Section

[Code of Federal Regulations]
[Title 40, Volume 17]
[Revised as of July 1, 2008]
From the U.S. Government Printing Office via GPO Access
[CITE: 40CFR82B App A]

[Page 539-545]

TITLE 40--PROTECTION OF ENVIRONMENT

CHAPTER I--ENVIRONMENTAL PROTECTION AGENCY (CONTINUED)

PART 82_PROTECTION OF STRATOSPHERIC OZONE--Table of Contents

Subpart B_Servicing of Motor Vehicle Air Conditioners

Sec. Appendix A to Subpart B of Part 82--Standard for Recycle/Recover
Equipment

Standard of Purity for Use in Mobile Air-Conditioning Systems

Foreword

Due to the CFC's damaging effect on the ozone layer, recycle of CFC-
12 (R-12) used in mobile air-conditioning systems is required to reduce
system venting during normal service operations. Establishing recycle
specifications for R-12 will assure that system operation with recycled
R-12 will provide the same level of performance as new refrigerant.
Extensive field testing with the EPA and the auto industry indicate
that reuse of R-12 removed from mobile air-conditioning systems can be
considered, if the refrigerant is cleaned to a specific standard. The
purpose of this standard is to establish the specific minimum levels of
R-12 purity required for recycled R-12 removed from mobile automotive
air-conditioning systems.

1. Scope

This information applies to refrigerant used to service automobiles,
light trucks, and other vehicles with similar CFC-12 systems. Systems
used on mobile vehicles for refrigerated cargo that have hermetically
sealed, rigid pipe are not covered in this document.

2. References

SAE J1989, Recommended Service Procedure for the Containment of R-12
SAE J1990, Extraction and Recycle Equipment for Mobile Automotive Air-
Conditioning Systems
ARI Standard 700-88

3. Purity Specification

The refrigerant in this document shall have been directly removed
from, and intended to be returned to, a mobile air-conditioning system.
The contaminants in this recycled refrigerant 12 shall be limited to
moisture, refrigerant oil, and noncondensable gases, which shall not
exceed the following level:
3.1 Moisture: 15 ppm by weight.
3.2 Refrigerant Oil: 4000 ppm by weight.
3.3 Noncondensable Gases (air): 330 ppm by wright.

4. Refrigeration Recycle Equipment Used in Direct Mobile Air-
Conditioning Service Operations Requirement

4.1 The equipment shall meet SAE J1990, which covers additional
moisture, acid, and filter requirements.
4.2 The equipment shall have a label indicating that it is certified
to meet this document.

5. Purity Specification of Recycled R-12 Refrigerant Supplied in
Containers From Other Recycle Sources

Purity specification of recycled R-12 refrigerant supplied in
containers from other recycle sources, for service of mobile air-
conditioning systems, shall meet ARI Standard 700-88 (Air Conditioning
and Refrigeration Institute).

6. Operation of the Recycle Equipment

This shall be done in accordance with SAE J1989.

Rationale

Not applicable.

Relationship of SAE Standard to ISO Standard

Not applicable.

Reference Section

SAE J1989, Recommended Service Procedure for the Containment of R-12
SAE J1990, Extraction and Recycle Equipment for Mobile Automotive Air-
Conditioning Systems
ARI Standard 700-88

Application

[[Page 540]]

Committee Composition

Developed by the SAE Defrost and Interior Climate Controls Standards
Committee

W.J. Atkinson, Sun Test Engineering, Paradise Valley, AZ--Chairman
J.J. Amin, Union Lake, MI
H.S. Andersson, Saab Scania, Sweden
P.E. Anglin, ITT Higbie Mfg. Co., Rochester, MI
R.W. Bishop, GMC, Lockport, NY
D. Hawks, General Motors Corporation, Pontiac, MI
J.J. Hernandez, NAVISTAR, Ft. Wayne, IN
H. Kaltner, Volkswagen AG, Germany, Federal Republic
D.F. Last, GMC, Troy, MI
D.E. Linn, Volkswagen of America, Warren, MI
J.H. McCorkel, Freightliner Corp., Charlotte, NC
C.J. McLachlan, Livonia, MI
H.L. Miner, Climate Control Inc., Decatur, IL
R.J. Niemiec, General Motors Corp., Pontiac, MI
N. Novak, Chrysler Corp., Detroit, MI
S. Oulouhojian, Mobile Air Conditioning Society, Upper Darby, PA
J. Phillips, Air International, Australia
R.H. Proctor, Murray Corp., Cockeysville, MD
G. Rolling, Behr America Inc., Ft. Worth, TX
C.D. Sweet, Signet Systems Inc., Harrodsburg, KY
J.P. Telesz, General Motors Corp., Lockport, NY

Extraction and Recycle Equipment for Mobile Automotive Air Conditioning
Systems

SAE Recommended Practice, SAE J1990 (1991) \1\

0. Foreword

Due to the CFC's damaging effect on the ozone layer, recycle of CFC-
12 (R-12) used in mobile air-conditioning systems is required to replace
system venting during normal service operations. Establishing recycle
specifications for R-12 will provide the same level of performance as
new refrigerant.
---------------------------------------------------------------------------

\1\ This standard is appropriate for equipment certified after
February 1, 1992. This equipment may be marked design certified for
compliance with SAE J1990 (1991). The standard for approval for
equipment certified on or before February 1, 1992 is SAE J1990 (1989).
This equipment may be marked design certified for compliance with SAE
J1990 (1989). Both types of equipment are considered approved under the
requirements of this regulation.
---------------------------------------------------------------------------

Extensive field testing with the EPA and the auto industry indicates
that R-12 can be reused, provided that it is cleaned to specifications
in SAE J1991. The purpose of this document is to establish the specific
minimum equipment specification required for recycle of R-12 that has
been directly removed from mobile systems for reuse in mobile automotive
air-conditioning systems.

1. Scope

The purpose of this document is to provide equipment specifications
for CFC-12 (R-12) recycling equipment. This information applies to
equipment used to service automobiles, light trucks, and other vehicles
with similar CFC-12 air-conditioning systems. Systems used on mobile
vehicles for refrigerated cargo that have hermetically sealed systems
are not covered in this document. The equipment in this document is
intended for use with refrigerant that has been directly removed from,
and intended to be returned to, a mobile air-conditioning system. Should
other revisions due to operational or technical requirements occur, this
document may be amended.

2. References

2.1 Applicable Documents:
2.1.1 SAE Publications--Available from SAE, 400 Commonwealth Drive,
Warrendale, PA 15096-0001.

SAE J1991--Standard of Purity for Use in Mobile Air-Conditioning Systems
SAE J2196--Service Hose for Automotive Air-Conditioning

2.1.2 CGA Publications--Available from CGA, Crystal Gateway
1, Ste. 501, 1235 Jefferson Davis Hwy., Arlington, VA 22202

CGA Pamphlet S-1.1--Pressure Relief Device Standard Part 1--Cylinders
for Compressed Gases

3. Specification and General Description

3.1 The equipment must be able to extract and process CFC-12 from
mobile air-conditioning systems. The equipment shall process the
contaminated R-12 samples as defined in 8.4 and shall clean the
refrigerant to the level as defined in SAE J1991.
3.2 The equipment shall be suitable for use in an automotive service
environment and be capable of continuous operation in ambients from 10
to 49 [deg]C.
3.3 The equipment must be certified by Underwriters Laboratories or
an equivalent certifying laboratory.
3.4 The equipment shall have a label ``Design Certified by (Company
Name) to Meet SAE J1991''. The minimum letter size shall be bold type 3
mm in height.

[[Page 541]]

4. Refrigeration Recycle Equipment Requirements

4.1 Moisture and Acid--The equipment shall incorporate a desiccant
package that must be replaced before saturated with moisture and whose
mineral acid capacity is at least 5% by weight of total system dry
desiccant.
4.1.1 The equipment shall be provided with a moisture detection
device that will reliably indicate when moisture in the CFC-12 exceeds
the allowable level and requires the filter/dryer replacement.
4.2 Filter--The equipment shall incorporate an in-line filter that
will trap particulates of 15 [micro]m or greater.
4.3 Noncondensable Gas.
4.3.1 The equipment shall either automatically purge noncondensables
(NCGs) if the acceptable level is exceeded or incorporate a device to
alert the operator that NCG level has been exceeded. NCG removal must be
part of normal operation of the equipment and instructions must be
provided to enable the task to be accomplished within 30 minutes.
4.3.2 Refrigerant loss from noncondensable gas purging during
testing described in Section 8 shall not exceed five percent (5%) by
weight of the total contaminated refrigerant removed from the test
system.
4.3.3 Transfer of Recycled Refrigerant--Recycled refrigerant for
recharging and transfer shall be taken from the liquid phase only.

5. Safety Requirements

5.1 The equipment must comply with applicable federal, state and
local requirements on equipment related to the handling of R-12
material. Safety precautions or notices related to the safe operation of
the equipment shall be prominently displayed on the equipment and should
also state ``Caution--Should Be Operated By Qualified Personnel''.

6. Operating Instructions

6.1 The equipment manufacturer must provide operating instructions,
necessary maintenance procedures, and source information for replacement
parts and repair.
6.2 The equipment must prominently display the manufacturer's name,
address and any items that require maintenance or replacement that
affect the proper operation of the equipment. Operation manuals must
cover information for complete maintenance of the equipment to assure
proper operation.

7. Functional Description

7.1 The equipment must be capable of ensuring recovery of the R-12
from the system being service, by reducing the system pressure below
atmospheric to a minimum of 102 mm of mercury.
7.2 To prevent overcharge, the equipment must be equipped to protect
the tank used to store the recycled refrigerant with a shutoff device
and a mechanical pressure relief valve.
7.3 Portable refillable tanks or containers used in conjunction with
this equipment must meet applicable Department of Transportation (DOT)
or Underwriters Laboratories (UL) Standards and be adaptable to existing
refrigerant service and charging equipment.
7.4 During operation, the equipment shall provide overfill
protection to assure the storage container, internal or external, liquid
fill does not exceed 80% of the tank's rated volume at 21.1 [deg]C (70
[deg]F) per DOT standards, CFR title 49, Sec. 173.304 and American
Society of Mechanical Engineers.
7.4.1 Additional Storage Tank Requirements.
7.4.1.1 The cylinder valve shall comply with the standard for
cylinder valves, UL 1769.
7.4.1.2 The pressure relief device shall comply with the Pressure
Relief Device Standard Part 1--Cylinders for Compressed Gases, CGA
Pamphlet S-1.1.
7.4.1.3 The tank assembly shall be marked to indicate the first
retest date, which shall be 5 years after date of manufacture. The
marking shall indicate that retest must be performed every subsequent 5
years. The marking shall be in letters at least \1/4\ in high.
7.5 All flexible hoses must meet SAE J2196 hose specification
effective January 1, 1992.
7.6 Service hoses must have shutoff devices located within 30 cm (12
in) of the connection point to the system being serviced to minimize
introduction of noncondensable gases into the recovery equipment and the
release of the refrigerant when being disconnected.
7.7 The equipment must be able to separate the lubricant from the
recovered refrigerant and accurately indicate the amount removed during
the process, in 30 ml units. Refrigerant dissolves in lubricant sample.
This creates the illusion that more lubricant has been recovered than
actually has been. The equipment lubricant measuring system must take in
account such dissolved refrigerant to prevent overcharging the vehicle
system with lubricant. Note: Use only new lubricant to replace the
amount removed during the recycle process. Used lubricant should be
discarded per applicable federal, state, and local requirements.
7.8 The equipment must be capable of continuous operation in ambient
of 10 to 49 [deg]C (50 to 120 [deg]F).
7.9 The equipment should be compatible with leak detection material
that may be present in the mobile AC system.

[[Page 542]]

8. Testing

This test procedure and the requirement are used for evaluation of
the equipment for its ability to clean the contaminated R-12
refrigerant.
8.1 The equipment shall clean the contaminated R-12 refrigerant to
the minimum purity level as defined in SAE J1991, when tested in
accordance with the following conditions:
8.2 For test validation, the equipment is to be operated according
to the manufacturer's instructions.
8.3 The equipment must be preconditioned with 13.6 kg (30 lb) of the
standard contaminated R-12 at an ambient of 21 [deg]C (70 [deg]F) before
starting the test cycle. Sample amounts are not to exceed 1.13 kg (2.5
lb) with sample amounts to be repeated every 5 min. The sample method
fixture, defined in Fig. 1, shall be operated at 24 [deg]C (75 [deg]F).
8.4 Contaminated R-12 Samples.
8.4.1 Standard contaminated R-12 refrigerant shall consist of liquid
R-12 with 100 ppm (by weight) moisture at 21 [deg]C (70 [deg]F) and
45,000 ppm (by weight) mineral oil 525 suspension nominal and 770 ppm by
weight of noncondensable gases (air).
8.4.2 High moisture contaminated sample shall consist of R-12 vapor
with 1,000 ppm (by weight) moisture.
8.4.3 High oil contaminated sample shall consist of R-12 with
200,000 ppm (by weight) mineral oil 525 suspension viscosity nominal.
8.5 Test Cycle.
8.5.1 After preconditioning as stated in 8.3, the test cycle is
started, processing the following contaminated samples through the
equipment:
8.5.1.1 3013.6 kg (30 lb) of standard contaminated R-12.
8.5.1.2 1 kg (2.2 lb) of high oil contaminated R-12.
8.5.1.3 4.5 kg (10 lb) of standard contaminated R-12.
8.5.1.4 1 kg (2.2 lb) of high moisture contaminated R-12.
8.6 Equipment Operating Ambient.
8.6.1 The R-12 is to be cleaned to the minimum purity level, as
defined in SAE J1991, with the equipment operating in a stable ambient
of 10, 21, and 49 [deg]C (50, 70, and 120 [deg]F) and processing the
samples as defined in 8.5.
8.7 Sample Analysis.
8.7.1 The processed contaminated sample shall be analyzed according
to the following procedure.
8.8 Quantitative Determination of Moisture.
8.8.1 The recycled liquid phase sample of CFC-12 shall be analyzed
for moisture content via Karl Fischer coulometer titration or an
equivalent method. The Karl Fischer apparatus is an instrument for
precise determination of small amounts of water dissolved in liquid and/
or gas samples.
8.8.2 In conducting the test, a weighed sample of 30 to 130 grams is
vaporized directly into the Karl Fischer analyte. A coulometer titration
is conducted and the results are calculated and displayed as parts per
million moisture (weight).
8.9 Determination of Percent Lubricant.
8.9.1 The amount of oil in the recycled sample of CFC-12 is to be
determined by gravimetric analysis.
8.9.2 Following venting of noncondensable, in accordance with the
manufacturer's operating instructions, the refrigerant container shall
be shaken for 5 minutes prior to extracting samples for test.
8.9.3 A weighted sample of 175 to 225 grams of liquid CFC-12 is
allowed to evaporate at room temperature. The percent oil is to be
calculated from the weight of the original sample and the residue
remaining after the evaporation.
8.10 Noncondensable Gas.
8.10.1 The amount of noncondensable gas is to be determined by gas
chromatography. A sample of vaporized refrigerant liquid shall be
separated and analyzed by gas chromatography. A Porapak Q column at 130
[deg]C and a hot wire detector may be used for analysis.
8.10.2 This test shall be conducted on recycled refrigerant (taken
from the liquid phase) within 30 minutes after the proper venting of
noncondensable.
8.10.3 Samples shall be shaken for 8 hours prior to retesting while
at a temperature of 24 2.8 [deg]C (75 5 [deg]F). Known volumes of refrigerant vapor are to be
injected for separation and analysis by means of gas chromatography. A
Porapak Q column at 130 [deg]C (266 [deg]F) and a hot wire detector are
to be used for the analysis.
8.10.4 This test shall be conducted at 21 and 49 [deg]C and may be
performed in conjunction with the testing defined in Section 8.6. The
equipment shall process at least 13.6 kg of standard contaminated
refrigerant for this test.
8.11 Sample Requirements.
8.11.1 The sample shall be tested as defined in 8.7, 8.8, 8.9, and
8.10 at ambient temperatures of 10, 21, and 49 [deg]C (50, 70, and 120
[deg]F) as defined in 8.6.1.

[[Page 543]]

[GRAPHIC] [TIFF OMITTED] TC01MY92.106

Recommended Service Procedure for the Containment of R-12

1. Scope

During service of mobile air-conditioning systems, containment of
the refrigerant is important. This procedure provides service guidelines
for technicians when repairing vehicles and operating equipment defined
in SAE J1990.

[[Page 544]]

2. References

SAE J1990, Extraction and Recycle Equipment for Mobile Automotive Air-
Conditioning Systems

3. Refrigerant Recovery Procedure

3. 1 Connect the recovery unit service hoses, which shall have
shutoff valves within 12 in (30 cm) of the service ends, to the vehicle
air-conditioning system service ports.
3.2 Operate the recovery equipment as covered by the equipment
manufacturers recommended procedure.
3.2.1 Start the recovery process and remove the refrigerant from the
vehicle AC system. Operate the recovery unit until the vehicle system
has been reduced from a pressure to a vacuum. With the recovery unit
shut off for at least 5 min, determine that there is no refrigerant
remaining in the vehicle AC system. If the vehicle system has pressure,
additional recovery operation is required to remove the remaining
refrigerant. Repeat the operation until the vehicle AC system vacuum
level remains stable for 2 min.
3.3 Close the valves in the service lines and then remove the
service lines from the vehicle system. Proceed with the repair/service.
If the recovery equipment has automatic closing valves, be sure they are
properly operating.

4. Service With Manifold Gage Set

4.1 Service hoses must have shutoff valves in the high, low, and
center service hoses within 12 in (30 cm) of the service ends. Valves
must be closed prior to hose removal from the air-conditioning system.
This will reduce the volume of refrigerant contained in the service hose
that would otherwise be vented to atmosphere.
4.2 During all service operations, the valves should be closed until
connected to the vehicle air-conditioning system or the charging source
to avoid introduction of air and to contain the refrigerant rather than
vent open to atmosphere.
4.3 When the manifold gage set is disconnected from the air-
conditioning system or when the center hose is moved to another device
which cannot accept refrigerant pressure, the gage set hoses should
first be attached to the reclaim equipment to recover the refrigerant
from the hoses.

5. Recycled Refrigerant Checking Procedure for Stored Portable Auxiliary
Container

5.1 To determine if the recycled refrigerant container has excess
noncondensable gases (air), the container must be stored at a
temperature of 65 [deg]F (18.3 [deg]C) or above for a period of time, 12
h, protected from direct sun.
5.2 Install a calibrated pressure gage, with 1 psig divisions (0.07
kg), to the container and determine the container pressure.
5.3 With a calibrated thermometer, measure the air temperature
within 4 in (10 cm) of the container surface.
5.4 Compare the observed container pressure and air temperature to
determine if the container exceeds the pressure limits found on Table 1,
e.g., air temperature 70 [deg]F (21 [deg]C) pressure must not exceed 80
psig (5.62 kg/cm \2\).

Table 1
----------------------------------------------------------------------------------------------------------------
Temp Temp Temp Temp Temp
[deg]F Psig [deg]F Psig [deg]F Psig [deg]F Psig [deg]F Psig
----------------------------------------------------------------------------------------------------------------
65 74 75 87 85 102 95 118 105 136
66 75 76 88 86 103 96 120 106 138
67 76 77 90 87 105 97 122 107 140
68 78 78 92 88 107 98 124 108 142
69 79 79 94 89 108 99 125 109 144
70 80 80 96 90 110 100 127 110 146
71 82 81 98 91 111 101 129 111 148
72 83 82 99 92 113 102 130 112 150
73 84 83 100 93 115 103 132 113 152
74 86 84 101 94 116 104 134 114 154
----------------------------------------------------------------------------------------------------------------

Table 1 (Metric)
----------------------------------------------------------------------------------------------------------------
Temp Temp Temp Temp Temp
[deg]C Pres [deg]C Pres [deg]C Pres [deg]C Pres [deg]C PRres
----------------------------------------------------------------------------------------------------------------
18.3 5.20 23.9 6.11 29.4 7.17 35.0 8.29 40.5 9.56
18.8 5.27 24.4 6.18 30.0 7.24 35.5 8.43 41.1 9.70
19.4 5.34 25.0 6.32 30.5 7.38 36.1 8.57 41.6 9.84
20.0 5.48 25.5 6.46 31.1 7.52 36.6 8.71 42.2 9.98
20.5 5.55 26.1 6.60 31.6 7.59 37.2 8.78 42.7 10.12
21.1 5.62 26.6 6.74 32.2 7.73 37.7 8.92 43.3 10.26
21.6 5.76 27.2 6.88 32.7 7.80 38.3 9.06 43.9 10.40
22.2 5.83 27.7 6.95 33.3 7.94 38.8 9.13 44.4 10.54
22.7 5.90 28.3 7.03 33.9 8.08 39.4 9.27 45.0 10.68
23.3 6.04 28.9 7.10 34.4 8.15 40.0 9.42 45.5 10.82
----------------------------------------------------------------------------------------------------------------
Pres kg/sq cm.

[[Page 545]]

5.5 If the container pressure is less than the Table 1 values and
has been recycled, limits of noncondensable gases (air) have not been
exceeded and the refrigerant may be used.
5.6 If the pressure is greater than the range and the container
contains recycled material, slowly vent from the top of the container a
small amount of vapor into the recycle equipment until the pressure is
less than the pressure shown on Table 1.
5.7 If the container still exceeds the pressure shown on Table 1,
the entire contents of the container shall be recycled.

6. Containers for Storage of Recycled Refrigerant

6.1 Recycled refrigerant should not be salvaged or stored in
disposable refrigerant containers. This is the type of container in
which virgin refrigerant is sold. Use only DOT CFR title 49 or UL
approved storage containers for recycled refrigerant.
6.2 Any container of recycled refrigerant that has been stored or
transferred must be checked prior to use as defined in section 5.

7. Transfer of Recycled Refrigerant

7.1 When external portable containers are used for transfer, the
container must be evacuated at least 27 in of vacuum (75 mm Hg absolute
pressure) prior to transfer of the recycled refrigerant. External
portable containers must meet DOT and UL standards.
7.2 To prevent on-site overfilling when transferring to external
containers, the safe filling level must be controlled by weight and must
not exceed 60% of container gross weight rating.

8. Disposal of Empty/Near Empty Containers

8.1 Since all the refrigerant may not be removed from disposable
refrigerant containers during normal system charging procedures, empty/
near empty container contents should be reclaimed prior to disposal of
the container.
8.2 Attach the container to the recovery unit and remove the
remaining refrigerant. When the container has been reduced from a
pressure to a vacuum, the container valve can be closed. The container
should be marked empty and is ready for disposal.

Rationale

Not applicable.

Relationship of SAE Standard to ISO Standard.

Not applicable.

Reference Section

SAE J1990, Extraction and Recycle Equipment for Mobile Automotive Air-
Conditioning Systems

Application

Committee Composition

Developed by the SAE Defrost and Interior Climate Control Standards
Committee

W.J. Atkinson, Sun Test Engineering, Paradise Valley, AZ--Chairman
J.J. Amin, Union Lake, MI
H.S. Andersson, Saab Scania, Sweden
P.E. Anglin, ITT Higbie Mfg. Co., Rochester, MI
R.W. Bishop, GMC, Lockport, NY
D.Hawks, General Motors Corporation, Pontiac, MI
J.J. Hernandez, NAVISTAR, Ft. Wayne, IN
H. Kaltner, Volkswagen AG, Germany, Federal Republic
D.F. Last, GMC, Troy, MI
D.E. Linn, Volkswagen of America, Warren, MI
J.H. McCorkel, Freightliner Corp., Charlotte, NC
C.J. McLachlan, Livonia, MI
H.L. Miner, Climate Control Inc., Decatur, IL
R.J. Niemiec, General Motors Corp., Pontiac, MI
N. Novak, Chrysler Corp., Detroit, MI
S. Oulouhojian, Mobile Air Conditioning Society, Upper Darby, PA
J. Phillips, Air International, Australia
R.H. Proctor, Murray Corp., Cockeysville, MD
G. Rolling, Behr America Inc., Ft. Worth, TX
C.D. Sweet, Signet Systems Inc., Harrodsburg, KY
J.P. Telesz, General Motors Corp., Lockport, NY