annual rate of 1,000 cubic yards in the powder or pellet form) after August 9, 1993. In order to confirm that the characteristics of the wastes do not change significantly, the facility must, on an annual basis, analyze a representative composite sample of the waste (in its final form) for the constituents listed in 40 CFR 261.24 using the method specified therein. The annual analytical results, including quality control information, must be compiled, certified according to 40 CFR 260.22(i)(12), maintained on-site for a minimum of five years, and made available for inspection upon request by any employee or representative of EPA or the State of Alabama. Failure to maintain the required records on-site will be considered by EPA, at its discretion, sufficient basis to revoke the exclusion to the extent directed by EPA. Aptus, Inc....... Coffeyville, Kiln residue and spray dryer/ Kansas. baghouse residue (EPA Hazardous Waste No. F027) generated during the treatment of cancelled pesticides containing 2,4,5-T and Silvex and related materials by Aptus' incinerator at Coffeyville, Kansas after December 27, 1991, so long as: (1) The incinerator is monitored continuously and is in compliance with operating permit conditions. Should the incinerator fail to comply with the permit conditions relevant to the mechanical operation of the incinerator, Aptus must test the residues generated during the run when the failure occurred according to the requirements of Conditions (2) through (4), regardless of whether or not the demonstration in Condition (5) has been made. (2) A minimum of four grab samples must be taken from each hopper (or other container) of kiln residue generated during each 24- hour run; all grabs collected during a given 24-hour run must then be composited to form one composite sample. A minimum of four grab samples must also be taken from each hopper (or other container) of spray dryer/ baghouse residue generated during each 24-hour run; all grabs collected during a given 24-hour run must then be composited to form one composite sample. Prior to the disposal of the residues from each 24-hour run, a TCLP leachate test must be performed on these composite samples and the leachate analyzed for the TC toxic metals, nickel, and cyanide. If arsenic, chromium, lead or silver TC leachate test results exceed 1.6 ppm, barium levels exceed 32 ppm, cadmium or selenium levels exceed 0.3 ppm, mercury levels exceed 0.07 ppm, nickel levels exceed 10 ppm, or cyanide levels exceed 6.5 ppm, the wastes must be retreated to achieve these levels or must be disposed in accordance with subtitle C of RCRA. Analyses must be performed according to appropriate methods. As applicable to the method-defined parameters of concern, analyses requiring use of SW-846 methods incorporated by reference in 40 CFR 260.11 must be used without substitution. As applicable, the SW-846 methods might include Methods 0010, 0011, 0020, 0023A, 0030, 0031, 0040, 0050, 0051, 0060, 0061, 1010A, 1020B, 1110A, 1310B, 1311, 1312, 1320, 1330A, 9010C, 9012B, 9040C, 9045D, 9060A, 9070A (uses EPA Method 1664, Rev. A), 9071B, and 9095B. (3) Aptus must generate, prior to the disposal of the residues, verification data from each 24 hour run for each treatment residue (i.e., kiln residue, spray dryer/baghouse residue) to demonstrate that the maximum allowable treatment residue concentrations listed below are not exceeded. Samples must be collected as specified in Condition (2). Analyses must be performed according to appropriate methods. As applicable to the method-defined parameters of concern, analyses requiring the use of SW-846 methods incorporated by reference in 40 CFR 260.11 must be used without substitution. As applicable, the SW-846 methods might include Methods 0010, 0011, 0020, 0023A, 0030, 0031, 0040, 0050, 0051, 0060, 0061, 1010A, 1020B, 1110A, 1310B, 1311, 1312, 1320, 1330A, 9010C, 9012B, 9040C, 9045D, 9060A, 9070A (uses EPA Method 1664, Rev. A), 9071B, and 9095B. Any residues which exceed any of the levels listed below must be retreated or must be disposed of as hazardous. Kiln residue and spray dryer/baghouse residue must not exceed the following levels: [[Page 123]] Aldrin--0.015 ppm, Benzene--9.7 ppm, Benzo(a)pyrene--0.43 ppm, Benzo(b)fluoranthene)--1.8 ppm, Chlordane--0.37 ppm, Chloroform-- 5.4 ppm, Chrysene--170 ppm, Dibenz(a,h)anthracene--0.083 ppm, 1.2-Dichloroethane--4.1 ppm, Dichloromethane--2.4 ppm, 2,4- Dichlorophenol--480 ppm, Dichlorvos--260 ppm, Disulfaton-- 23 ppm, Endosulfan I--310 ppm, Fluorene--120 ppm, Indeno(1,2,3,cd)-pyrene--330 ppm, Methyl parathion--210 ppm, Nitrosodiphenylamine--130 ppm, Phenanthrene--150 ppm, Polychlorinated biphenyls--0.31 ppm, Tetrachlorethylene--59 ppm, 2,4,5-TP (silvex)--110 ppm, 2,4,6- Trichlorophenol--3.9 ppm. (4) Aptus must generate, prior to disposal of residues, verification data from each 24- hour run for each treatment residue (i.e., kiln residue, spray dryer/baghouse residue) to demonstrate that the residues do not contain tetra-, penta-, or hexachlorodibenzo-p-dioxins or furans at levels of regulatory concern. Samples must be collected as specified in Condition (2). The TCDD equivalent levels for the solid residues must be less than 5 ppt. Any residues with detected dioxins or furans in excess of this level must be retreated or must be disposed of as acutely hazardous. For tetra- and penta- chlorinated dioxin and furan homologs, the maximum practical quantitation limit must not exceed 15 ppt for the solid residues. For hexachlorinated dioxin and furan homologs, the maximum practical quantitation limit must not exceed 37 ppt for the solid residues. (5) The test data from Conditions (1), (2), (3), and (4) must be kept on file by Aptus for inspection purposes and must be compiled, summarized, and submitted to the Director for the Characterization and Assessment Division, Office of Solid Waste, by certified mail on a monthly basis and when the treatment of the cancelled pesticides and related materials is concluded. The testing requirements for Conditions (2), (3), and (4) will continue until Aptus provides the Director with the results of four consecutive batch analyses for the petitioned wastes, none of which exceed the maximum allowable levels listed in these conditions and the director notifies Aptus that the conditions have been lifted. All data submitted will be placed in the RCRA public docket. (6) Aptus must provide a signed copy of the following certification statement when submitting data in response to the conditions listed above: ``Under civil and criminal penalty of law for the making or submission of false or fraudulent statements or representations, I certify that the information contained in or accompanying this document is true, accurate, and complete. As to the (those) identified section(s) of this document for which I cannot personally verify its (their) truth and accuracy, I certify as the company official having supervisory responsibility for the persons who, acting under my direct instructions, made the verification that this information is true, accurate, and complete.'' Arco Building Sugarcreek, Ohio. Dewatered wastewater treatment Products. sludge (EPA Hazardous Waste No. F019) generated from the chemical conversion coating of aluminum after August 15, 1986. Arco Chemical Co. Miami, FL........ Dewatered wastewater treatment sludge (EPA Hazardous Waste No. FO19) generated from the chemical conversion coating of aluminum after April 29, 1986. Arkansas Vertac Superfund Kiln ash, cyclone ash, and calcium Department of site, chloride salts from incineration Pollution Jacksonville, of residues (EPA Hazardous Waste Control and Arkansas. No. F020 and F023) generated from Ecology. the primary production of 2,4,5-T and 2,4-D after August 24, 1990. This one-time exclusion applies only to the incineration of the waste materials described in the petition, and it is conditional upon the data obtained from ADPC&E's full-scale incineration facility. To ensure that hazardous constituents are not present in the waste at levels of regulatory concern once the full- scale treatment facility is in operation, ADPC&E must implement a testing program for the petitioned waste. This testing program must meet the following conditions for the exclusion to be valid: (1) Testing: Sample collection and analyses (including quality control (QC) procedures) must be performed according to appropriate methods. As applicable to the method-defined parameters of concern, analyses requiring the use of SW-846 methods incorporated by reference in 40 CFR 260.11 must be used without substitution. As applicable, the SW-846 methods might include Methods 0010, 0011, 0020, 0023A, 0030, 0031, 0040, 0050, 0051, 0060, 0061, 1010A, 1020B, 1110A, 1310B, 1311, 1312, 1320, 1330A, 9010C, 9012B, 9040C, 9045D, 9060A, 9070A (uses EPA Method 1664, Rev. A), 9071B, and 9095B. [[Page 124]] (A) Initial testing: Representative grab samples must be taken from each drum and kiln ash and cyclone ash generated from each 24 hours of operation, and the grab samples composited to form one composite sample of ash for each 24-hour period. Representative grab samples must also be taken from each drum of calcium chloride salts generated from each 24 hours of operation and composited to form one composite sample of calcium chloride salts for each 24- hour period. The initial testing requirements must be fullfilled for the following wastes: (i) Incineration by- products generated prior to and during the incinerator's trial burn; (ii) incineration by-products from the treatment of 2,4-D wastes for one week (or 7 days if incineration is not on consecutive days) after completion of the trial burn; (iii) incineration by- products from the treatment of blended 2,4-D and 2,4, 5- T wastes for two weeks (or 14 days if incineration is not on consecutive days) after completion of the trial burn; and (iv) incineration by-products from the treatment of blended 2,4-D and 2,4,5-T wastes for one week (or 7 days if incineration is not on consecutive days) when the percentage of 2, 4, 5-T wastes exceeds the maximum percentage treated under Condition (1)(A)(iii). Prior to disposal of the residues from each 24-hour sampling period, the daily composite must be analyzed for all the constituents listed in Condition (3). ADPC&E must report the analytical test data, including quality control information, obtained during this initial period no later than 90 days after the start of the operation. (B) Subsequent testing: Representative grab samples of each drum of kiln and cyclone ash generated from each week of operation must be composited to form one composite sample of ash for each weekly period. Representative grab samples of each drum of calcium chloride salts generated from each week of operation must also be composited to form one composite sample of calcium chloride salts for each weekly period. Prior to disposal of the residues from each weekly sampling period, the weekly composites must be analyzed for all of the constituents listed in Condition (3). The analytical data, including quality control information, must be compiled and maintained on site for a minimum of three years. These data must be furnished upon request and made available for inspection by any employee or representative of EPA. (2) Waste holding: The incineration residues that are generated must be stored as hazardous until the initial verification analyses or subsequent analyses are completed. If the composite incineration residue samples (from either Condition (1)(A) or Condition (1)(B)) do not exceed any of the delisting levels set in Condition (3), the incineration residues corresponding to these samples may be managed and disposed of in accordance with all applicable solid waste regulations. If any composite incineration residue sample exceeds any of the delisting levels set in Condition (3), the incineration residues generated during the time period corresponding to this sample must be retreated until they meet these levels (analyses must be repeated) or managed and disposed of in accordance with subtitle C of RCRA. Incineration residues which are generated but for which analysis is not complete or valid must be managed and disposed of in accordance with subtitle C of RCRA, until valid analyses demonstrate that the wastes meet the delisting levels. (3) Delisting levels: If concentrations in one or more of the incineration residues for any of the hazardous constituents listed below exceed their respective maximum allowable concentrations also listed below, the batch of failing waste must either be re- treated until it meets these levels or managed and disposed of in accordance with subtitle C of RCRA. (A) Inorganics (Leachable): Arsenic, 0.32 ppm; Barium, 6.3 ppm; Cadmium, 0.06 ppm; Chromium, 0.32 ppm; Cyanide, 4.4 ppm; Lead, 0.32 ppm; Mercury, 0.01 ppm; Nickel, 4.4 ppm; Selenium, 0.06 ppm; Silver, 0.32 ppm. Metal concentrations must be measured in the waste leachate as per 40 CFR 261.24. Cyanide extractions must be conducted using distilled water. (B) Organics: Benzene, 0.87 ppm; Benzo(a)anthracene, 0.10 ppm; Benzo(a)pyrene, 0.04 ppm; Benzo (b)fluoranthene, 0.16 ppm; Chlorobenzene, 152 ppm; o- Chlorophenol, 44 ppm; Chrysene, 15 ppm; 2, 4-D, 107 ppm; DDE, 1.0 ppm; Dibenz(a,h)anthracene, 0.007 ppm; 1, 4-Dichlorobenzene, 265 ppm; 1, 1- Dichloroethylene, 1.3 ppm; trans-1,2-Dichloroethylene, 37 ppm; Dichloromethane, 0.23 ppm; 2,4- Dichlorophenol, 43 ppm; Hexachlorobenzene, 0.26 ppm; Indeno (1,2,3-cd) pyrene, 30 ppm; Polychlorinated biphenyls, 12 ppm; 2,4,5-T, 1 x 10\6\ ppm; 1,2,4,5- Tetrachlorobenzene, 56 ppm; Tetrachloroethylene, 3.4 ppm; Trichloroethylene, 1.1 ppm; 2,4,5-Trichlorophenol, 21,000 ppm; 2,4,6- Trichlorophenol, 0.35 ppm. [[Page 125]] (C) Chlorinated dioxins and furans: 2,3,7,8- Tetrachlorodibenzo-p-dioxin equivalents, 4 x 10-7 ppm. The petitioned by-product must be analyzed for the tetra-, penta-, hexa-, and heptachlorodibenzo-p- dioxins, and the tetra-, penta-, hexa-, and heptachlorodibenzofurans to determine the 2, 3, 7, 8- tetra-chlorodibenzo-p-dioxin equivalent concentration. The analysis must be conducted using a measurement system that achieves practical quantitation limits of 15 parts per trillion (ppt) for the tetra- and penta- homologs, and 37 ppt for the hexa- and hepta-homologs. (4) Termination of testing: Due to the possible variability of the incinerator feeds, the testing requirements of Condition (1)(B) will continue indefinitely. (5) Data submittals: Within one week of system start-up, ADPC&E must notify the Section Chief, Variances Section (see address below) when the full- scale incineration system is on-line and waste treatment has begun. The data obtained through Condition (1)(A) must be submitted to PSPD/OSW (5303W), U.S. EPA, 1200 Pennsylvania Ave., NW., Washington, DC 20460, within the time period specified. At the Section Chief's request, ADPC&E must submit analytical data obtained through Condition (1)(B) within the time period specified by the Section Chief. Failure to submit the required data obtained from Condition (1)(A) within the specified time period or to maintain the required records for the time specified in Condition (1)(B) (or to submit data within the time specified by the Section Chief) will be considered by the Agency, at its discretion, sufficient basis to revoke ADPC&E's exclusion to the extent directed by EPA. All data must be accompanied by the following certification statement: ``Under civil and criminal penalty of law for the making or submission of false or fraudulent statements or representations (pursuant to the applicable provisions of the Federal Code, which include, but may not be limited to, 18 U.S.C. 1001 and 42 U.S.C. 6928), I certify that the information contained in or accompanying this document is true, accurate and complete. As to the (those) identified section(s) of this document for which I cannot personally verify its (their) truth and accuracy, I certify as the company official having supervisory responsibility for the persons who, acting under my direct instructions, made the verification that this information is true, accurate and complete. In the event that any of this information is determined by EPA in its sole discretion to be false, inaccurate or incomplete, and upon conveyance of this fact to the company, I recognize and agree that this exclusion of wastes will be void as if it never had effect or to the extent directed by EPA and that the company will be liable for any actions taken in contravention of the company's RCRA and CERCLA obligations premised upon the company's reliance on the void exclusion.'' AutoAlliance Flat Rock, Wastewater treatment sludges, International Michigan. F019, that are generated by Inc.. AutoAlliance International, Inc. (AAI) at Flat Rock, Michigan at a maximum annual rate of 2,000 cubic yards per year. The sludges must be disposed of in a lined landfill with leachate collection which is licensed, permitted, or otherwise authorized to accept the delisted wastewater treatment sludges in accordance with 40 CFR part 258. The exclusion becomes effective as of April 6, 2007. (1) Delisting Levels: (A) The concentrations in a leachate extract of the waste measured in any sample must not exceed the following levels (mg/L): arsenic-- 0.3; cadmium--0.5; chromium-- 4.95; lead--5; nickel--90.5; selenium--1; tin--721; zinc--898; p-cresol--11.4; and formaldehyde-- 84.2. ................. (B) The total concentration measured in any sample must not exceed the following levels (mg/ kg): mercury--8.92; and formaldehyde--689. (2) Quarterly Verification Testing: To verify that the waste does not exceed the specified delisting levels, AAI must collect and analyze one representative sample of the waste on a quarterly basis. Sample collection and analyses, including quality control procedures, must be performed using appropriate methods. SW-846 Method 1311 must be used for generation of the leachate extract used in the testing of the delisting levels if oil and grease comprise less than 1% of the waste. SW-846 Method 1330A must be used for generation of the leaching extract if oil and grease comprise 1% or more of the waste. SW-846 Method 9071B must be used for determination of oil and grease. SW-846 Methods 1311, 1330A, and 9071B are incorporated by reference in 40 CFR 260.11. (3) Changes in Operating Conditions: AAI must notify the EPA in writing if the manufacturing process, the chemicals used in the manufacturing process, the treatment process, or the chemicals used in the treatment process change significantly. AAI must handle wastes generated after the process change as hazardous until it has demonstrated that the wastes continue to meet the delisting levels and that no new hazardous constituents listed in Appendix VIII of part 261 have been introduced and it has received written approval from EPA. (4) Data Submittals: AAI must submit the data obtained through verification testing or as required by other conditions of this rule to both U.S. EPA Region 5, 77 W. Jackson Blvd., Chicago, IL 60604 and MDEQ, Waste and Hazardous Materials Division, Hazardous Waste Section, at P.O. Box 30241, Lansing, Michigan 48909. The quarterly verification data and certification of proper disposal must be submitted annually upon the anniversary of the effective date of this exclusion. AAI must compile, summarize and maintain on site for a minimum of five years records of operating conditions and analytical data. AAI must make these records available for inspection. A signed copy of the certification statement in 40 CFR 260.22(i)(12) must accompany all data. [[Page 126]] (5) Reopener Language: (A) If, anytime after disposal of the delisted waste AAI possesses or is otherwise made aware of any data (including but not limited to leachate data or groundwater monitoring data) relevant to the delisted waste indicating that any constituent is at a level in the leachate higher than the specified delisting level, or is in the groundwater at a concentration higher than the maximum allowable groundwater concentration in paragraph (e), then AAI must report such data, in writing, to the Regional Administrator within 10 days of first possessing or being made aware of that data. (B) Based on the information described in paragraph (a) and any other information received from any source, the Regional Administrator will make a preliminary determination as to whether the reported information requires Agency action to protect human health or the environment. Further action may include suspending, or revoking the exclusion, or other appropriate response necessary to protect human health and the environment. (C) If the Regional Administrator determines that the reported information does require Agency action, the Regional Administrator will inform AAI in writing of the actions the Regional Administrator believes are necessary to protect human health and the environment. The notice shall include a statement of the proposed action and a statement providing AAI with an opportunity to present information as to why the proposed Agency action is not necessary or to suggest an alternative action. AAI shall have 30 days from the date of the Regional Administrator's notice to present the information. (D) If after 30 days AAI presents no further information, the Regional Administrator will issue a final written determination describing the Agency actions that are necessary to protect human health or the environment. Any required action described in the Regional Administrator's determination shall become effective immediately, unless the Regional Administrator provides otherwise. (E) Maximum Allowable Groundwater Concentrations ([micro]g/L): arsenic--5; cadmium--5; chromium-- 100; lead--15; nickel--750; selenium--50; tin--22,500; zinc-- 11,300; p-cresol--188; and formaldehyde--1,380. BBC Brown Boveri, Sanford, FL...... Dewatered Wastewater treatment Inc.. sludges (EPA Hazardous Waste No. F006) generated from electroplating operations after October 17, 1986. Bekaert Corp..... Dyersburg, TN.... Dewatered wastewater treatment plant (WWTP) sludge (EPA Hazardous Waste Nos. F006) generated at a maximum rate of 1250 cubic yards per calendar year after May 27, 2004, and disposed in a Subtitle D landfill. For the exclusion to be valid, Bekaert must implement a verification testing program that meets the following paragraphs: (1) Delisting Levels: All leachable concentrations for those constituents must not exceed the maximum allowable concentrations in mg/l specified in this paragraph. Bekaert must use the leaching method specified at 40 CFR 261.24 to measure constituents in the waste leachate. (A) Inorganic Constituents TCLP (mg/l): Cadmium--0.672; Chromium-- 5.0; Nickel--127; Zinc--1260.0. (B) Organic Constituents TCLP (mg/ l): Methyl ethyl ketone--200.0. (2) Waste Holding and Handling: (A) Bekaert must accumulate the hazardous waste dewatered WWTP sludge in accordance with the applicable regulations of 40 CFR 262.34 and continue to dispose of the dewatered WWTP sludge as hazardous waste. (B) Once the first quarterly sampling and analyses event described in paragraph (3) is completed and valid analyses demonstrate that no constituent is present in the sample at a level which exceeds the delisting levels set in paragraph (1), Bekaert can manage and dispose of the dewatered WWTP sludge as nonhazardous according to all applicable solid waste regulations. (C) If constituent levels in any sample taken by Bekaert exceed any of the delisting levels set in paragraph (1), Bekaert must do the following: (i) notify EPA in accordance with paragraph (7) and (ii) manage and dispose the dewatered WWTP sludge as hazardous waste generated under Subtitle C of RCRA. (D) Quarterly Verification Testing Requirements: Upon this exclusion becoming final, Bekaert may begin the quarterly testing requirements of paragraph (3) on its dewatered WWTP sludge. (3) Quarterly Testing Requirements: Upon this exclusion becoming final, Bekaert may perform quarterly analytical testing by sampling and analyzing the dewatered WWTP sludge as follows: (A)(i) Collect four representative composite samples of the hazardous waste dewatered WWTP sludge at quarterly (ninety (90) day) intervals after EPA grants the final exclusion. The first composite sample may be taken at any time after EPA grants the final approval. (ii) Analyze the samples for all constituents listed in paragraph (1). Any roll-offs from which the composite sample is taken exceeding the delisting levels listed in paragraph (1) must be disposed as hazardous waste in a Subtitle C landfill. (iii) Within forty-five (45) days after taking its first quarterly sample, Bekaert will report its first quarterly analytical test data to EPA. If levels of constituents measured in the sample of the dewatered WWTP sludge do not exceed the levels set forth in paragraph (1) of this exclusion, Bekaert can manage and dispose the nonhazardous dewatered WWTP sludge according to all applicable solid waste regulations. (4) Annual Testing: [[Page 127]] (A) If Bekaert completes the quarterly testing specified in paragraph (3) above and no sample contains a constituent with a level which exceeds the limits set forth in paragraph (1), Bekaert may begin annual testing as follows: Bekaert must test one representative composite sample of the dewatered WWTP sludge for all constituents listed in paragraph (1) at least once per calendar year. (B) The sample for the annual testing shall be a representative composite sample for all constituents listed in paragraph (1). (C) The sample for the annual testing taken for the second and subsequent annual testing events shall be taken within the same calendar month as the first annual sample taken. (5) Changes in Operating Conditions: If Bekaert significantly changes the process described in its petition or starts any processes that generate(s) the waste that may or could affect the composition or type of waste generated as established under paragraph (1) (by illustration, but not limitation, changes in equipment or operating conditions of the treatment process), it must notify the EPA in writing; it may no longer handle the wastes generated from the new process as nonhazardous until the wastes meet the delisting levels set in paragraph (1) and it has received written approval to do so from the EPA. (6) Data Submittals: Bekaert must submit the information described below. If Bekaert fails to submit the required data within the specified time or maintain the required records on-site for the specified time, the EPA, at its discretion, will consider this sufficient basis to reopen the exclusion as described in paragraph (7). Bekaert must: (A) Submit the data obtained through paragraph (3) to the Chief, North Section, RCRA Enforcement and Compliance Branch, Waste Division, U. S. Environmental Protection Agency Region 4, 61 Forsyth Street, SW., Atlanta, Georgia, 30303, within the time specified. (B) Compile records of analytical data from paragraph (3), summarized, and maintained on- site for a minimum of five years. (C) Furnish these records and data when either the EPA or the State of Tennessee request them for inspection. (D) Send along with all data a signed copy of the following certification statement, to attest to the truth and accuracy of the data submitted: ``Under civil and criminal penalty of law for the making or submission of false or fraudulent statements or representations (pursuant to the applicable provisions of the Federal Code, which include, but may not be limited to, 18 U.S.C. 1001 and 42 U.S.C. 6928), I certify that the information contained in or accompanying this document is true, accurate and complete. As to the (those) identified section(s) of this document for which I cannot personally verify its (their) truth and accuracy, I certify as the company official having supervisory responsibility for the persons who, acting under my direct instructions, made the verification that this information is true, accurate and complete. If any of this information is determined by the EPA in its sole discretion to be false, inaccurate or incomplete, and upon conveyance of this fact to the company, I recognize and agree that this exclusion of waste will be void as if it never had effect or to the extent directed by the EPA and that the company will be liable for any actions taken in contravention of the company's RCRA and CERCLA obligations premised upon the company's reliance on the void exclusion.'' (7) Reopener: (A) If, anytime after disposal of the delisted waste Bekaert possesses or is otherwise made aware of any environmental data (including but not limited to leachate data or ground water monitoring data) or any other data relevant to the delisted waste indicating that any constituent identified for the delisting verification testing is at level higher than the delisting level allowed by the Regional Administrator or his delegate in granting the petition, then the facility must report the data, in writing, to the Regional Administrator or his delegate within ten (10) days of first possessing or being made aware of that data. (B) If either the quarterly or annual testing of the waste does not meet the delisting requirements in paragraph (1), Bekaert must report the data, in writing, to the Regional Administrator or his delegate within ten (10) days of first possessing or being made aware of that data. (C) If Bekaert fails to submit the information described in paragraphs (5), (6)(A) or (6)(B) or if any other information is received from any source, the Regional Administrator or his delegate will make a preliminary determination as to whether the reported information requires the EPA action to protect human health or the environment. Further action may include suspending, or revoking the exclusion, or other appropriate response necessary to protect human health and the environment. (D) If the Regional Administrator or his delegate determines that the reported information requires action the EPA, the Regional Administrator or his delegate will notify the facility in writing of the actions the Regional Administrator or his delegate believes are necessary to protect human health and the environment. The notification shall include a statement of the proposed action and a statement providing the facility with an opportunity to present information as to why the proposed the EPA action is not necessary. The facility shall have ten (10) days from the date of the Regional Administrator or his delegate's notice to present such information. [[Page 128]] (E) Following the receipt of information from the facility described in paragraph (6)(D) or (if no information is presented under paragraph (6)(D)) the initial receipt of information described in paragraphs (5), (6)(A) or (6)(B), the Regional Administrator or his delegate will issue a final written determination describing the EPA actions that are necessary to protect human health or the environment. Any required action described in the Regional Administrator or his delegate's determination shall become effective immediately, unless the Regional Administrator or his delegate provides otherwise. (8) Notification Requirements: Bekaert must do following before transporting the delisted waste: (A) Provide a one-time written notification to any State Regulatory Agency to which or through which it will transport the delisted waste described above for disposal, sixty (60) days before beginning such activities. (B) Update the one-time written notification if Bekaert ships the delisted waste into a different disposal facility. (C) Failure to provide this notification will result in a violation of the delisting variance and a possible revocation of the decision. Bethlehem Steel Sparrows Point, Stabilized filter cake (at a Corporation. Maryland. maximum annual rate of 1100 cubic yards) from the treatment of wastewater treatment sludges (EPA Hazardous Waste No. F006) generated from electroplating operations after [insert date of publication in Federal Register]. Bethlehem Steel (BSC) must implement a testing program that meets the following conditions for the exclusion to be valid: (1) Testing: Sample collection and analyses (including quality control (QC) procedures) must be performed using appropriate methods. As applicable to the method-defined parameters of concern, analyses requiring the use of SW-846 methods incorporated by reference in 40 CFR 260.11 must be used without substitution. As applicable, the SW-846 methods might include Methods 0010, 0011, 0020, 0023A, 0030, 0031, 0040, 0050, 0051, 0060, 0061, 1010A, 1020B, 1110A, 1310B, 1311, 1312, 1320, 1330A, 9010C, 9012B, 9040C, 9045D, 9060A, 9070A (uses EPA Method 1664, Rev. A), 9071B, and 9095B. If EPA judges the stabilization process to be effective under the conditions used during the initial verification testing, BSC may replace the testing required in Condition (1)(A) with the testing required in Condition (1)(B). BSC must continue to test as specified in Condition (1)(A) until and unless notified by EPA in writing that testing in Condition (1)(A) may be replaced by Condition (1)(B) (to the extent directed by EPA). (A) Initial Verification Testing: During at least the first eight weeks of operation of the full- scale treatment system, BSC must collect and analyze weekly composites representative of the stabilized waste. Weekly composites must be composed of representative grab samples collected from every batch during each week of stabilization. The composite samples must be collected and analyzed, prior to the disposal of the stabilized filter cake, for all constituents listed in Condition (3). BSC must report the analytical test data, including a record of the ratios of lime kiln dust and fly ash used and quality control information, obtained during this initial period no later than 60 days after the collection of the last composite of stabilized filter cake. (B) Subsequent Verification Testing: Following written notification by EPA, BSC may substitute the testing condition in (1)(B) for (1)(A). BSC must collect and analyze at least one composite representative of the stabilized filter cake generated each month. Monthly composites must be comprised of representative samples collected from all batches that are stabilized in a one-month period. The monthly samples must be analyzed prior to the disposal of the stabilized filter cake for chromium, lead and nickel. BSC may, at its discretion, analyze composite samples more frequently to demonstrate that smaller batches of waste are non- hazardous. (C) Annual Verification Testing: In order to confirm that the characteristics of the treated waste do not change significantly, BSC must, on an annual basis, analyze a representative composite sample of stabilized filter cake for all TC constituents listed in 40 CFR Sec. 261.24 using the method specified therein. This composite sample must represent the stabilized filter cake generated over one week. (2) Waste Holding and Handling: BSC must store, as hazardous, all stabilized filter cake generated until verification testing (as specified in Conditions (1)(A) and (1)(B)) is completed and valid analyses demonstrate that the delisting levels set forth in Condition (3) are met. If the levels of hazardous constituents measured in the samples of stabilized filter cake generated are below all the levels set forth in Condition (3), then the stabilized filter cake is non- hazardous and may be managed and disposed of in accordance with all applicable solid waste regulations. If hazardous constituent levels in any weekly or monthly composite sample equal or exceed any of the delisting levels set in Condition (3), the stabilized filter cake generated during the time period corresponding to this sample must be retreated until it is below these levels or managed and disposed of in accordance with Subtitle C of RCRA. (3) Delisting Levels: All concentrations must be measured in the waste leachate by the method specified in 40 CFR Sec. 261.24. The leachable concentrations for the constituents must be below the following levels (ppm): arsenic-- 4.8; barium--100; cadmium--0.48; chromium--5.0; lead--1.4; mercury--0.19; nickel--9.6; selenium--1.0; silver--5.0. [[Page 129]] (4) Changes in Operating Conditions: After completing the initial verification test period in Condition (1)(A), if BSC decides to significantly change the stabilization process (e.g., stabilization reagents) developed under Condition (1), then BSC must notify EPA in writing prior to instituting the change. After written approval by EPA, BSC may manage waste generated from the changed process as non-hazardous under this exclusion, provided the other conditions of this exclusion are fulfilled. (5) Data Submittals: Two weeks prior to system start-up, BSC must notify in writing (see address below) when stabilization of the dewatered filter cake will begin. The data obtained through Condition (1)(A) must be submitted to Waste and Chemicals Management Division (Mail Code 3HW11), U.S. EPA Region III, 1650 Arch St., Philadelphia, PA 19103 within the time period specified. The analytical data, including quality control information and records of ratios of lime kiln dust and fly ash used, must be compiled and maintained on site for a minimum of five years. These data must be furnished upon request and made available for inspection by EPA or the State of Maryland. Failure to submit the required data within the specified time period or maintain the required records on site for the specified time will be considered by the Agency, at its discretion, sufficient basis to revoke the exclusion to the extent directed by EPA. All data must be accompanied by a signed copy of the following certification statement to attest to the truth and accuracy of the data submitted: ``Under civil and criminal penalty of law for the making or submission of false or fraudulent statements or representations (pursuant to the applicable provisions of the Federal Code, which include, but may not be limited to, 18 U.S.C Sec. 1001 and 42 U.S.C Sec. 6928), I certify that the information contained in or accompanying this document is true, accurate and complete. As to the (those) identified section(s) of this document for which I cannot personally verify its (their) truth and accuracy, I certify as the company official having supervisory responsibility for the persons who, acting under my direct instructions, made the verification that this information is true, accurate and complete. In the event that any of this information is determined by EPA in its sole discretion to be false, inaccurate or incomplete, and upon conveyance of this fact to the company, I recognize and agree that this exclusion of waste will be void as if it never had effect or to the extent directed by EPA and that the company will be liable for any actions taken in contravention of the company's RCRA and CERCLA obligations premised upon the company's reliance on the void exclusion.'' BMW Manufacturing Greer, South Wastewater treatment sludge (EPA Co., LLC. Carolina. Hazardous Waste No. F019) that BMW Manufacturing Corporation (BMW) generates by treating wastewater from automobile assembly plant located on Highway 101 South in Greer, South Carolina. This is a conditional exclusion for up to 2,850 cubic yards of waste (hereinafter referred to as ``BMW Sludge'') that will be generated each year and disposed in a Subtitle D landfill after August 31, 2005. With prior approval by the EPA, following a public comment period, BMW may also beneficially reuse the sludge. BMW must demonstrate that the following conditions are met for the exclusion to be valid. (1) Delisting Levels: All leachable concentrations for these metals and cyanide must not exceed the following levels (ppm): Barium-100; Cadmium-1; Chromium-5; Cyanide-33.6, Lead-5; and Nickel-70.3. These metal and cyanide concentrations must be measured in the waste leachate obtained by the method specified in 40 CFR 261.24, except that for cyanide, deionized water must be the leaching medium. Cyanide concentrations in waste or leachate must be measured by the method specified in 40 CFR 268.40, Note 7. (2) Annual Verification Testing Requirements: Sample collection and analyses, including quality control procedures, must be performed using appropriate methods. As applicable to the method-defined parameters of concern, analyses requiring the use of SW-846 methods incorporated by reference in 40 CFR 260.11 must be used without substitution. As applicable, the SW-846 methods might include Methods 0010, 0011, 0020, 0023A, 0030, 0031, 0040, 0050, 0051, 0060, 0061, 1010A, 1020B, 1110A, 1310B, 1311, 1312, 1320, 1330A, 9010C, 9012B, 9040C, 9045D, 9060A, 9070A, (uses EPA Method 1664, Rev. A), 9071B, and 9095B. Methods must meet Performance Based Measurement System Criteria in which the Data Quality Objectives are to demonstrate that representative samples of the BMW Sludge meet the delisting levels in Condition (1). (A) Annual Verification Testing: BMW must implement an annual testing program to demonstrate that constituent concentrations measured in the TCLP extract do not exceed the delisting levels established in Condition (1). (3) Waste Holding and Handling: BMW must hold sludge containers utilized for verification sampling until composite sample results are obtained. If the levels of constituents measured in the composite samples of BMW Sludge do not exceed the levels set forth in Condition (1), then the BMW Sludge is non-hazardous and must be managed in accordance with all applicable solid waste regulations. If constituent levels in a composite sample exceed any of the delisting levels set forth in Condition (1), the batch of BMW Sludge generated during the time period corresponding to this sample must be managed and disposed of in accordance with Subtitle C of RCRA. [[Page 130]] (4) Changes in Operating Conditions: BMW must notify EPA in writing when significant changes in the manufacturing or wastewater treatment processes are implemented. EPA will determine whether these changes will result in additional constituents of concern. If so, EPA will notify BMW in writing that the BMW Sludge must be managed as hazardous waste F019 until BMW has demonstrated that the wastes meet the delisting levels set forth in Condition (1) and any levels established by EPA for the additional constituents of concern, and BMW has received written approval from EPA. If EPA determines that the changes do not result in additional constituents of concern, EPA will notify BMW, in writing, that BMW must verify that the BMW Sludge continues to meet Condition (1) delisting levels. (5) Data Retention: Records of analytical data from Condition (2) must be compiled, summarized, and maintained by BMW for a minimum of three years, and must be furnished upon request by EPA or the State of South Carolina, and made available for inspection. Failure to maintain the required records for the specified time will be considered by EPA, at its discretion, sufficient basis to revoke the exclusion to the extent directed by EPA. All data must be accompanied by a signed copy of the certification statement in 40 CFR 260.22(i)(12). (6) Reopener Language: (A) If, at any time after disposal of the delisted waste, BMW possesses or is otherwise made aware of any environmental data (including but not limited to leachate data or groundwater monitoring data) or any other data relevant to the delisted waste indicating that any constituent identified in the delisting verification testing is at a level higher than the delisting level allowed by EPA in granting the petition, BMW must report the data, in writing, to EPA and South Carolina within 10 days of first possessing or being made aware of that data. (B) If the testing of the waste, as required by Condition (2)(A), does not meet the delisting requirements of Condition (1), BMW must report the data, in writing, to EPA and South Carolina within 10 days of first possessing or being made aware of that data. (C) Based on the information described in paragraphs (6)(A) or (6)(B) and any other information received from any source, EPA will make a preliminary determination as to whether the reported information requires that EPA take action to protect human health or the environment. Further action may include suspending or revoking the exclusion, or other appropriate response necessary to protect human health and the environment. (D) If EPA determines that the reported information does require Agency action, EPA will notify the facility in writing of the action believed necessary to protect human health and the environment. The notice shall include a statement of the proposed action and a statement providing BMW with an opportunity to present information as to why the proposed action is not necessary. BMW shall have 10 days from the date of EPA's notice to present such information. (E) Following the receipt of information from BMW, as described in paragraph (6)(D), or if no such information is received within 10 days, EPA will issue a final written determination describing the Agency actions that are necessary to protect human health or the environment, given the information received in accordance with paragraphs (6)(A) or (6)(B). Any required action described in EPA's determination shall become effective immediately, unless EPA provides otherwise. (7) Notification Requirements: BMW must provide a one-time written notification to any State Regulatory Agency in a State to which or through which the delisted waste described above will be transported, at least 60 days prior to the commencement of such activities. Failure to provide such a notification will result in a violation of the delisting conditions and a possible revocation of the decision to delist. Boeing Commercial Auburn, Residually contaminated soils in Airplane Co.. Washington. an inactive sludge pile containment area on March 27, 1990, previously used to store wastewater treatment sludges generated from electroplating operations (EPA Hazardous Waste No. F006). Bommer Industries Landrum, SC...... Wastewater treatment sludges (EPA Inc.. Hazardous Waste No. F006) generated from their electroplating operations and contained in evaporation ponds 1 and 2 on August 12, 1987. BWX] Technologies Lynchburg, VA.... Wastewater treatment sludge from electroplating operations (EPA Hazardous Waste No. F006) generated at a maximum annual rate of 500 cubic yards per year, after January 14, 2000, and disposed of in a Subtitle D landfill. BWX Technologies must meet the following conditions for the exclusion to be valid: (1) Delisting Levels: All leachable concentrations for the following constituents measure using the SW-846 method 1311 (the TCLP) must not exceed the following levels (mg/l). (a) Inorganic constituents--Antimony- 0.6; Arsenic-5.0; Barium-100; Beryllium-0.4; Cadmium-0.5; Chromium-5.0; Cobalt-210; Copper- 130; Lead-1.5; Mercury-0.2; Nickel-70; Silver-5.0; Thallium- 0.2; Tin-2100; Zinc-1000; Fluoride-400. (b) Organic constituents--Acetone-400; Methylene Chloride-0.5. (2) Verification testing schedule: BWX Technologies must analyze a representative sample of the filter cake from the pickle acid treatment system on an annual, calendar year basis using methods with appropriate detection levels and quality control procedures. If the level of any constituent measured in the sample of filter cake exceeds the levels set forth in Paragraph 1, then the waste is hazardous and must be managed in accordance with Subtitle C of RCRA. Data from the annual verification testing must be submitted to EPA within 60 days of the sampling event. [[Page 131]] (3) Changes in Operating Conditions: If BWX Technologies significantly changes the manufacturing or treatment process described in the petition, or the chemicals used in the manufacturing or treatment process, BWX Technologies may not manage the filter cake generated from the new process under this exclusion until it has met the following conditions: (a) BWX Technologies must demonstrate that the waste meets the delisting levels set forth in Paragraph 1; (b) it must demonstrate that no new hazardous constituents listed in appendix VIII of part 261 have been introduced into the manufacturing or treatment process: and (c) it must obtain prior written approval from EPA to manage the waste under this exclusion. (4) Data Submittals: The data obtained under Paragraphs 2 and 3 must be submitted to The Waste and Chemicals Management Division, U.S. EPA Region III, 1650 Arch Street, Philadelphia, PA 19103. Records of operating conditions and analytical data must be compiled, summarized, and maintained on site for a minimum of five years and must be furnished upon request by EPA or the Commonwealth of Virginia, and made available for inspection. Failure to submit the required data within the specified time period or to maintain the required records on site for the specified time period will be considered by EPA, at its discretion, sufficient basis to revoke the exclusion to the extent determined necessary by EPA. All data must be accompanied by a signed copy of the certification statement set forth in 40 CFR 260.22(i)(12) to attest to the truth and accuracy of the data submitted. (5) Reopener: (a) If BWX Technologies discovers that a condition at the facility or an assumption related to the disposal of the excluded waste that was modeled or predicted in the petition does not occur as modeled or predicted, then BWX Technologies must report any information relevant to that condition, in writing, to the Regional Administrator or his delegate within 10 days of discovering that condition. (b) Upon receiving information described in paragraph (a) of this section, regardless of its source, the Regional Administrator or his delegate will determine whether the reported condition requires further action. Further action may include repealing the exclusion, modifying the exclusion, or other appropriate response necessary to protect human health and the environment. (6) Notification Requirements: BWX Technologies must provide a one- time written notification to any State Regulatory Agency to which or through which the delisted waste described above will be transported for disposal at least 60 days prior to the commencement of such activities. Failure to provide such a notification will be deemed to be a violation of this exclusion and may result in a revocation of the decision. Capitol Products Harrisburg, PA... Dewatered wastewater treatment Corp.. sludges (EPA Hazardous Waste No. FO19) generated from the chemical conversion coating of aluminum after September 12, 1986. Capitol Products Kentland, IN..... Dewatered wastewater treatment Corporation. sludges (EPA Hazardous Waste No. F019) generated from the chemical conversion coating of aluminum after November 17, 1986. Care Free Charlotte, Wastewater treatment sludge (EPA Aluminum Michigan. Hazardous Waste No. F019) Products, Inc.. generated from the chemical conversion coating of aluminum (generated at a maximum annual rate of 100 cubic yards), after August 21, 1992. In order to confirm that the characteristics of the waste do not change significantly, the facility must, on an annual basis, analyze a representative composite sample for the constituents listed in Sec. 261.24 using the method specified therein. The annual analytical results, including quality control information, must be compiled, certified according to Sec. 260.22(i)(12), maintained on-site for a minimum of five years, and made available for inspection upon request by any employee or representative of EPA or the State of Michigan. Failure to maintain the required records on-site will be considered by EPA, at its discretion, sufficient basis to revoke the exclusion to the extent directed by EPA. Chamberlian- Hot Springs, AR.. Dewatered wastewater treatment Featherlite, sludges (EPA Hazardous Waste No. Inc.. F019) generated from the chemical conversion coating of aluminum after July 16, 1986. Cincinnati Cincinnati, OH... Sluiced bottom ash (approximately Metropolitan 25,000 cubic yards) contained in Sewer District. the South Lagoon, on September 13, 1985 which contains EPA Hazardous Waste Nos. F001, F002, F003, F004, and F005. Clay Equipment Cedar Falls, Iowa Dewatered wastewater treatment Corporation. sludges (EPA Hazardous Waste No. F006) and spent cyanide bath solutions (EPA Hazardous Waste No. F009) generated from electroplating operations and disposed of in an on-site surface impoundment. This is a onetime exclusion. This exclusion was published on August 1, 1989. Continental Can Olympia, WA...... Dewatered wastewater treatment Co.. sludges (DPA Hazardous Waste No. FO19) generated from the chemical conversion coating of aluminum after September 12, 1986. DaimlerChrysler Jefferson North Waste water treatment plant Corporation. Assembly Plant, sludge, F019, that is generated Detroit, by DaimlerChrysler Corporation at Michigan. the Jefferson North Assembly Plant (DCC-JNAP) at a maximum annual rate of 2,000 cubic yards per year. The sludge must be disposed of in a lined landfill with leachate collection, which is licensed, permitted, or otherwise authorized to accept the delisted wastewater treatment sludge in accordance with 40 CFR part 258. The exclusion becomes effective as of February 26, 2004. [[Page 132]] 1. Delisting Levels: (A) The concentrations in a TCLP extract of the waste measured in any sample may not exceed the following levels (mg/L): Antimony--0.659; Arsenic--0.3; Cadmium--0.48; Chromium--4.95; Lead--5; Nickel--90.5; Selenium-- 1; Thallium--0.282; Tin--721; Zinc--898; Acetone--228; p- Cresol--11.4; Formaldehyde--84.2; and Methylene chloride--0.288. (B) The total concentrations measured in any sample may not exceed the following levels (mg/ kg): Mercury--8.92; and Formaldehyde--689. (C) The sum of the ratios of the TCLP concentrations to the delisting levels for nickel and either thallium or cadmium shall not exceed 1.0. 2. Quarterly Verification Testing: To verify that the waste does not exceed the specified delisting levels, DCC-JNAP must collect and analyze one representative sample of the waste on a quarterly basis. 3. Changes in Operating Conditions: DCC-JNAP must notify the EPA in writing if the manufacturing process, the chemicals used in the manufacturing process, the treatment process, or the chemicals used in the treatment process significantly change. DCC- JNAP must handle wastes generated after the process change as hazardous until it has demonstrated that the wastes continue to meet the delisting levels and that no new hazardous constituents listed in appendix VIII of part 261 have been introduced and it has received written approval from EPA. 4. Data Submittals: DCC-JNAP must submit the data obtained through verification testing or as required by other conditions of this rule to both U.S. EPA Region 5, Waste Management Branch (DW- 8J), 77 W. Jackson Blvd., Chicago, IL 60604 and MDEQ, Waste Management Division, Hazardous Waste Program Section, at P.O. Box 30241, Lansing, Michigan 48909. The quarterly verification data and certification of proper disposal must be submitted annually upon the anniversary of the effective date of this exclusion. The facility must compile, summarize, and maintain on site for a minimum of five years records of operating conditions and analytical data. The facility must make these records available for inspection. All data must be accompanied by a signed copy of the certification statement in 40 CFR 260.22(i)(12). 5. Reopener Language--(a) If, anytime after disposal of the delisted waste, DCC-JNAP possesses or is otherwise made aware of any data (including but not limited to leachate data or groundwater monitoring data) relevant to the delisted waste indicating that any constituent is at a level in the leachate higher than the specified delisting level, or is in the groundwater at a concentration higher than the maximum allowable groundwater concentration in paragraph (e), then DCC-JNAP must report such data, in writing, to the Regional Administrator within 10 days of first possessing or being made aware of that data. (b) Based on the information described in paragraph (a) and any other information received from any source, the Regional Administrator will make a preliminary determination as to whether the reported information requires Agency action to protect human health or the environment. Further action may include suspending, or revoking the exclusion, or other appropriate response necessary to protect human health and the environment. (c) If the Regional Administrator determines that the reported information does require Agency action, the Regional Administrator will notify DCC- JNAP in writing of the actions the Regional Administrator believes are necessary to protect human health and the environment. The notice shall include a statement of the proposed action and a statement providing DCC- JNAP with an opportunity to present information as to why the proposed Agency action is not necessary or to suggest an alternative action. DCC-JNAP shall have 30 days from the date of the Regional Administrator's notice to present the information. (d) If after 30 days the facility presents no further information, the Regional Administrator will issue a final written determination describing the Agency actions that are necessary to protect human health or the environment. Any required action described in the Regional Administrator's determination shall become effective immediately, unless the Regional Administrator provides otherwise. (e) Maximum Allowable Groundwater Concentrations ([micro]g/L): Antimony--6; Arsenic--4.87; Cadmium--5; Chromium--100; Lead-- 15; Nickel--750; Selenium--50; Thallium--2; Tin--22,500; Zinc-- 11,300; acetone--3,750; p-Cresol-- 188; Formaldehyde--1,380; and Methylene chloride--5. Dover Corp., Tulsa, OK........ Dewatered wastewater treatment Norris Div.. sludge (EPA Hazardous Waste No. FO06) generated from their electroplating operations after April 29, 1986. DuraTherm, San Leon, Texas.. Desorber solids, (at a maximum Incorporated. generation of 20,000 cubic yards per calendar year) generated by DuraTherm using the thermal desorption treatment process, (EPA Hazardous Waste No. F037 and F038) and that is disposed of in subtitle D landfills after April 24, 2000. For the exclusion to be valid, DuraTherm must implement a testing program that meets the following Paragraphs: (1) Delisting Levels: All leachable concentrations for those constituents must not exceed the following levels (ppm). The petitioner must use an acceptable leaching method, for example SW-846, Method 1311 to measure constituents in the waste leachate. Desorber solids (i) Inorganic Constituents Arsenic--1.35; Antimony--0.162; Barium--54.0; Beryllium--0.108; Cadmium--0.135; Chromium--0.6; Lead--0.405; Nickel--2.7; Selenium--1.0; Silver--5.0; Vanadium--5.4; Zinc-- 270. [[Page 133]] (ii) Organic Constituents Anthracene--0.28; Benzene--0.135; Benzo(a) anthracene--0.059; Benzo(b)fluoranthene--0.11; Benzo(a)pyrene--0.061; Bis- ethylhexylphthalate--0.28; Carbon Disulfide--3.8; Chlorobenzene-- 0.057; Chrysene--0.059; o,m,p Cresols--54; Dibenzo (a,h) anthracene--0.055; 2,4 Dimethyl phenol--18.9; Dioctyl phthalate-- 0.017; Ethylbenzene--0.057; Fluoranthene--0.068; Fluorene-- 0.059; Naphthalene--0.059; Phenanthrene--0.059; Phenol--6.2; Pyrene--0.067; Styrene--2.7; Trichloroethylene--0.054; Toluene--0.08; Xylene--0.032 (2) Waste Holding and Handling: (A) DuraTherm must store the desorber solids as described in its RCRA permit, or continue to dispose of as hazardous all desorber solids generated, until they have completed verification testing described in Paragraph (3)(A) and (B), as appropriate, and valid analyses show that paragraph (1) is satisfied. (B) In order to isolate wastes that have been processed in the unit prior to one of the waste codes to be delisted, DuraTherm must designate the first batch of F037, F038, K048, K049, K050, or K051 wastes as hazardous. Subsequent batches of these wastes which satisfy paragraph (1) are eligible for delisting if they meet the criteria in paragraph (1) and no additional constituents (other than those of the delisted waste streams) from the previously processed wastes are detected. (C) Levels of constituents measured in the samples of the desorber solids that do not exceed the levels set forth in Paragraph (1) are nonhazardous. DuraTherm can manage and dispose the nonhazardous desorber solids according to all applicable solid waste regulations. (D) If constituent levels in a sample exceed any of the delisting levels set in Paragraph (1), DuraTherm must retreat or stabilize the batches of waste used to generate the representative sample until it meets the levels in paragraph(1). DuraTherm must repeat the analyses of the treated waste. (E) If the facility has not treated the waste, DuraTherm must manage and dispose the waste generated under subtitle C of RCRA. (3) Verification Testing Requirements: DuraTherm must perform sample collection and analyses, including quality control procedures, using appropriate methods. As applicable to the method-defined parameters of concern, analyses requiring the use of SW-846 methods incorporated by reference in 40 CFR 260.11 must be used without substitution. As applicable, the SW-846 methods might include Methods 0010, 0011, 0020, 0023A, 0030, 0031, 0040, 0050, 0051, 0060, 0061, 1010A, 1020B, 1110A, 1310B, 1311, 1312, 1320, 1330A, 9010C, 9012B, 9040C, 9045D, 9060A, 9070A (uses EPA Method 1664, Rev. A), 9071B, and 9095B. If EPA judges the process to be effective under the operating conditions used during the initial verification testing, DuraTherm may replace the testing required in Paragraph (3)(A) with the testing required in Paragraph (3)(B). DuraTherm must continue to test as specified in Paragraph (3)(A) until and unless notified by EPA in writing that testing in Paragraph (3)(A) may be replaced by Paragraph (3)(B). (A) Initial Verification Testing: After EPA grants the final exclusion, DuraTherm must do the following: (i) Collect and analyze composites of the desorber solids. (ii) Make two composites of representative grab samples collected. (iii) Analyze the waste, before disposal, for all of the constituents listed in Paragraph 1. (iv) Sixty (60) days after this exclusion becomes final, report the operational and analytical test data, including quality control information. (v) Submit the test plan for conducting the multiple pH leaching procedure to EPA for approval at least 10 days before conducting the analysis. (vi) Conduct a multiple pH leaching procedure on 10 samples collected during the sixty-day test period. (vii) The ten samples should include both non-stabilized and stabilized residual solids. If none of the samples collected during the sixty-day test period need to be stabilized, DuraTherm should provide multiple pH data on the first sample of stabilized wastes generated. (vii) Perform the toxicity characteristic leaching procedure using three different pH extraction fluids to simulate disposal under three conditions and submit the results within 60 days of completion. Simulate an acidic landfill environment, basic landfill environment, and a landfill environment similar to the pH of the waste. (B) Subsequent Verification Testing: Following written notification by EPA, DuraTherm may substitute the testing conditions in (3)(B) for (3)(A)(i). DuraTherm must continue to monitor operating conditions, and analyze representative samples each quarter of operation during the first year of waste generation. The samples must represent the waste generated in one quarter. DuraTherm must run the multiple pH procedure on these waste samples. (C) Termination of Organic Testing: (i) DuraTherm must continue testing as required under Paragraph (3)(B) for organic constituents in Paragraph (1)(A)(ii), until the analytical results submitted under Paragraph (3)(B) show a minimum of two consecutive samples below the delisting levels in Paragraph (1)(A)(i), DuraTherm may then request that EPA stop quarterly organic testing. After EPA notifies DuraTherm in writing, the company may end quarterly organic testing. (ii) Following cancellation of the quarterly testing, DuraTherm must continue to test a representative composite sample for all constituents listed in Paragraph (1) annually (by twelve months after final exclusion). [[Page 134]] (4) Changes in Operating Conditions: If DuraTherm significantly changes the process described in its petition or starts any processes that generate(s) the waste that may or could affect the composition or type of waste generated as established under Paragraph (1) (by illustration, but not limitation, changes in equipment or operating conditions of the treatment process), they must notify EPA in writing; they may no longer handle the wastes generated from the new process as nonhazardous until the wastes meet the delisting levels set in Paragraph (1) and they have received written approval to do so from EPA. (5) Data Submittals: DuraTherm must submit the information described below. If DuraTherm fails to submit the required data within the specified time or maintain the required records on- site for the specified time, EPA, at its discretion, will consider this sufficient basis to reopen the exclusion as described in Paragraph 6. DuraTherm must: (A) Submit the data obtained through Paragraph 3 to Mr. William Gallagher, Chief, Region 6 Delisting Program, EPA, 1445 Ross Avenue, Dallas, Texas 75202- 2733, Mail Code, (6PD-O) within the time specified. (B) Compile records of operating conditions and analytical data from Paragraph (3), summarized, and maintained on-site for a minimum of five years. (C) Furnish these records and data when EPA or the State of Texas request them for inspection. (D) Send along with all data a signed copy of the following certification statement, to attest to the truth and accuracy of the data submitted: Under civil and criminal penalty of law for the making or submission of false or fraudulent statements or representations (pursuant to the applicable provisions of the Federal Code, which include, but may not be limited to, 18 U.S.C. 1001 and 42 U.S.C. 6928), I certify that the information contained in or accompanying this document is true, accurate and complete. As to the (those) identified section(s) of this document for which I cannot personally verify its (their) truth and accuracy, I certify as the company official having supervisory responsibility for the persons who, acting under my direct instructions, made the verification that this information is true, accurate and complete. If any of this information is determined by EPA in its sole discretion to be false, inaccurate or incomplete, and upon conveyance of this fact to the company, I recognize and agree that this exclusion of waste will be void as if it never had effect or to the extent directed by EPA and that the company will be liable for any actions taken in contravention of the company's RCRA and CERCLA obligations premised upon the company's reliance on the void exclusion. (6) Reopener Language: (A) If, anytime after disposal of the delisted waste, DuraTherm possesses or is otherwise made aware of any environmental data (including but not limited to leachate data or groundwater monitoring data) or any other data relevant to the delisted waste indicating that any constituent identified for the delisting verification testing is at level higher than the delisting level allowed by the Regional Administrator or his delegate in granting the petition, then the facility must report the data, in writing, to the Regional Administrator or his delegate within 10 days of first possessing or being made aware of that data. (B) If the annual testing of the waste does not meet the delisting requirements in Paragraph 1, DuraTherm must report the data, in writing, to the Regional Administrator or his delegate within 10 days of first possessing or being made aware of that data. (C) If DuraTherm fails to submit the information described in paragraphs (5),(6)(A) or (6)(B) or if any other information is received from any source, the Regional Administrator or his delegate will make a preliminary determination as to whether the reported information requires Agency action to protect human health or the environment. Further action may include suspending, or revoking the exclusion, or other appropriate response necessary to protect human health and the environment. (D) If the Regional Administrator or his delegate determines that the reported information does require Agency action, the Regional Administrator or his delegate will notify the facility in writing of the actions the Regional Administrator or his delegate believes are necessary to protect human health and the environment. The notice shall include a statement of the proposed action and a statement providing the facility with an opportunity to present information as to why the proposed Agency action is not necessary. The facility shall have 10 days from the date of the Regional Administrator or his delegate's notice to present such information. (E) Following the receipt of information from the facility described in paragraph (6)(D) or (if no information is presented under paragraph (6)(D)) the initial receipt of information described in paragraphs (5), (6)(A) or (6)(B), the Regional Administrator or his delegate will issue a final written determination describing the Agency actions that are necessary to protect human health or the environment. Any required action described in the Regional Administrator or his delegate's determination shall become effective immediately, unless the Regional Administrator or his delegate provides otherwise. (7) Notification Requirements: DuraTherm must do following before transporting the delisted waste: Failure to provide this notification will result in a violation of the delisting petition and a possible revocation of the decision. [[Page 135]] (A) Provide a one-time written notification to any State Regulatory Agency to which or through which they will transport the delisted waste described above for disposal, 60 days before beginning such activities. (B) Update the one-time written notification if they ship the delisted waste into a different disposal facility. Eastman Chemical Longview, Texas.. Wastewater treatment sludge, (at a Company. maximum generation of 82,100 cubic yards per calendar year) generated by Eastman (EPA Hazardous Waste Nos. F001, F002, F003, F005 generated at Eastman when disposed of in a Subtitle D landfill. Eastman must implement a testing program that meets the following conditions for the exclusion to be valid: (1) Delisting Levels: All concentrations for the following constituents must not exceed the following levels (mg/l). For the wastewater treatment sludge constituents must be measured in the waste leachate by the method specified in 40 CFR 261.24. Wastewater treatment sludge: (i) Inorganic Constituents: Antimony-0.0515; Barium-7.30; Cobalt-2.25; Chromium-5.0; Lead- 5.0; Mercury-0.0015; Nickel-2.83; Selenium-0.22; Silver-0.384; Vanadium-2.11; Zinc-28.0 (ii) Organic Constituents: Acenaphthene-1.25; Acetone--7.13; bis(2-ethylhexylphthalate--0.28; 2-butanone--42.8; Chloroform-- 0.0099; Fluorene--0.55; Methanol- 35.7; Methylene Chloride--0.486; naphthalene-0.0321. (2) Waste Holding and Handling: If the concentrations of the sludge exceed the levels provided in Condition 1, then the sludge must be treated in the Fluidized Bed Incinerator (FBI) and meet the requirements of that September 25, 1996 delisting exclusion to be non-hazardous (as FBI ash). If the sludge meets the delisting levels provided in Condition 1, then it's non-hazardous (as sludge). If the waste water treatment sludge is not managed in the manner above, Eastman must manage it in accordance with applicable RCRA Subtitle C requirements. If the levels of constituents measured in the samples of the waste water treatment sludge do not exceed the levels set forth in Condition (1), then the waste is nonhazardous and may be managed and disposed of in accordance with all applicable solid waste regulations. During the verification period, Eastman must manage the waste in the FBI incinerator prior to disposal. (3) Verification Testing Requirements: Eastman must perform sample collection and analyses, including quality control procedures, using appropriate methods. As applicable to the method-defined parameters of concern, analyses requiring the use of SW-846 methods incorporated by reference in 40 CFR 260.11 must be used without substitution. As applicable, the SW-846 methods might include Methods 0010, 0011, 0020, 0023A, 0030, 0031, 0040, 0050, 0051, 0060, 0061, 1010A, 1020B, 1110A, 1310B, 1311, 1312, 1320, 1330A, 9010C, 9012B, 9040C, 9045D, 9060A, 9070A (uses EPA Method 1664, Rev. A), 9071B, and 9095B. After completion of the initial verification period, Eastman may replace the testing required in Condition (3)(A) with the testing required in Condition (3)(B). Eastman must continue to test as specified in Condition (3)(A) until and unless notified by EPA in writing that testing in Condition (3)(A) may be replaced by Condition (3)(B). (A) Initial Verification Testing: At quarterly intervals for one year after the final exclusion is granted, Eastman must collect and analyze composites of the wastewater treatment sludge for constituents listed in Condition (1). (B) Subsequent Verification Testing: Following termination of the quarterly testing, Eastman must continue to test a representative composite sample for all constituents listed in Condition (1) on an annual basis (no later than twelve months after the final exclusion). (4) Changes in Operating Conditions. If Eastman significantly changes the process which generate(s) the waste(s) and which may or could affect the composition or type of waste(s) generated as established under Condition (1) (by illustration, but not limitation, change in equipment or operating conditions of the treatment process or generation of volumes in excess 82,100 cubic yards of waste annually), Eastman must (A) notify the EPA in writing of the change and (B) may no longer handle or manage the waste generated from the new process as nonhazardous until Eastman has demonstrated through testing the waste meets the delisting levels set in Condition (1) and (C) Eastman has received written approval to begin managing the wastes as non-hazardous from EPA. (5) Data Submittals. Eastman must submit or maintain, as applicable, the information described below. If Eastman fails to submit the required data within the specified time or maintain the required records on- site for the specified time, EPA, at its discretion, will consider this sufficient basis to reopen the exclusion as described in Condition (6). Eastman must: (A) Submit the data obtained through Condition (3) to Mr. William Gallagher, Chief, Region 6 Delisting Program, EPA, 1445 Ross Avenue, Dallas, Texas 75202- 2733, Mail Code, (6PD-O) within the time specified. (B) Compile records of operating conditions and analytical data from Condition (3), summarized, and maintained on-site for a minimum of five years. (C) Furnish these records and data when EPA or the State of Texas request them for inspection. (D) Send along with all data a signed copy of the following certification statement, to attest to the truth and accuracy of the data submitted: [[Page 136]] (i) Under civil and criminal penalty of law for the making or submission of false or fraudulent statements or representations (pursuant to the applicable provisions of the Federal Code, which include, but may not be limited to, 18 U.S.C. 1001 and 42 U.S.C. 6928), I certify that the information contained in or accompanying this document is true, accurate and complete. (ii) As to the (those) identified section(s) of this document for which I cannot personally verify its (their) truth and accuracy, I certify as the company official having supervisory responsibility for the persons who, acting under my direct instructions, made the verification that this information is true, accurate and complete. (iii) If any of this information is determined by EPA in its sole discretion to be false, inaccurate or incomplete, and upon conveyance of this fact to the company, I recognize and agree that this exclusion of waste will be void as if it never had effect or to the extent directed by EPA and that the company will be liable for any actions taken in contravention of the company's RCRA and CERCLA obligations premised upon the company's reliance on the void exclusion. (6) Reopener Language: (A) If, anytime after disposal of the delisted waste, Eastman possesses or is otherwise made aware of any environmental data (including but not limited to leachate data or groundwater monitoring data) or any other data relevant to the delisted waste indicating that any constituent identified for the delisting verification testing is at level higher than the delisting level allowed by the Regional Administrator or his delegate in granting the petition, then the facility must report the data, in writing, to the Regional Administrator or his delegate within 10 days of first possessing or being made aware of that data. (B) If the annual testing of the waste does not meet the delisting requirements in Condition (1), Eastman must report the data, in writing, to the Regional Administrator or his delegate within 10 days of first possessing or being made aware of that data. (C) If Eastman fails to submit the information described in Conditions (5),(6)(A) or (6)(B) or if any other information is received from any source, the Regional Administrator or his delegate will make a preliminary determination as to whether the reported information requires Agency action to protect human health or the environment. Further action may include suspending, or revoking the exclusion, or other appropriate response necessary to protect human health and the environment. (D) If the Regional Administrator or his delegate determines that the reported information does require Agency action, the Regional Administrator or his delegate will notify the facility in writing of the actions the Regional Administrator or his delegate believes are necessary to protect human health and the environment. The notice shall include a statement of the proposed action and a statement providing the facility with an opportunity to present information as to why the proposed Agency action is not necessary. The facility shall have 10 days from the date of the Regional Administrator or his delegate's notice to present such information. (E) Following the receipt of information from the facility described in Condition (6)(D) or (if no information is presented under Condition (6)(D)) the initial receipt of information described in Conditions (5), (6)(A) or (6)(B), the Regional Administrator or his delegate will issue a final written determination describing the Agency actions that are necessary to protect human health or the environment. Any required action described in the Regional Administrator or his delegate's determination shall become effective immediately, unless the Regional Administrator or his delegate provides otherwise. (7) Notification Requirements. Eastman must do following before transporting the delisted waste off-site: Failure to provide this notification will result in a violation of the delisting petition and a possible revocation of the exclusion. (A) Provide a one-time written notification to any State Regulatory Agency to which or through which they will transport the delisted waste described above for disposal, 60 days before beginning such activities. (B) Update the one-time written notification if they ship the delisted waste into a different disposal facility. Eli Lilly and Clinton, Indiana. Incinerator scrubber liquids, Company. entering and contained in their onsite surface impoundment, and solids settling from these liquids originating from the burning of spent solvents (EPA Hazardous Waste Nos. F002, F003, and F005) contained in their onsite surface impoundment and solids retention area on August 18, 1988 and any new incinerator scubber liquids and settled solids generated in the surface impoundment and disposed of in the retention are after August 12, 1988. Envirite of Harvey, Illinois. See waste description under Illinois Envirite of Pennsylvania. (formerly Envirite Corporation). Envirite of Ohio Canton, Ohio..... See waste description under (formerly Envirite of Pennsylvania. Envirite Corporation). [[Page 137]] Envirite of York, Dewatered wastewater sludges (EPA Pennsylvania Pennsylvania. Hazardous Waste No .F006) (formerly generated from electroplating Envirite operations; spent cyanide plating Corporation). solutions (EPA Hazardous Waste No. F007) generated from electroplating operations; plating bath residues from the bottom of plating baths (EPA Hazardous Waste No. F008) generated from electroplating operations where cyanides are used in the process; spent stripping and cleaning bath solutions (EPA Hazardous Waste No. F009) generated from electroplating operations where cyanides are used in the process; spent cyanide solutions from salt bath pot cleaning (EPA Hazardous Waste No. F011) generated from metal heat treating operations; quenching wastewater treatment sludges (EPA Hazardous Waste No. F012) generated from metal heat treating where cyanides are used in the process; wastewater treatment sludges (EPA Hazardous Waste No. F019) generated from the chemical conversion coating of aluminum after November 14, 1986. To ensure that hazardous constituents are not present in the waste at levels of regulatory concern, the facility must implement a contingency testing program for the petitioned waste. This testing program must meet the following conditions for the exclusions to be valid: (1) Each batch of treatment residue must be representatively sampled and tested using the EP Toxicity test for arsenic, barium, cadmium, chromium, lead, selenium, silver, mercury, and nickel. If the extract concentrations for chromium, lead, arsenic, and silver exceed 0.315 ppm; barium levels exceed 6.3 ppm; cadmium and selenium exceed 0.063 ppm; mercury exceeds 0.0126 ppm; or nickel levels exceed 2.205 ppm; the waste must be re-treated or managed and disposed as a hazardous waste under 40 CFR Parts 262 to 265 and the permitting standards of 40 CFR Part 270. (2) Each batch of treatment residue must be tested for leachable cyanide. If the leachable cyanide levels (using the EP Toxicity test without acetic acid adjustment) exceed 1.26 ppm, the waste must be re- treated or managed and disposed as a hazardous waste under 40 CFR Parts 262 to 265 and the permitting standards of 40 CFR Part 270. (3) Each batch of waste must be tested for the total content of specific organic toxicants. If the total content of anthracene exceeds 76.8 ppm, 1,2-diphenyl hydrazine exceeds 0.001 ppm, methylene chloride exceeds 8.18 ppm, methyl ethyl ketone exceeds 326 ppm, n-nitrosodiphenylamine exceeds 11.9 ppm, phenol exceeds 1,566 ppm, tetrachloroethylene exceeds 0.188 ppm, or trichloroethylene exceeds 0.592 ppm, the waste must be managed and disposed as a hazardous waste under 40 CFR Parts 262 to 265 and the permitting standards of 40 CFR Part 270. (4) A grab sample must be collected from each batch to form one monthly composite sample which must be tested using GC/MS analysis for the compounds listed in 3, above, as well as the remaining organics on the priority pollutant list. (See 47 FR 52309, November 19, 1982, for a list of the priority pollutants.) (5) The data from conditions 1-4 must be kept on file at the facility for inspection purposes and must be compiled, summarized, and submitted to the Administrator by certified mail semi-annually. The Agency will review this information and if needed will propose to modify or withdraw the exclusion. The organics testing described in conditions 3 and 4, above, are not required until six months from the date of promulgation. The Agency's decision to conditionally exclude the treatment residue generated from the wastewater treatment systems at these facilities applies only to the wastewater and solids treatment systems as they presently exist as described in the delisting petition. The exclusion does not apply to the proposed process additions described in the petition as recovery including crystallization, electrolytic metals recovery, evaporative recovery, and ion exchange. EPA's Mobile Denney Farm Site; Process wastewater, rotary kiln Incineration McDowell, MO. ash, CHEAF media, and other System. solids (except spent activated carbon) (EPA Hazardous Waste Nos. F020, F022, F023, F026, F027, and F028) generated during the field demonstration of EPA's Mobile Incinerator at the Denney Farm Site in McDowell, Missouri, after July 25, 1985, so long as: (1) The incinerator is functioning properly; (2) a grab sample is taken from each tank of wastewater generated and the EP leachate values do not exceed 0.03 ppm for mercury, 0.14 ppm for selenium, and 0.68 ppm for chromium; and (3) a grab sample is taken from each drum of soil or ash generated and a core sample is collected from each CHEAF roll generated and the EP leachate values of daily composites do not exceed 0.044 ppm in ash or CHEAF media for mercury or 0.22 ppm in ash or CHEAF media for selenium. Falconer Glass Falconer, NY..... Wastewater treatment sludges from Indust., Inc.. the filter press and magnetic drum separator (EPA Hazardous Waste No. F006) generated from electroplating operations after July 16, 1986. Florida Daytona Beach, This is a one-time exclusion. Production Florida. Wastewater treatment sludges (EPA Engineering Hazardous Waste No. F006) Company. generated from electroplating operations and contained in four on-site trenches on January 23, 1987. Ford Motor Dearborn, Wastewater treatment plant sludge, Company, Michigan. F019, that is generated by Ford Dearborn Truck Motor Company at the Dearborn Assembly Plant. Truck Asembly Plant at a maximum annual rate of 2,000 cubic yards per year. The sludge must be disposed of in a lined landfill with leachate collection which is licensed, permitted, or otherwise authorized to accept the delisted wastewater treatment sludge in accordance with 40 CFR part 258. The exclusion becomes effective as of April 25, 2005. [[Page 138]] 1. Delisting Levels: (A) The concentrations in a TCLP extract of the waste measured in any sample may not exceed the following levels (mg/L): antimony--0.7; arsenic--0.3; barium--100; cadmium--0.5; chromium--5; lead--5; nickel--90; selenium--1; thallium--0.3; zinc-- 900; p-cresol--11; di-n-octyl phthlate--0.11; formaldehyde--80; and pentachlorophenol--0.009. (B) The total concentration measured in any sample may not exceed the following levels (mg/kg): mercury--9; and formaldehyde-- 700. 2. Quarterly Verification Testing: To verify that the waste does not exceed the specified delisting levels, Dearborn Truck Assembly Plant must collect and analyze one representative sample of the waste on a quarterly basis. 3. Changes in Operating Conditions: Dearborn Truck Assembly Plant must notify the EPA in writing if the manufacturing process, the chemicals used in the manufacturing process, the treatment process, or the chemicals used in the treatment process change significantly. Dearborn Truck Assembly Plant must handle wastes generated after the process change as hazardous until it has demonstrated that the wastes continue to meet the delisting levels and that no new hazardous constituents listed in appendix VIII of part 261 have been introduced and it has received written approval from EPA. 4. Data Submittals: Dearborn Truck Assembly Plant [Redln Off] must submit the data obtained through verification testing or as required by other conditions of this rule to both U.S. EPA Region 5, Waste Management Branch (DW- 8J), 77 W. Jackson Blvd., Chicago, IL 60604 and MDEQ, Waste Management Division, Hazardous Waste Program Section, at P.O. Box 30241, Lansing, Michigan 48909. The quarterly verification data and certification of proper disposal must be submitted annually upon the anniversary of the effective date of this exclusion. Dearborn Truck Assembly Plant must compile, summarize and maintain on site for a minimum of five years records of operating conditions and analytical data. Dearborn Truck Assembly Plant must make these records available for inspection. All data must be accompanied by a signed copy of the certification statement in 40 CFR 260.22(i)(12). 5. Reopener Language--(a) If, anytime after disposal of the delisted waste, Dearborn Truck Assembly Plant possesses or is otherwise made aware of any data (including but not limited to leachate data or groundwater monitoring data) relevant to the delisted waste indicating that any constituent is at a level in the leachate higher than the specified delisting level, or is in the groundwater at a concentration higher than the maximum allowable groundwater concentration in paragraph (e), then Dearborn Truck Assembly Plant must report such data, in writing, to the Regional Administrator within 10 days of first possessing or being made aware of that data. (b) Based on the information described in paragraph (a) and any other information received from any source, the Regional Administrator will make a preliminary determination as to whether the reported information requires Agency action to protect human health or the environment. Further action may include suspending, or revoking the exclusion, or other appropriate response necessary to protect human health and the environment. (c) If the Regional Administrator determines that the reported information does require Agency action, the Regional Administrator will notify Dearborn Truck Assembly Plant in writing of the actions the Regional Administrator believes are necessary to protect human health and the environment. The notice shall include a statement of the proposed action and a statement providing Dearborn Truck Assembly Plant with an opportunity to present information as to why the proposed Agency action is not necessary or to suggest an alternative action. Dearborn Truck Assembly Plant shall have 30 days from the date of the Regional Administrator's notice to present the information. (d) If after 30 days the Dearborn Truck Assembly Plant presents no further information, the Regional Administrator will issue a final written determination describing the Agency actions that are necessary to protect human health or the environment. Any required action described in the Regional Administrator's determination shall become effective immediately, unless the Regional Administrator provides otherwise. (e) Maximum Allowable Groundwater Concentrations ([micro]g/L): antimony--6; arsenic--5; barium-- 2,000; cadmium--5; chromium--100; lead--15; nickel--800; selenium-- 50; thallium--2; tin--20,000; zinc--11,000; p-Cresol--200; Di-n- octyl phthlate--1.3; Formaldehyde--1,400; and Pentachlorophenol--0.15. Ford Motor Claycomo, Wastewater treatment sludge, F019, Company, Kansas Missouri. that is generated at the Ford City Assembly Motor Company (Ford) Kansas City Plant. Assembly Plant (KCAP) at a maximum annual rate of 2,000 cubic yards per year. The sludge must be disposed of in a lined landfill with leachate collection, which is licensed, permitted, or otherwise authorized to accept the delisted wastewater treatment sludge in accordance with 40 CFR part 258. The exclusion becomes effective as of June 6, 2007. 1. Delisting Levels: (a) The concentrations in a TCLP extract of the waste measured in any sample may not equal or exceed the following levels (mg/L): barium--100; chromium--5; mercury--0.155; nickel--90; thallium--0.282; zinc--898; cyanides--11.5; ethyl benzene-- 42.6; toluene--60.8; total xylenes--18.9; bis(2-ethylhexyl) phthalate--0.365; p-cresol--11.4; 2,4-dinitrotoluene--0.13; formaldehyde--343; and napthalene--.728; (b) The total concentrations measured in any sample may not exceed the following levels (mg/ kg): chromium 760000; mercury-- 10.4; thallium--116000; 2,4- dinitrotoluene--100000; and formaldehyde--6880. [[Page 139]] 2. Quarterly Verification Testing: To verify that the waste does not exceed the specified delisting levels, Ford must collect and analyze one representative sample of KCAP's sludge on a quarterly basis. 3. Changes in Operating Conditions: Ford must notify the EPA in writing if the manufacturing process, the chemicals used in the manufacturing process, the treatment process, or the chemicals used in the treatment process at KCAP significantly change. Ford must handle wastes generated at KCAP after the process change as hazardous until it has demonstrated that the waste continues to meet the delisting levels and that no new hazardous constituents listed in appendix VIII of part 261 have been introduced and Ford has received written approval from EPA for the changes. 4. Data Submittals: Ford must submit the data obtained through verification testing at KCAP or as required by other conditions of this rule to EPA Region 7, Air, RCRA and Toxics Division, 901 N. 5th, Kansas City, Kansas 66101. The quarterly verification data and certification of proper disposal must be submitted annually upon the anniversary of the effective date of this exclusion. Ford must compile, summarize, and maintain at KCAP records of operating conditions and analytical data for a minimum of five years. Ford must make these records available for inspection. All data must be accompanied by a signed copy of the certification statement in 40 CFR 260.22(i)(12). 5. Reopener Language--(a) If, anytime after disposal of the delisted waste, Ford possesses or is otherwise made aware of any data (including but not limited to leachate data or groundwater monitoring data) relevant to the delisted waste at KCAP indicating that any constituent is at a level in the leachate higher than the specified delisting level, or is in the groundwater at a concentration higher than the maximum allowable groundwater concentration in paragraph (e), then Ford must report such data in writing to the Regional Administrator within 10 days of first possessing or being made aware of that data. (b) Based on the information described in paragraph (a) and any other information received from any source, the Regional Administrator will make a preliminary determination as to whether the reported information requires Agency action to protect human health or the environment. Further action may include suspending, or revoking the exclusion, or other appropriate response necessary to protect human health and the environment. (c) If the Regional Administrator determines that the reported information does require Agency action, the Regional Administrator will notify Ford in writing of the actions the Regional Administrator believes are necessary to protect human health and the environment. The notice shall include a statement of the proposed action and a statement providing Ford with an opportunity to present information as to why the proposed Agency action is not necessary or to suggest an alternative action. Ford shall have 30 days from the date of the Regional Administrator's notice to present the information. (d) If after 30 days Ford presents no further information, the Regional Administrator will issue a final written determination describing the Agency actions that are necessary to protect human health or the environment. Any required action described in the Regional Administrator's determination shall become effective immediately, unless the Regional Administrator provides otherwise. Ford Motor Wayne, Michigan.. Waste water treatment plant Company, sludge, F019, that is generated Michigan Truck by Ford Motor Company at the Plant and Wayne Wayne Integrated Stamping and Integrated Assembly Plant from wastewaters Stamping and from both the Wayne Integrated Assembly Plant.. Stamping and Assembly Plant and the Michigan Truck Plant, Wayne, Michigan at a maximum annual rate of 2,000 cubic yards per year. The sludge must be disposed of in a lined landfill with leachate collection, which is licensed, permitted, or otherwise authorized to accept the delisted wastewater treatment sludge in accordance with 40 CFR part 258. The exclusion becomes effective as of July 30, 2003. 1. Delisting Levels: (A) The TCLP concentrations measured in any sample may not exceed the following levels (mg/L): Antimony--0.659; Arsenic--0.3; Cadmium--0.48; Chromium--4.95; Lead--5; Nickel--90.5; Selenium-- 1; Thallium--0.282; Tin--721; Zinc--898; p-Cresol--11.4; and Formaldehyde--84.2. (B) The total concentrations measured in any sample may not exceed the following levels (mg/kg): Mercury--8.92; and Formaldehyde-- 689. (C) The sum of the ratios of the TCLP concentrations to the delisting levels for nickel and thallium and for nickel and cadmium shall not exceed 1.0. 2. Quarterly Verification Testing: To verify that the waste does not exceed the specified delisting levels, the facility must collect and analyze one waste sample on a quarterly basis. 3. Changes in Operating Conditions: The facility must notify the EPA in writing if the manufacturing process, the chemicals used in the manufacturing process, the treatment process, or the chemicals used in the treatment process significantly change. The facility must handle wastes generated after the process change as hazardous until it has demonstrated that the wastes continue to meet the delisting levels and that no new hazardous constituents listed in appendix VIII of part 261 have been introduced and it has received written approval from EPA. [[Page 140]] 4. Data Submittals: The facility must submit the data obtained through verification testing or as required by other conditions of this rule to both U.S. EPA Region 5, Waste Management Branch (DW-8J), 77 W. Jackson Blvd., Chicago, IL 60604 and MDEQ, Waste Management Division, Hazardous Waste Program Section, at P.O. Box 30241, Lansing, Michigan 48909. The quarterly verification data and certification of proper disposal must be submitted annually upon the anniversary of the effective date of this exclusion. The facility must compile, summarize, and maintain on site for a minimum of five years records of operating conditions and analytical data. The facility must make these records available for inspection. All data must be accompanied by a signed copy of the certification statement in 40 CFR 260.22(i)(12). 5. Reopener Language--(a) If, anytime after disposal of the delisted waste, the facility possesses or is otherwise made aware of any data (including but not limited to leachate data or groundwater monitoring data) relevant to the delisted waste indicating that any constituent is at a level in the leachate higher than the specified delisting level, or is in the groundwater at a concentration higher than the maximum allowable groundwater concentration in paragraph (e), then the facility must report such data, in writing, to the Regional Administrator within 10 days of first possessing or being made aware of that data. (b) Based on the information described in paragraph (a) and any other information received from any source, the Regional Administrator will make a preliminary determination as to whether the reported information requires Agency action to protect human health or the environment. Further action may include suspending, or revoking the exclusion, or other appropriate response necessary to protect human health and the environment. (c) If the Regional Administrator determines that the reported information does require Agency action, the Regional Administrator will notify the facility in writing of the actions the Regional Administrator believes are necessary to protect human health and the environment. The notice shall include a statement of the proposed action and a statement providing the facility with an opportunity to present information as to why the proposed Agency action is not necessary or to suggest an alternative action. The facility shall have 30 days from the date of the Regional Administrator's notice to present the information. (d) If after 30 days the facility presents no further information, the Regional Administrator will issue a final written determination describing the Agency actions that are necessary to protect human health or the environment. Any required action described in the Regional Administrator's determination shall become effective immediately, unless the Regional Administrator provides otherwise. (e) Maximum Allowable Groundwater Concentrations (ug/ L): Antimony--6; Arsenic--4.87; Cadmium--5; Chromium--100; Lead--15; Nickel--750; Selenium--50; Thallium--2; Tin-- 22,500; Zinc--11,300; p-Cresol-- 188; and Formaldehyde--1,380. Ford Motor Wixom, Michigan.. Waste water treatment plant Company, Wixom sludge, F019, that is generated Assembly Plant. by Ford Motor Company at the Wixom Assembly Plant, Wixom, Michigan at a maximum annual rate of 2,000 cubic yards per year. The sludge must be disposed of in a lined landfill with leachate collection, which is licensed, permitted, or otherwise authorized to accept the delisted wastewater treatment sludge in accordance with 40 CFR Part 258. The exclusion becomes effective as of July 30, 2003. The conditions in paragraphs (2) through (5) for Ford Motor Company--Michigan Truck Plant and Wayne Integrated Stamping Plant-- Wayne, Michigan also apply. Delisting Levels: (A) The TCLP concentrations measured in any sample may not exceed the following levels (mg/L): Antimony--0.659; Arsenic--0.3; Cadmium--0.48; Chromium--4.95; Lead--5; Nickel--90.5; Selenium-- 1; Thallium--0.282; Tin--721; Zinc--898; p-Cresol--11.4; and Formaldehyde--84.2. (B) The total concentrations measured in any sample may not exceed the following levels (mg/kg): Mercury--8.92; and Formaldehyde-- 689. (C) The sum of the ratios of the TCLP concentrations to the delisting levels for nickel and thallium and for nickel and cadmium shall not exceed 1.0. GE's Former RCA Barceloneta, PR.. Wastewater treatment plant (WWTP) del Caribe. sludges from chemical etching operation (EPA Hazardous Waste No. F006) and contaminated soil mixed with sludge. This is a one- time exclusion for a range of 5,000 to 15,000 cubic yards of WWTP sludge on condition of disposal in a Subtitle D landfill. This exclusion was published on February 1, 2007. 1. Reopener Language--(a) If, anytime after disposal of the delisted waste, GE discovers that any condition or assumption related to the characterization of the excluded waste which was used in the evaluation of the petition or that was predicted through modeling is not as reported in the petition, then GE must report any information relevant to that condition or assumption, in writing, to the Director of the Division of Environmental Planning and Protection in Region 2 within 10 days of first of discovering that information. (b) Upon receiving information described in paragraph (a) of this section, regardless of its source, the Director will determine whether the reported condition requires further action. Further action may include repealing the exclusion, modifying the exclusion, or other appropriate action deemed necessary to protect human health or the environment. 2. Notifications--GE must provide a one-time written notification to any State or Commonwealth Regulatory Agency in any State or Commonwealth to which or through which the waste described above will be transported for disposal at least 60 days prior to the commencement of such activities. Failure to provide such a notification will result in a violation of the waste exclusion and a possible revocation of the decision. [[Page 141]] General Electric Shreveport Wastewater treatment sludges (EPA Company. Louisiana. Hazardous Waste No. F006) generated from electroplating operations and contained in four on-site treatment ponds on August 12, 1987. General Motors... Arlington, TX.... Wastewater Treatment Sludge (WWTP) (EPA Hazardous Waste No. F019) generated at a maximum annual rate of 3,000 cubic yards per calendar year after January 3, 2007 and disposed in a Subtitle D landfill. For the exclusion to be valid, GM- Arlington must implement a verification testing program that meets the following paragraphs: (1) Delisting Levels: All leachable concentrations for those constituents must not exceed the following levels (mg/l for TCLP). (i) Inorganic Constituents: Barium-100; Cadmium-0.36; Chromium- 5 (3.71) ; Cobalt-18.02; Lead-5; Nickel-67.8; Silver-5; Tin-540; Zinc-673. (ii) Organic Constituents: Acetone-171; Ethylbenzene-31.9; N- Butyl Alcohol-171; Toluene-45.6; Bis(2-Ethylhexyl) Phthalate-0.27; p-Cresol-8.55; Naphthalene-3.11. (2) Waste Management: (A) GM- Arlington must manage as hazardous all WWTP sludge generated, until it has completed initial verification testing described in paragraph (3)(A) and (B), as appropriate, and valid analyses show that paragraph(1) is satisfied. (B) Levels of constituents measured in the samples of the WWTP sludge that do not exceed the levels set forth in paragraph (1) are non-hazardous. GM-Arlington can manage and dispose of the non- hazardous WWTP sludge according to all applicable solid waste regulations. (C) If constituent levels in a sample exceed any of the delisting levels set in paragraph (1), GM- Arlington can collect one additional sample and perform expedited analyses to verify if the constituent exceeds the delisting level. If this sample confirms the exceedance, GM- Arlington must, from that point forward, treat the waste as hazardous until it is demonstrated that the waste again meets the levels in paragraph (1). GM- Arlington must manage and dispose of the waste generated under Subtitle C of RCRA from the time it becomes aware of any exceedance. (D) Upon completion of the Verification Testing described in paragraph 3(A) and (B), as appropriate, and the transmittal of the results to EPA, and if the testing results meet the requirements of paragraph (1), GM- Arlington may proceed to manage its WWTP sludge as non-hazardous waste. If subsequent Verification Testing indicates an exceedance of the Delisting Levels in paragraph (1), GM-Arlington must manage the WWTP sludge as a hazardous waste until two consecutive quarterly testing samples show levels below the Delisting Levels in paragraph (1). (3) Verification Testing Requirements: GM-Arlington must perform sample collection and analyses, including quality control procedures, according to appropriate methods such as those found in SW-846 or other reliable sources (with the exception of analyses requiring the use of SW- 846 methods incorporated by reference in 40 CFR 260.11, which must be used without substitution) for all constituents listed in paragraph (1). If EPA judges the process to be effective under the operating conditions used during the initial verification testing, GM- Arlington may replace the testing required in paragraph (3)(A) with the testing required in paragraph (3)(B). GM-Arlington Plant must continue to test as specified in paragraph (3)(A) until and unless notified by EPA in writing that testing in paragraph (3)(A) may be replaced by paragraph (3)(B). (A) Initial Verification Testing: After EPA grants the final exclusion, GM-Arlington must do the following: (i) Within 30 days of this exclusion becoming final, collect two (2) samples, before disposal, of the WWTP sludge. (ii) The samples are to be analyzed and compared against the Delisting Levels in paragraph (1). (iii) Within 60 days of the exclusion becoming final, GM- Arlington must report to EPA the initial verification analytical test data for the WWTP sludge, including analytical quality control information for the first thirty (30) days of operation after this exclusion becomes final. If levels of constituents measured in these samples of the WWTP sludge do not exceed the levels set forth in paragraph (1), GM- Arlington can manage and dispose of the WWTP sludge according to all applicable solid waste regulations. (B) Subsequent Verification Testing: Following written notification by EPA, GM-Arlington may substitute the testing conditions in paragraph (3)(B) for paragraph (3)(A). GM- Arlington must continue to monitor operating conditions, and analyze two representative samples of the WWTP sludge for the next three quarters of operation during the first year of waste generation. The samples must represent the waste generated during the quarter. Quarterly reports are due to EPA, thirty days after the samples are taken. After the first year of analytical sampling, verification sampling can be performed on a single annual sample of the WWTP sludge. The results are to be compared to the delisting levels in paragraph (1). (C) Termination of Testing: (i) After the first year of quarterly testing, if the delisting levels in paragraph (1) are being met, GM-Arlington may then request that EPA not require quarterly testing. (ii) Following cancellation of the quarterly testing by EPA letter, GM-Arlington must continue to test one representative sample for all constituents listed in paragraph (1) annually. Results must be provided to EPA within 30 days of the testing. [[Page 142]] (4) Changes in Operating Conditions: If GM-Arlington significantly changes the process described in its petition or starts any process that generates the waste that may or could significantly affect the composition or type of waste generated as established under paragraph (1) (by illustration, but not limitation, changes in equipment or operating conditions of the treatment process), it must notify EPA in writing; it may no longer handle the wastes generated from the new process as nonhazardous until the wastes meet the delisting levels set in paragraph (1) and it has received written approval to do so from EPA. (5) Data Submittals: GM-Arlington must submit the information described below. If GM-Arlington fails to submit the required data within the specified time or maintain the required records on- site for the specified time, EPA, at its discretion, will consider this sufficient basis to reopen the exclusion as described in paragraph 6. GM-Arlington must: (A) Submit the data obtained through paragraph(3) to the Section Chief, Region 6 Corrective Action and Waste Minimization Section, EPA, 1445 Ross Avenue, Dallas, Texas 75202-2733, Mail Code, (6PD-C) within the time specified. (B) Compile records of operating conditions and analytical data from paragraph (3), summarized, and maintained on-site for a minimum of five years. (C) Furnish these records and data when EPA or the State of Texas requests them for inspection. (D) Send along with all data a signed copy of the following certification statement, to attest to the truth and accuracy of the data submitted: ``Under civil and criminal penalty of law for the making or submission of false or fraudulent statements or representations (pursuant to the applicable provisions of the Federal Code, which include, but may not be limited to, 18 U.S.C. 1001 and 42 U.S.C. 6928), I certify that the information contained in or accompanying this document is true, accurate and complete. As to the (those) identified section(s) of this document for which I cannot personally verify its (their) truth and accuracy, I certify as the company official having supervisory responsibility for the persons who, acting under my direct instructions, made the verification that this information is true, accurate and complete. If any of this information is determined by EPA in its sole discretion to be false, inaccurate or incomplete, and upon conveyance of this fact to the company, I recognize and agree that this exclusion of waste will be void as if it never had effect or to the extent directed by EPA and that the company will be liable for any actions taken in contravention of the company's RCRA and CERCLA obligations premised upon the company's reliance on the void exclusion.'' (6) Re-opener; (A) If, anytime after disposal of the delisted waste, GM- Arlington possesses or is otherwise made aware of any environmental data (including but not limited to leachate data or groundwater monitoring data) or any other data relevant to the delisted waste indicating that any constituent identified for the delisting verification testing is at a level higher than the delisting level allowed by EPA in granting the petition, then the facility must report the data, in writing, to EPA within 10 days of first possessing or being made aware of that data. (B) If either the quarterly or annual testing of the waste does not meet the delisting requirements in paragraph 1, GM- Arlington must report the data, in writing, to EPA within 10 days of first possessing or being made aware of that data. (C) If GM-Arlington fails to submit the information described in paragraphs (5), (6)(A) or (6)(B) or if any other information is received from any source, EPA will make a preliminary determination as to whether the reported information requires action to protect human health and/ or the environment. Further action may include suspending, or revoking the exclusion, or other appropriate response necessary to protect human health and the environment. (D) If EPA determines that the reported information requires action, EPA will notify the facility in writing of the actions it believes are necessary to protect human health and the environment. The notice shall include a statement of the proposed action and a statement providing the facility with an opportunity to present information explaining why the proposed EPA action is not necessary. The facility shall have 10 days from the date of EPA's notice to present such information. (E) Following the receipt of information from the facility described in paragraph (6)(D) or (if no information is presented under paragraph (6)(D)) the initial receipt of information described in paragraphs (5), (6)(A) or (6)(B), EPA will issue a final written determination describing the actions that are necessary to protect human health and/or the environment. Any required action described in EPA's determination shall become effective immediately, unless EPA provides otherwise. (7) Notification Requirements: GM- Arlington must do the following before transporting the delisted waste. Failure to provide this notification will result in a violation of the delisting petition and a possible revocation of the decision. (A) Provide a one-time written notification to any state Regulatory Agency to which or through which it will transport the delisted waste described above for disposal, 60 days before beginning such activities. (B) Update the one-time written notification if it ships the delisted waste into a different disposal facility. (C) Failure to provide this notification will result in a violation of the delisting variance and a possible revocation of the decision. [[Page 143]] General Motors Lake Orion, Wastewater treatment plant (WWTP) Corporation. Michigan. sludge from the chemical conversion coating (phosphate coating) of aluminum (EPA Hazardous Waste No. F019) generated at a maximum annual rate of 1,500 tons per year (or 1,500 cubic yards per year), after October 24, 1997 and disposed of in a Subtitle D landfill. 1. Verification Testing: GM must implement an annual testing program to demonstrate, based on the analysis of a minimum of four representative samples, that the constituent concentrations measured in the TCLP (or OWEP, where appropriate) extract of the waste are within specific levels. The constituent concentrations must not exceed the following levels (mg/l) which are back- calculated from the delisting health-based levels and a DAF of 90: Arsenic--4.5; Cobalt--189; Copper--126; Nickel--63; Vanadium--18; Zinc--900; 1,2- Dichloroethane--0.45; Ethylbenzene--63; 4-Methylphenol-- 16.2; Naphthalene--90; Phenol-- 1800; and Xylene--900. The constituent concentrations must also be less than the following levels (mg/l) which are the toxicity characteristic levels: Barium--100.0; and Chromium (total)--5.0. 2. Changes in Operating Conditions: If GM significantly changes the manufacturing or treatment process or the chemicals used in the manufacturing or treatment process, GM may handle the WWTP filter press sludge generated from the new process under this exclusion after the facility has demonstrated that the waste meets the levels set forth in paragraph 1 and that no new hazardous constituents listed in Appendix VIII of Part 261 have been introduced. 3. Data Submittals: The data obtained through annual verification testing or paragraph 2 must be submitted to U.S. EPA Region 5, 77 W. Jackson Blvd., Chicago, IL 60604-3590, within 60 days of sampling. Records of operating conditions and analytical data must be compiled, summarized, and maintained on site for a minimum of five years and must be made available for inspection. All data must be accompanied by a signed copy of the certification statement in 260.22(I)(12). General Motors Lordstown, Ohio.. Waste water treatment plant Corporation sludge, F019, that is generated Assembly Plant at General Motors Corporation's Lordstown Assembly Plant at a maximum annual rate of 2,000 cubic yards per year. The sludge must be disposed of in a Subtitle D landfill which is licensed, permitted, or otherwise authorized by a state to accept the delisted wastewater treatment sludge. The exclusion becomes effective as of October 12, 2004. 1. Delisting Levels: (A) The constituent concentrations measured in the TCLP extract may not exceed the following levels (mg/L): antimony--0.66; arsenic-- 0.30; chromium--5; lead--5; mercury--0.15; nickel--90; selenium--1; silver--5; thallium-- 0.28; tin--720; zinc--900; fluoride--130; p-cresol--11; formaldehyde--84; and methylene chloride--0.29 (B) The total constituent concentration measured in any sample of the waste may not exceed the following levels (mg/kg): chromium--4,100 ; formaldehyde-- 700; and mercury--10. (C) Maximum allowable groundwater concentrations ([micro]g/L) are as follows: antimony--6; arsenic-- 4.88; chromium--100; lead--15; mercury--2; nickel--750; selenium--50; silver--188; thallium--2; tin--22,500; zinc-- 11,300; fluoride--4,000; p- cresol--188; formaldehyde--1,390; and methylene chloride--5. 2. Quarterly Verification Testing: To verify that the waste does not exceed the specified delisting levels, GM must collect and analyze one waste sample on a quarterly basis using methods with appropriate detection levels and elements of quality control. 3. Changes in Operating Conditions: The facility must notify the EPA in writing if the manufacturing process, the chemicals used in the manufacturing process, the treatment process, or the chemicals used in the treatment process significantly change. GM must handle wastes generated after the process change as hazardous until it has demonstrated that the wastes continue to meet the delisting levels and that no new hazardous constituents listed in appendix VIII of part 261 have been introduced and it has received written approval from EPA. 4. Data Submittals: The facility must submit the data obtained through verification testing or as required by other conditions of this rule to U.S. EPA Region 5, Waste Management Branch, RCRA Delisting Program (DW-8J), 77 W. Jackson Blvd., Chicago, IL 60604. The quarterly verification data and certification of proper disposal must be submitted annually upon the anniversary of the effective date of this exclusion. The facility must compile, summarize, and maintain on site for a minimum of five years records of operating conditions and analytical data. The facility must make these records available for inspection. All data must be accompanied by a signed copy of the certification statement in 40 CFR 260.22(i)(12). [[Page 144]] 5. Reopener Language: (A) If, anytime after disposal of the delisted waste, GM possesses or is otherwise made aware of any data (including but not limited to leachate data or groundwater monitoring data) relevant to the delisted waste indicating that any constituent is at a level in the leachate higher than the specified delisting level, or is in the groundwater at a concentration higher than the maximum allowable groundwater concentration in paragraph (1), then GM must report such data, in writing, to the Regional Administrator within 10 days of first possessing or being made aware of that data. (B) Based on the information described in paragraph (A) and any other information received from any source, the Regional Administrator will make a preliminary determination as to whether the reported information requires Agency action to protect human health or the environment. Further action may include suspending, or revoking the exclusion, or other appropriate response necessary to protect human health and the environment. (C) If the Regional Administrator determines that the reported information does require Agency action, the Regional Administrator will notify the facility in writing of the actions the Regional Administrator believes are necessary to protect human health and the environment. The notice shall include a statement of the proposed action and a statement providing GM with an opportunity to present information as to why the proposed Agency action is not necessary or to suggest an alternative action. GM shall have 30 days from the date of the Regional Administrator's notice to present the information. (D) If after 30 days GM presents no further information, the Regional Administrator will issue a final written determination describing the Agency actions that are necessary to protect human health or the environment. Any required action described in the Regional Administrator's determination shall become effective immediately, unless the Regional Administrator provides otherwise. General Motors Elyria, OH....... The residue generated from the use Corp., Fisher of the Chemfix [reg] treatment Body Division. process on sludge (EPA Hazardous Waste No. F006) generated from electroplating operations and contained in three on-site surface impoundments on November 14, 1986. To assure that stabilization occurs, the following conditions apply to this exclusion: (1) Mixing ratios shall be monitored continuously to assure consistent treatment. (2) One grab sample of the treated waste shall be taken each hour as it is pumped to the holding area (cell) from each trailer unit. At the end of each production day, the grab samples from the individual trailer units will be composited and the EP toxicity test will be run on each composite sample. If lead or total chromium concentrations exceed 0.315 ppm or if nickel exceeds 2.17 ppm, in the EP extract, the waste will be removed and retreated or disposed of as a hazardous waste. (3) The treated waste shall be pumped into bermed cells which are constructed to assure that the treated waste is identifiable and retrievable (i.e., the material can be removed and either disposed of as a hazardous waste or retreated if conditions 1 or 2 are not met). Failure to satisfy any of these conditions would render the exclusion void. This is a one- time exclusion, applicable only to the residue generated from the use of the Chemfix [reg] treatment process on the sludge currently contained in the three on-site surface impoundments. General Motors Flint, Michigan.. Waste water treatment plant Corporation, sludge, F019, that is generated Flint Truck. by General Motors Corporation at Flint Truck, Flint, Michigan at a maximum annual rate of 3,000 cubic yards per year. The sludge must be disposed of in a lined landfill with leachate collection, which is licensed, permitted, or otherwise authorized to accept the delisted wastewater treatment sludge in accordance with 40 CFR part 258. The exclusion becomes effective as of July 30, 2003. The conditions in paragraphs (2) through (5) for Ford Motor Company--Michigan Truck Plant and Wayne Integrated Stamping Plant-- Wayne, Michigan also apply. Delisting Levels: (A) The TCLP concentrations measured in any sample may not exceed the following levels (mg/L): Antimony--0.494; Arsenic--0.224; Cadmium--0.36; Chromium--3.71; Lead--5; Nickel--67.8; Selenium-- 1; Thallium--0.211; Tin--540; Zinc--673; p-Cresol--8.55; and Formaldehyde--63. (B) The total concentrations measured in any sample may not exceed the following levels (mg/kg): Mercury--6.34; and Formaldehyde-- 535. (C) The sum of the ratios of the TCLP concentration to the delisting level for nickel and thallium and for nickel and cadmium shall not exceed 1.0. General Motors Detroit, Michigan Waste water treatment plant Corporation, sludge, F019, that is generated Hamtramck. by General Motors Corporation at Hamtramck, Detroit, Michigan at a maximum annual rate of 3,000 cubic yards per year. The sludge must be disposed of in a lined landfill with leachate collection, which is licensed, permitted, or otherwise authorized to accept the delisted wastewater treatment sludge in accordance with 40 CFR part 258. The exclusion becomes effective as of July 30, 2003. The conditions in paragraphs (2) through (5) for Ford Motor Company--Michigan Truck Plant and Wayne Integrated Stamping Plant-- Wayne, Michigan also apply. A maximum allowable groundwater concentration of 3,750 [micro]g/L for n-butyl alcohol is added to paragraph (5)(e). Delisting Levels: (A) The TCLP concentrations measured in any sample may not exceed the following levels (mg/L): Antimony--0.494; Arsenic--0.224; Cadmium--0.36; Chromium--3.71; Lead--5; Nickel--67.8; Selenium-- 1; Thallium--0.211; Tin--540; Zinc--673; p-Cresol--8.55; Formaldehyde--63; and n-Butyl alcohol--171. (B) The total concentrations measured in any sample may not exceed the following levels (mg/kg): Mercury--6.34; and Formaldehyde-- 535. (C) The sum of the ratios of the TCLP concentration to the delisting level for nickel and thallium and for nickel and cadmium shall not exceed 1.0. [[Page 145]] General Motors Janesville, Wastewater treatment sludge, F019, Corporation, Wisconsin. that is generated at the General Janesville Truck Motors Corporation (GM) Assembly Plant Janesville Truck Assembly Plant (JTAP) at a maximum annual rate of 3,000 cubic yards per year. The sludge must be disposed of in a lined landfill with leachate collection, which is licensed, permitted, or otherwise authorized to accept the delisted wastewater treatment sludge in accordance with 40 CFR part 258. The exclusion becomes effective as of January 24, 2006. 1. Delisting Levels: (A) The concentrations in a TCLP extract of the waste measured in any sample may not exceed the following levels (mg/L): antimony--0.49; arsenic--0.22; cadmium--0.36; chromium--3.7; lead--5; nickel--68; selenium--1; thallium--0.21; tin--540; zinc-- 670; p-cresol--8.5; and formaldehyde--43. (B) The total concentrations measured in any sample may not exceed the following levels (mg/kg): chromium--5,300; mercury--7; and formaldehyde--540. 2. Quarterly Verification Testing: To verify that the waste does not exceed the specified delisting levels, GM must collect and analyze one representative sample of JTAP's sludge on a quarterly basis. 3. Changes in Operating Conditions: GM must notify the EPA in writing if the manufacturing process, the chemicals used in the manufacturing process, the treatment process, or the chemicals used in the treatment process at JTAP significantly change. GM must handle wastes generated at JTAP after the process change as hazardous until it has demonstrated that the waste continues to meet the delisting levels and that no new hazardous constituents listed in appendix VIII of part 261 have been introduced and GM has received written approval from EPA. 4. Data Submittals: GM must submit the data obtained through verification testing at JTAP or as required by other conditions of this rule to EPA Region 5, Waste Management Branch (DW-8J), 77 W. Jackson Blvd., Chicago, IL 60604. The quarterly verification data and certification of proper disposal must be submitted annually upon the anniversary of the effective date of this exclusion. GM must compile, summarize, and maintain at JTAP records of operating conditions and analytical data for a minimum of five years. GM must make these records available for inspection. All data must be accompanied by a signed copy of the certification statement in 40 CFR 260.22(i)(12). 5. Reopener Language--(a) If, anytime after disposal of the delisted waste, GM possesses or is otherwise made aware of any data (including but not limited to leachate data or groundwater monitoring data) relevant to the delisted waste at JTAP indicating that any constituent is at a level in the leachate higher than the specified delisting level, or is in the groundwater at a concentration higher than the maximum allowable groundwater concentration in paragraph (e), then GM must report such data in writing to the Regional Administrator within 10 days of first possessing or being made aware of that data. (b) Based on the information described in paragraph (a) and any other information received from any source, the Regional Administrator will make a preliminary determination as to whether the reported information requires Agency action to protect human health or the environment. Further action may include suspending, or revoking the exclusion, or other appropriate response necessary to protect human health and the environment. (c) If the Regional Administrator determines that the reported information does require Agency action, the Regional Administrator will notify GM in writing of the actions the Regional Administrator believes are necessary to protect human health and the environment. The notice shall include a statement of the proposed action and a statement providing GM with an opportunity to present information as to why the proposed Agency action is not necessary or to suggest an alternative action. GM shall have 30 days from the date of the Regional Administrator's notice to present the information. (d) If after 30 days GM presents no further information, the Regional Administrator will issue a final written determination describing the Agency actions that are necessary to protect human health or the environment. Any required action described in the Regional Administrator's determination shall become effective immediately, unless the Regional Administrator provides otherwise. (e) Maximum Allowable Groundwater Concentrations (mg/L):; antimony-- 0.006; arsenic--0.005; cadmium-- 0.005; chromium--0.1; lead-- 0.015; nickel--0.750; selenium-- 0.050; tin--23; zinc--11; p- Cresol--0.190; and formaldehyde-- 0.950. General Motors Lansing, Michigan Wastewater treatment plant (WWTP) Corporation. sludge from the chemical Lansing Car conversion coating (phosphate Assembly--Body coating) of aluminum (EPA Plant. Hazardous Waste No. F019) generated at a maximum annual rate of 1,250 cubic yards per year and disposed of in a Subtitle D landfill, after May 16, 2000. 1. Delisting Levels: (A) The constituent concentrations measured in the TCLP extract may not exceed the following levels (mg/L): Antimony--0.576; Arsenic--4.8; Barium--100; Beryllium--0.384; Cadmium--0.48; Chromium (total)--5; Cobalt--201.6; Copper--124.8; Lead--1.44; Mercury--0.192; Nickel--67.2; Selenium--1; Silver--5; Thallium--0.192; Tin--2016; Vanadium--28.8; Zinc--960; Cyanide--19.2; Fluoride--384; Acetone--336; m,p--Cresol-- 19.2; 1,1--Dichloroethane-- 0.0864; Ethylbenzene--67.2; Formaldehyde--672; Phenol-- 1920; Toluene--96; 1,1,1-- Trichloroethane--19.2; Xylene-- 960. (B) The total concentration of formaldehyde in the waste may not exceed 2100 mg/kg. [[Page 146]] (C) Analysis for determining reactivity from sulfide must be added to verification testing when an EPA-approved method becomes available. 2. Verification Testing: GM must implement an annual testing program to demonstrate that the constituent concentrations measured in the TCLP extract (or OWEP, where appropriate) of the waste do not exceed the delisting levels established in Condition (1). 3. Changes in Operating Conditions: If GM significantly changes the manufacturing or treatment process or the chemicals used in the manufacturing or treatment process, GM must notify the EPA of the changes in writing. GM must handle wastes generated after the process change as hazardous until GM has demonstrated that the wastes meet the delisting levels set forth in Condition (1), that no new hazardous constituents listed in Appendix VIII of Part 261 have been introduced, and GM has received written approval from EPA. 4. Data Submittals: GM must submit the data obtained through annual verification testing or as required by other conditions of this rule to U.S. EPA Region 5, 77 W. Jackson Blvd. (DW-8J), Chicago, IL 60604, within 60 days of sampling. GM must compile, summarize, and maintain on site for a minimum of five years records of operating conditions and analytical data. GM must make these records available for inspection. All data must be accompanied by a signed copy of the certification statement in 40 CFR 260.22(i)(12). 5. Reopener Language--(a) If, anytime after disposal of the delisted waste, GM possesses or is otherwise made aware of any environmental data (including but not limited to leachate data or groundwater monitoring data) or any other data relevant to the delisted waste indicating that any constituent identified in Condition (1) is at a level in the leachate higher than the delisting level established in Condition (1), or is at a level in the ground water or soil higher than the level predicted by the CML model, then GM must notify the Regional Administrator in writing within 10 days and must report the data within 45 days of first possessing or being made aware of that data. (b) Based on the information described in paragraph (a) and any other information received from any source, the Regional Administrator will make a preliminary determination as to whether the reported information requires Agency action to protect human health or the environment. Further action may include suspending, or revoking the exclusion, or other appropriate response necessary to protect human health and the environment. (c) If the Regional Administrator determines that the reported information does require Agency action, the Regional Administrator will notify GM in writing of the actions the Regional Administrator believes are necessary to protect human health and the environment. The notice shall include a statement of the proposed action and a statement providing GM with an opportunity to present information as to why the proposed Agency action is not necessary or to suggest an alternative action. GM shall have 10 days from the date of the Regional Administrator's notice to present the information. (d) If after 10 days GM presents no further information, the Regional Administrator will issue a final written determination describing the Agency actions that are necessary to protect human health or the environment. Any required action described in the Regional Administrator's determination shall become effective immediately, unless the Regional Administrator provides otherwise. General Motors Pontiac, Michigan Waste water treatment plant Corporation, sludge, F019, that is generated Pontiac East. by General Motors Corporation at Pontiac East, Pontiac, Michigan at a maximum annual rate of 3,000 cubic yards per year. The sludge must be disposed of in a lined landfill with leachate collection, which is licensed, permitted, or otherwise authorized to accept the delisted wastewater treatment sludge in accordance with 40 CFR part 258. The exclusion becomes effective as of July 30, 2003. The conditions in paragraphs (2) through (5) for Ford Motor Company--Michigan Truck Plant and Wayne Integrated Stamping Plant-- Wayne, Michigan also apply. Delisting Levels: (A) The TCLP concentrations measured in any sample may not exceed the following levels (mg/L): Antimony--0.494; Arsenic--0.224; Cadmium--0.36; Chromium--3.71; Lead--5; Nickel--67.8; Selenium-- 1; Thallium--0.211; Tin--540; Zinc--673; p-Cresol--8.55; and Formaldehyde--63. (B) The total concentrations measured in any sample may not exceed the following levels (mg/kg): Mercury--6.34; and Formaldehyde-- 535. (C) The sum of the ratios of the TCLP concentrations to the delisting levels for nickel and thallium and for nickel and cadmium shall not exceed 1.0. Geological Morrisville, Wastewater treatment sludge filter Reclamation Pennsylvania. cake from the treatment of EPA Operations and Hazardous Waste No. F039, Waste Systems, generated at a maximum annual Inc. rate of 2000 cubic yards, after December 4, 2001, and disposed of in a Subtitle D landfill. The exclusion covers the filter cake resulting from the treatment of hazardous waste leachate derived from only ``old'' GROWS and non- hazardous leachate derived from only non-hazardous waste sources. The exclusion does not address the waste disposed of in the ``old'' GROWS' Landfill or the grit generated during the removal of heavy solids from the landfill leachate. To ensure that hazardous constituents are not present in the filter cake at levels of regulatory concern, GROWS must implement a testing program for the petitioned waste. This testing program must meet the conditions listed below in order for the exclusion to be valid: [[Page 147]] (1) Testing: Sample collection and analyses, including quality control (QC) procedures, must be performed using appropriate methods. As applicable to the method-defined parameters of concern, analyses requiring the use of SW-846 methods incorporated by reference in 40 CFR 260.11 must be used without substitution. As applicable, the SW-846 methods might include Methods 0010, 0011, 0020, 0023A, 0030, 0031, 0040, 0050, 0051, 0060, 0061, 1010A, 1020B, 1110A, 1310B, 1311, 1312, 1320, 1330A, 9010C, 9012B, 9040C, 9045D, 9060A, 9070A (uses EPA Method 1664, Rev. A), 9071B, and 9095B. (A) Sample Collection: Each batch of waste generated over a four- week period must be collected in containers with a maximum capacity of 20-cubic yards. At the end of the four-week period, each container must be divided into four quadrants and a single, full-depth core sample shall be collected from each quadrant. All of the full-depth core samples then must be composited under laboratory conditions to produce one representative composite sample for the four-week period. (B) Sample Analysis: Each four- week composite sample must be analyzed for all of the constituents listed in Condition (3). The analytical data, including quality control information, must be submitted to The Waste and Chemicals Management Division, U.S. EPA Region III, 1650 Arch Street, Philadelphia, PA 19103, and the Pennsylvania Department of Environmental Protection, Bureau of Land Recycling and Waste Management, Rachel Carson State Office Building, 400 Market Street, 14th Floor, Harrisburg, PA 17105. Data from the annual verification testing must be compiled and submitted to EPA and the Pennsylvania Department of Environmental Protection within sixty (60) days from the end of the calendar year. All data must be accompanied by a signed copy of the statement set forth in 40 CFR 260.22(i)(12) to certify to the truth and accuracy of the data submitted. Records of operating conditions and analytical data must be compiled, summarized, and maintained on- site for a minimum of three years and must be furnished upon request by any employee or representative of EPA or the Pennsylvania Department of Environmental Protection, and made available for inspection. (2) Waste Holding: The dewatered filter cake must be stored as hazardous until the verification analyses are completed. If the four-week composite sample does not exceed any of the delisting levels set forth in Condition (3), the filter cake waste corresponding to this sample may be managed and disposed of in accordance with all applicable solid waste regulations. If the four-week composite sample exceeds any of the delisting levels set forth in Condition (3), the filter cake waste generated during the time period corresponding to the four-week composite sample must be retreated until it meets these levels (analyses must be repeated) or managed and disposed of in accordance with Subtitle C of RCRA. Filter cake which is generated but for which analyses are not complete or valid must be managed and disposed of in accordance with Subtitle C of RCRA, until valid analyses demonstrate that the waste meets the delisting levels. (3) Delisting Levels: If the concentrations in the four-week composite sample of the filter cake waste for any of the hazardous constituents listed below exceed their respective maximum allowable concentrations (mg/l or mg/kg) also listed below, the four-week batch of failing filter cake waste must either be retreated until it meets these levels or managed and disposed of in accordance with Subtitle C of RCRA. GROWS has the option of determining whether the filter cake waste exceeds the maximum allowable concentrations for the organic constituents by either performing the analysis on a TCLP leachate of the waste or performing total constituent analysis on the waste, and then comparing the results to the corresponding maximum allowable concentration level. ------------------------------------------------------------------------ (A) Inorganics Maximum Allowable Leachate Conc. (mg/ l) Constituent: Arsenic................. 3.00e-01 Barium.................. 2.34e+01 Cadmium................. 1.80e-01 Chromium................ 5.00e+00 Lead.................... 5.00e+00 Mercury................. 7.70e-02 Nickel.................. 9.05e+00 Selenium................ 6.97e-01 Silver.................. 1.23e+00 Cyanide................. 4.33e+00 Cyanide extractions must be conducted using distilled water in place of the leaching media specified in the TCLP procedure. (B) Organics Maximum allowable Maximum allowable leachate conc. (mg/ total conc. (mg/ l) kg) [[Page 148]] Constituent: Acetone................. 2.28e+01 4.56e+02 Acetonitrile............ 3.92e+00 7.84e+01 Acetophenone............ 2.28e+01 4.56e+02 Acrolein................ 1.53e+03 3.06e+04 Acrylonitrile........... 7.80e-03 1.56e-01 Aldrin.................. 5.81e-06 1.16e-04 Aniline................. 7.39e-01 1.48e+01 Anthracene.............. 8.00e+00 1.60e+02 Benz(a)anthracene....... 1.93e-04 3.86e-03 Benzene................. 1.45e-01 2.90e+00 Benzo(a)pyrene.......... 1.18e-05 2.36e-04 Benzo(b)fluoranthene.... 1.07e-04 2.14e-03 Benzo(k)fluoranthene.... 1.49e-03 2.98e-02 Bis(2-chloroethyl)ether. 3.19e-02 6.38e-01 Bis(2- 8.96e-02 1.79e+00 ethylhexyl)phthalate. Bromodichloromethane.... 6.80e-02 1.36e+00 Bromoform 5.33e-01 1.07e+01 (Tribromomethane). Butyl-4,6-dinitrophenol, 2.28e-01 4.56e+00 2-sec-(Dinoseb). Butylbenzylphthalate.... 9.29e+00 1.86e+02 Carbon disulfide........ 2.28e+01 4.56e+02 Carbon tetrachloride.... 4.50e-02 9.00e-01 Chlordane............... 5.11e-04 1.02e-02 Chloro-3-methylphenol 4- 2.97e+02 5.94e+03 Chloroaniline, p-....... 9.14e-01 1.83e+01 Chlorobenzene........... 6.08e+00 1.22e+02 Chlorobenzilate......... 4.85e-02 9.70e-01 Chlorodibromomethane.... 5.02e-02 1.00e+00 Chloroform.............. 7.79e-02 1.56e+00 Chlorophenol, 2-........ 1.14e+00 2.28e+01 Chrysene................ 2.04e-02 4.08e-01 Cresol.................. 1.14e+00 2.28e+01 DDD..................... 5.83e-04 1.17e-02 DDE..................... 1.37e-04 2.74e-03 DDT..................... 2.57e-04 5.14e-03 Dibenz(a,h)anthracene... 5.59e-06 1.12e-04 Dibromo-3-chloropropane, 3.51e-03 7.02e-02 1,2-. Dichlorobenzene 1,3-.... 9.35e+00 1.87e+02 Dichlorobenzene, 1,2-... 1.25e+01 2.50e+02 Dichlorobenzene, 1,4-... 1.39e-01 2.78e+00 Dichlorobenzidine, 3,3'- 9.36e-03 1.87e-01 Dichlorodifluoromethane. 4.57e+01 9.14e+02 Dichloroethane, 1,1-.... 1.20e+00 2.40e+01 Dichloroethane, 1,2-.... 2.57e-03 5.14e-02 Dichloroethylene, 1,1-.. 7.02e-03 1.40e-01 Dichloroethylene, trans- 4.57e+00 9.14e+01 1,2-. Dichlorophenol, 2,4-.... 6.85e-01 1.37e+01 Dichlorophenoxyacetic 2.28e+00 4.56e+01 acid, 2,4-(2,4-D). Dichloropropane, 1,2-... 1.14e-01 2.28e+00 Dichloropropene, 1,3-... 2.34e-02 4.68e-01 Dieldrin................ 6.23e+01 1.25e+03 Diethyl phthalate....... 2.21e+02 4.42e+03 Dimethoate.............. 6.01e+01 1.20e+03 Dimethyl phthalate...... 1.20e+02 2.40e+03 Dimethylbenz(a)anthracen 1.55e-06 3.10e-05 e, 7,12-. Dimethylphenol, 2,4-.... 4.57e+00 9.14e+01 Di-n-butyl phthalate.... 5.29e+00 1.06e+02 Dinitrobenzene, 1,3-.... 2.28e-02 4.56e-01 Dinitromethylphenol, 4,6- 2.16e-02 4.32e-01 ,2-. Dinitrophenol, 2,4-..... 4.57e-01 9.14e+00 Dinitrotoluene, 2,6-.... 6.54e-03 1.31e-01 Di-n-octyl phthalate.... 1.12e-02 2.24e-01 Dioxane, 1,4-........... 3.83e-01 7.66e+00 Diphenylamine........... 3.76e+00 7.52e+01 Disulfoton.............. 3.80e+02 7.60e+03 Endosulfan.............. 1.37e+00 2.74e+01 Endrin.................. 2.00e-02 4.00e-01 Ethylbenzene............ 1.66e+01 3.32e+02 Ethylene Dibromide...... 4.13e-03 8.26e-02 Fluoranthene............ 5.16e-01 1.03e+01 Fluorene................ 1.78e+00 3.56e+01 Heptachlor.............. 8.00e-03 1.60e-01 Heptachlor epoxide...... 8.00e-03 1.60e-01 Hexachloro-1,3-butadiene 9.61e-03 1.92e-01 Hexachlorobenzene....... 9.67e-05 1.93e-03 Hexachlorocyclohexane, 4.00e-01 8.00e+00 gamma-(Lindane). [[Page 149]] Hexachlorocyclopentadien 1.66e+04 3.32e+05 e. Hexachloroethane........ 1.76e-01 3.52e+00 Hexachlorophene......... 3.13e-04 6.26e-03 Indeno(1,2,3-cd) pyrene. 6.04e-05 1.21e-03 Isobutyl alcohol........ 6.85e+01 1.37e+03 Isophorone.............. 4.44e+00 8.88e+01 Methacrylonitrile....... 2.28e-02 4.56e-01 Methoxychlor............ 1.00e+01 2.00e+02 Methyl bromide 1.28e+02 2.56e+03 (Bromomethane). Methyl chloride 1.80e-01 3.60e+00 (Chloromethane). Methyl ethyl ketone..... 1.37e+02 2.74e+03 Methyl isobutyl ketone.. 1.83e+01 3.66e+02 Methyl methacrylate..... 1.03e+03 2.06e+04 Methyl parathion........ 1.27e+02 2.54e+03 Methylene chloride...... 2.88e-01 5.76e+00 Naphthalene............. 1.50e+00 3.00e+01 Nitrobenzene............ 1.14e-01 2.28e+00 Nitrosodiethylamine..... 2.81e-05 5.62e-04 Nitrosodimethylamine.... 8.26e-05 1.65e-03 Nitrosodi-n-butylamine.. 7.80e-04 1.56e-02 N-Nitrosodi-n- 6.02e-04 1.20e-02 propylamine. N-Nitrosodiphenylamine.. 8.60e-01 1.72e+01 N-Nitrosopyrrolidine.... 2.01e-03 4.02e-02 Pentachlorobenzene...... 1.15e-02 2.30e-01 Pentachloronitrobenzene 5.00e-03 1.00e-01 (PCNB). Pentachlorophenol....... 4.10e-03 8.20e-02 Phenanthrene............ 2.09e-01 4.18e+00 Phenol.................. 1.37e+02 2.74e+03 Polychlorinated 3.00e-05 6.00e-04 biphenyls. Pronamide............... 1.71e+01 3.42e+02 Pyrene.................. 3.96e-01 7.92e+00 Pyridine................ 2.28e-01 4.56e+00 Styrene................. 6.08e+00 1.22e+02 Tetrachlorobenzene, 9.43e-03 1.89e-01 1,2,4,5-. Tetrachloroethane, 4.39e-01 8.78e+00 1,1,2,2-. Tetrachloroethylene..... 8.55e-02 1.71e+00 Tetrachlorophenol, 1.81e+00 3.62e+01 2,3,4,6-. Tetraethyl 3.01e+05 6.02e+06 dithiopyrophosphate (Sulfotep). Toluene................. 4.57e+01 9.14e+02 Toxaphene............... 5.00e-01 1.00e+01 Trichlorobenzene, 1,2,4- 7.24e-01 1.45e+01 Trichloroethane, 1,1,1-. 7.60e+00 1.52e+02 Trichloroethane, 1,1,2-. 7.80e-02 1.56e+00 Trichloroethylene....... 3.04e-01 6.08e+00 Trichlorofluoromethane.. 6.85e+01 1.37e+03 Trichlorophenol, 2,4,5-. 9.16e+00 1.83e+02 Trichlorophenol, 2,4,6-. 2.76e-01 5.52e+00 Trichlorophenoxyacetic 2.28e+00 4.56e+01 acid, 2,4,5-(245-T). Trichlorophenoxypropioni 1.00e+00 2.00e+01 c acid, 2,4,5-(Silvex). Trichloropropane, 1,2,3- 7.69e-04 1.54e-02 Trinitrobenzene, sym-... 6.49e+00 1.30e+02 Vinyl chloride.......... 2.34e-03 4.68e-02 Xylenes (total)......... 3.20e+02 6.40e+03 Table 1--Wastes Excluded From Non-Specific Sources ------------------------------------------------------------------------ Facility Address Waste description ------------------------------------------------------------------------ (4) Changes in Operating Conditions: If GROWS significantly changes the treatment process or the chemicals used in the treatment process, GROWS may not manage the treatment sludge filter cake generated from the new process under this exclusion until it has met the following conditions: (a) GROWS must demonstrate that the waste meets the delisting levels set forth in Paragraph 3; (b) it must demonstrate that no new hazardous constituents listed in Appendix VIII of Part 261 have been introduced into the manufacturing or treatment process: and (c) it must obtain prior written approval from EPA and the Pennsylvania Department of Environmental Protection to manage the waste under this exclusion. (5) Reopener: (a) If GROWS discovers that a condition at the facility or an assumption related to the disposal of the excluded waste that was modeled or predicted in the petition does not occur as modeled or predicted, then GROWS must report any information relevant to that condition, in writing, to the Regional Administrator or his delegate and to the Pennsylvania Department of Environmental Protection within 10 days of discovering that condition. (b) Upon receiving information described in paragraph (a) of this section, regardless of its source, the Regional Administrator or his delegate and the Pennsylvania Department of Environmental Protection will determine whether the reported condition requires further action. Further action may include repealing the exclusion, modifying the exclusion, or other appropriate response necessary to protect human health and the environment. [[Page 150]] Goodyear Tire and Randleman, NC.... Dewatered wastewater treatment Rubber Co. sludges (EPA Hazardous Waste No. F006) generated from electroplating operations. Gould, Inc....... McConnels ville, Wastewater treatment sludge (EPA OH. Hazardous Waste No. F006) generated from electroplating operations after November 27, 1985. Hoechst Celanese Bucks, Alabama... Distillation bottoms generated (at Corporation. a maximum annual rate of 31,500 cubic yards) from the production of sodium hydrosulfite (EPA Hazardous Waste No. F003). This exclusion was published on July 17, 1990. This exclusion does not include the waste contained in Hoechst Celanese's on-site surface impoundment. Hoechst Celanese Leeds, South Distillation bottoms generated (at Corporation. Carolina. a maximum annual rate of 38,500 cubic yards) from the production of sodium hydrosulfite (EPA Hazardous Waste No. F003). This exclusion was published on July 17, 1990. Hanover Wire Hanover, Dewatered filter cake (EPA Cloth Division. Pennsylvania. Hazardous Waste No. F006) generated from electroplating operations after August 15, 1986. Holston Army Kingsport, Dewatered wastewater treatment Ammunition Plant. Tennessee. sludges (EPA Hazardous Waste Nos. F003, F005, and K044) generated from the manufacturing and processing of explosives and containing spent non-halogenated solvents after November 14, 1986. Imperial Clevite. Salem, IN........ Solid resin cakes containing EPA Hazardous Waste No. F002 generated after August 27, 1985, from solvent recovery operations. Indiana Steel & Munci, IN........ Dewatered wastewater treatment Wire Corporation sludges (EPA Hazardous Waste Nos. (formerly F006 and K062) generated from General Cable electroplating operations and Co.). steel finishing operations after October 24, 1986. This exclusion does not apply to sludges in any on-site impoundments as of this date. International Terre Haute, Spent non-halogenated solvents and Minerals and Indiana. still bottoms (EPA Hazardous Chemical Waste No. F003) generated from Corporation. the recovery of n-butyl alchohol after August 15, 1986. Kawneer Company, Springdale, Wastewater treatment filter press Incorporated. Arkansas. sludge (EPA Hazardous Waste No. F019) generated (at a maximum annual rate of 26 cubic yards) from the chemical conversion coating of aluminum. This exclusion was published on November 13, 1990. Kay-Fries, Inc... Stoney Point, NY. Biological aeration lagoon sludge and filter press sludge generated after September 21, 1984, which contain EPA Hazardous Waste Nos. F003 and F005 as well as that disposed of in a holding lagoon as of September 21, 1984. Keymark Corp..... Fonda, NY........ Wastewater treatment sludge (EPA Hazardous Waste No. F019) generated from chemical conversion coating of aluminum after November 27, 1985. Keymark Corp..... Fonda, NY........ Wastewater treatment sludges (EPA Hazardous Waste No. F019) generated from the chemical conversion coating of aluminum and contained in an on-site impoundment on August 12, 1987. This is a one-time exclusion. Lawrence Berkeley Berkeley, Treated ignitable and spent National California. halogenated and non-halogenated Laboratory. solvent mixed waste (D001, F002, F003, and F005), and bubbler water on silica gel generated during treatment at the National Tritium Labeling Facility (NTLF) of the Lawrence Berkeley National Laboratory (LBNL). This is a one- time exclusion for 200 U.S. gallons of treatment residues that will be disposed of in a Nuclear Regulatory Commission (NRC) licensed or Department of Energy (DOE) approved low-level radioactive waste disposal facility, after August 7, 2003. (1) Waste Management: The treated waste residue and bubbler water on silica gel must be managed in accordance with DOE or NRC requirements prior to and during disposal. (2) Reopener Language: (A) If, anytime after disposal of the delisted waste, LBNL possesses or is otherwise made aware of any data (including but not limited to leachate data or groundwater monitoring data) relevant to the delisted waste indicating that any organic constituent from the waste is detected in the leachate or the groundwater, then LBNL must report such data, in writing, to the Regional Administrator within 10 days of first possessing or being made aware of that data. (B) Based on the information described in paragraph (2)(A) and any other information received from any source, the Regional Administrator will make a preliminary determination as to whether the reported information requires Agency action to protect human health or the environment. Further action may include suspending, or revoking the exclusion, or other appropriate response necessary to protect human health and the environment. (C) If the Regional Administrator determines that the reported information does require Agency action, the Regional Administrator will notify LBNL in writing of the actions the Regional Administrator believes are necessary to protect human health and the environment. The notice shall include a statement of the proposed action and a statement providing LBNL with an opportunity to present information as to why the proposed Agency action is not necessary or to suggest an alternative action. LBNL shall have 30 days from the date of the Regional Administrator's notice to present the information. (D) If after 30 days LBNL presents no further information, the Regional Administrator will issue a final written determination describing the Agency actions that are necessary to protect human health or the environment. Any required action described in the Regional Administrator's determination shall become effective immediately, unless the Regional Administrator provides otherwise. [[Page 151]] (3) Notification Requirements: LBNL must do the following before transporting the delisted waste off-site:(A) Provide a one-time written notification to any State Regulatory Agency to which or through which they will transport the delisted waste described above for disposal, 60 days before beginning such activities. (B) Update the one-time written notification if LBNL ships the delisted waste to a different disposal facility. Failure to provide this notification will result in a violation of the delisting petition and a possible revocation of the exclusion. Lederle Pearl River, NY.. Spent non-halogenated solvents and Laboratories. still bottoms (EPA Hazardous Waste Nos. F003 and F005) generated from the recovery of the following solvents: Xylene, acetone, ethyl acetate, ethyl ether, methyl isobutyl ketone, n- butyl alcohol, cyclohexanone, methanol, toluene, and pyridine after August 2, 1988. Excusion applies to primary and secondary filter press sludges and compost soils generated from these sludges. Lincoln Plating Lincoln, NE...... Wastewater treatment sludges (EPA Company. Hazardous Waste No. F006) generated from electroplating operations after November 17, 1986. Loxcreen Company, Hayti, MO........ Dewatered wastewater treatment Inc.. sludges (EPA Hazardous Waste No. F019) generated from the chemical conversion coating of aluminum after July 16, 1986. MAHLE, Inc....... Morristown, Wastewater treatment sludge filter Tennessee. cake (EPA Hazardous Waste No. F019) generated from the chemical conversion coating of aluminum (generated at a maximum annual rate of 33 cubic yards), after August 21, 1992. In order to confirm that the characteristics of the waste do not change significantly, the facility must, on an annual basis sample and test for the constituents listed in 40 CFR 261.24 using the method specified therein. The annual analytical results (including quality control information) must be compiled, certified according to 40 CFR 260.22(i)(12), maintained on-site for a minimum of five years, and made available for inspection upon request by representatives of EPA or the State of Tennessee. Failure to maintain the required records on- site will be considered by EPA, at its discretion, sufficient basis to revoke the exclusion to the extent directed by EPA. Marquette Milwaukee, Wastewater treatment sludge (EPA Electronics Wisconsin. Hazardous Waste No. F006) Incorporated. generated from electroplating operations. This exclusion was published on April 20, 1989. Martin Marietta Ocala, Florida... Dewatered wastewater treatment Aerospace. sludges (EPA Hazardous Waste No. F006) generated from electroplating operations after January 23, 1987. Mason Bay St. Louis, Wastewater treatment sludge filter Chamberlain, Mississippi. cake (EPA Hazardous Waste No. Incorporated. F019) generated (at a maximum annual rate of 1,262 cubic yards) from the chemical conversion coating of aluminum. This exclusion was published on October 27, 1989. Maytag Company... Newton, IA....... Wastewater treatment sludges (EPA Hazardous Waste No. F006) generated from electroplating operations and wastewater treatment sludges (EPA Hazardous Waste No. F019) generated from the chemical conversion coating of aluminum November 17, 1986. McDonnell Douglas Tulsa, Oklahoma.. Stabilized wastewater treatment Corporation. sludges from surface impoundments previously closed as a landfill (at a maximum generation of 85,000 cubic yards on a one-time basis). EPA Hazardous Waste No. F019, F002, F003, and F005 generated at U.S. Air Force Plant No. 3, Tulsa, Oklahoma and is disposed of in Subtitle D landfills after February 26, 1999. McDonnell Douglas must implement a testing program that meets the following conditions for the exclusion to be valid: (1) Delisting Levels: All leachable concentrations for the constituents in Conditions (1)(A) and (1)(B) in the approximately 5,000 cubic yards of combined stabilization materials and excavated sludges from the bottom portion of the northwest lagoon of the surface impoundments which are closed as a landfill must not exceed the following levels (ppm) after the stabilization process is completed in accordance with Condition (3). Constituents must be measured in the waste leachate by the method specified in 40 CFR 261.24. Cyanide extractions must be conducted using distilled water in the place of the leaching media per 40 CFR 261.24. Constituents in Condition (1)(C) must be measured as the total concentrations in the waste(ppm). (A) Inorganic Constituents (leachate) Antimony-0.336; Cadmium-0.280; Chromium (total)-5.0; Lead-0.84; Cyanide-11.2; (B) Organic Constituents (leachate) Benzene-0.28; trans-1,2- Dichloroethene-5.6; Tetrachloroethylene-0.280; Trichloroethylene-0.280 (C) Organic Constituents (total analysis). Benzene-10.; Ethylbenzene-10.; Toluene-30.; Xylenes-30.; trans- 1,2-Dichloroethene-30.; Tetrachloroethylene-6.0; Trichloroethylene-6.0. McDonnell Douglas Corporation shall control volatile emissions from the stabilization process by collection of the volatile chemicals as they are emitted from the waste but before release to the ambient air. and the facility shall use dust control measures. These two controls must be adequate to protect human health and the environment. The approximately 80,000 cubic yards of previously stabilized waste in the upper northwest lagoon, entire northeast lagoon, and entire south lagoon of the surface impoundments which were closed as a landfill requires no verification testing. [[Page 152]] (2) Waste Holding and Handling: McDonnell Douglas must store as hazardous all stabilized waste from the bottom portion of the northwest lagoon area of the closed landfill as generated until verification testing as specified in Condition (3), is completed and valid analyses demonstrate that Condition (1) is satisfied. If the levels of constituents measured in the samples of the stabilized waste do not exceed the levels set forth in Condition (1), then the waste is nonhazardous and may be managed and disposed of in a Subtitle D landfill in accordance with all applicable solid waste regulations. If constituent levels in a sample exceed any of the delisting levels set in Condition (1), the waste generated during the time period corresponding to this sample must be restabilized until delisting levels are met or managed and disposed of in accordance with Subtitle C of RCRA. (3) Verification Testing Requirements: Sample collection and analyses, including quality control procedures, must be performed using appropriate methods. As applicable to the method-defined parameters of concern, analyses requiring the use of SW-846 methods incorporated by reference in 40 CFR 260.11 must be used without substitution. As applicable, the SW-846 methods might include Methods 0010, 0011, 0020, 0023A, 0030, 0031, 0040, 0050, 0051, 0060, 0061, 1010A, 1020B, 1110A, 1310B, 1311, 1312, 1320, 1330A, 9010C, 9012B, 9040C, 9045D, 9060A, 9070A (uses EPA Method 1664, Rev. A), 9071B, and 9095B. McDonnell Douglas must stabilize the previously unstabilized waste from the bottom portion of the northwest lagoon of the surface impoundment (which was closed as a landfill) using fly ash, kiln dust or similar accepted materials in batches of 500 cubic yards or less. McDonnell Douglas must analyze one composite sample from each batch of 500 cubic yards or less. A minimum of four grab samples must be taken from each waste pile (or other designated holding area) of stabilized waste generated from each batch run. Each composited batch sample must be analyzed, prior to disposal of the waste in the batch represented by that sample, for constituents listed in Condition (1). There are no verification testing requirements for the stabilized wastes in the upper portions of the northwest lagoon, the entire northeast lagoon, and the entire south lagoon of the surface impoundments which were closed as a landfill. (4) Changes in Operating Conditions: If McDonnell Douglas significantly changes the stabilization process established under Condition (3) (e.g., use of new stabilization agents), McDonnell Douglas must notify the Agency in writing. After written approval by EPA, McDonnell Douglas may handle the wastes generated as non-hazardous, if the wastes meet the delisting levels set in Condition (1). (5) Data Submittals: Records of operating conditions and analytical data from Condition (3) must be compiled, summarized, and maintained on site for a minimum of five years. These records and data must be furnished upon request by EPA, or the State of Oklahoma, or both, and made available for inspection. Failure to submit the required data within the specified time period or maintain the required records on site for the specified time will be considered by EPA, at its discretion, sufficient basis to revoke the exclusion to the extent directed by EPA. All data must be accompanied by a signed copy of the following certification statement to attest to the truth and accuracy of the data submitted: Under civil and criminal penalty of law for the making or submission of false or fraudulent statements or representations (pursuant to the applicable provisions of the Federal Code, which include, but may not be limited to, 18 U.S.C. Sec. 1001 and 42 U.S.C. Sec. 6928), I certify that the information contained in or accompanying this document is true, accurate and complete. As to the (those) identified section(s) of this document for which I cannot personally verify its (their) truth and accuracy, I certify as the company official having supervisory responsibility for the persons who, acting under my direct instructions, made the verification that this information is true, accurate and complete. In the event that any of this information is determined by EPA in its sole discretion to be false, inaccurate or incomplete, and upon conveyance of this fact to the company, I recognize and agree that this exclusion of waste will be void as if it never had effect or to the extent directed by EPA and that the company will be liable for any actions taken in contravention of the company's RCRA and CERCLA obligations premised upon the company's reliance on the void exclusion. (6) Reopener Language (a) If McDonnell Douglas discovers that a condition at the facility or an assumption related to the disposal of the excluded waste that was modeled or predicted in the petition does not occur as modeled or predicted, then McDonnell Douglas must report any information relevant to that condition, in writing, to the Regional Administrator or his delegate within 10 days of discovering that condition. (b) Upon receiving information described in paragraph (a) from any source, the Regional Administrator or his delegate will determine whether the reported condition requires further action. Further action may include revoking the exclusion, modifying the exclusion, or other appropriate response necessary to protect human health and the environment. [[Page 153]] (7) Notification Requirements: McDonnell Douglas must provide a one-time written notification to any State Regulatory Agency to which or through which the delisted waste described above will be transported for disposal at least 60 days prior to the commencement of such activity. The one-time written notification must be updated if the delisted waste is shipped to a different disposal facility. Failure to provide such a notification will result in a violation of the delisting petition and a possible revocation of the decision. Merck & Company, Elkton, Virginia. One-time exclusion for fly ash Incorporated. (EPA Hazardous Waste No. F002) from the incineration of wastewater treatment sludge generated from pharmaceutical production processes and stored in an on-site fly ash lagoon. This exclusion was published on May 12, 1989. Metropolitan Cincinnati, OH... Sluiced bottom ash sludge Sewer District (approximately 25,000 cubic of Greater yards), contained in the North Cincinnati. Lagoon, on September 21, 1984, which contains EPA Hazardous Wastes Nos. F001, F002, F003, F004, and F005. Michelin Tire Sandy Springs, Dewatered wastewater treatment Corp.. South Carolina. sludge (EPA Hazardous Wastes No. F006) generated from electroplating operations after November 14, 1986. Monroe Auto Paragould, AR.... Wastewater treatment sludge (EPA Equipment. Hazardous Waste No. F006) generated from electroplating operations after vacuum filtration after November 27, 1985. This exclusion does not apply to the sludge contained in the on-site impoundment. Nissan North Smyrna, Tennessee Wastewater treatment sludge (EPA America, Inc.. Hazardous Waste No. F019) that Nissan North American, Inc. (Nissan) generates by treating wastewater from automobile assembly plant located on 983 Nissan Drive in Smyrna, Tennessee. This is a conditional exclusion for up to 3,500 cubic yards of waste (hereinafter referred to as ``Nissan Sludge'') that will be generated each year and disposed in a Subtitle D landfill after February 27, 2006. Nissan must continue to demonstrate that the following conditions are met for the exclusion to be valid. (1) Delisting Levels: All leachable concentrations for these metals, cyanide, and organic constituents must not exceed the following levels (ppm): Barium-100.0; Cadmium- 0.422; Chromium-5.0; Cyanide- 7.73, Lead-5.0; and Nickel-60.7; Bis-(2-ethylhexyl) phthalate- 0.601; Di-n-octyl phthalate- 0.0752; and 4-Methylphenol-7.66. These concentrations must be measured in the waste leachate obtained by the method specified in 40 CFR 261.24, except that for cyanide, deionized water must be the leaching medium. Cyanide concentrations in waste or leachate must be measured by the method specified in 40 CFR 268.40, Note 7. (2) Verification Testing Requirements: Sample collection and analyses, including quality control procedures, must be performed using appropriate methods. As applicable to the method-defined parameters of concern, analyses requiring the use of SW-846 methods incorporated by reference in 40 CFR 260.11 must be used without substitution. As applicable, the SW-846 methods might include Methods 0010, 0011, 0020, 0023A, 0030, 0031, 0040, 0050, 0051,